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    • 1. 发明授权
    • Process for preparing thermoset composite articles
    • 制备热固性复合制品的方法
    • US5672311A
    • 1997-09-30
    • US859636
    • 1992-03-20
    • Clayton A. MayWalter V. BreitigamRonald S. Bauer
    • Clayton A. MayWalter V. BreitigamRonald S. Bauer
    • B29C70/06B29C70/42B29K105/06B32B27/06B32B37/00C08J3/24C08J5/24B29B17/00
    • C08J3/244B29C70/42C08J5/24
    • A process for preparing thermoset composite articles under relatively mild conditions includes exposing a laminate containing a partially-cured thermosettable resin and a fibrous substrate to an elevated temperature which increases over time, the elevated temperature being below the glass transition temperature of the resin but sufficient to promote further curing and increase the glass transition temperature thereof to the ultimate glass transition temperature of the resin. The temperature of exposure is generally increased at a rate which maintains the temperature within about 20.degree. C. below the glass transition temperature of the thermoset-table resin, so that cure of the resin proceeds in the glassy state. The pressure during the process is generally maintained below about 50 psi and is preferably atmospheric pressure. The process enables the production of thermoset composite articles suitable for high-performance applications without lengthy autoclave treatments.
    • 在相对温和的条件下制备热固性复合材料制品的方法包括将含有部分固化的可热固化树脂和纤维基材的层压板暴露于随时间增加的高温下,升高的温度低于树脂的玻璃化转变温度,但足以 促进进一步固化并将其玻璃化转变温度提高到树脂的最终玻璃化转变温度。 暴露温度通常以保持温度低于热固性树脂的玻璃化转变温度约20℃的速率增加,使得树脂的固化在玻璃状态下进行。 该过程中的压力通常保持在约50psi以下,优选为大气压。 该方法使得能够生产适用于高性能应用的热固性复合制品,而不需要长时间的高压釜处理。