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1. 发明授权

US5684087A Process for producing thermoplastic granulated polymer material from polymer solutions 失效
标题翻译：从聚合物溶液制备热塑性粒状聚合物材料的方法
公开(公告)号：US5684087A
公开(公告)日：1997-11-04
申请号：US719775
申请日：1996-09-25
申请人： Claus Wulff , Gottfried Zaby , Clemens Casper , Klemens Kohlgruber , Thomas Bamberger , Hugo Obermann
发明人： Claus Wulff , Gottfried Zaby , Clemens Casper , Klemens Kohlgruber , Thomas Bamberger , Hugo Obermann
IPC分类号： C08J3/12 , B29B9/00 , B29B9/06 , B29K69/00 , C08G63/89 , C08G64/40 , C08J3/14 , C08G63/48
CPC分类号： C08J3/14 , B29B7/7485 , B29B9/06 , C08G63/89 , C08G64/403
摘要： This invention relates to a process for producing granulated polymer materials from polymer solutions, in which organic solvent of the polymer solution is evaporated in a heat exchanger, optionally with the admixture of steam, or in a holding tube with the admixture of steam, and the paste-like mixture of concentrated solution, solvent vapour and optionally of condensed steam is separated in a separator provided with rotating built-in components for cleaning off the walls. The pre-concentrated polymer solution is further concentrated in the separator by supplying heat by way of heating the separator walls or the rotating built-in components and by the shearing energy of the rotating built-in components.Residual degassing of the solvent is effected before granulation, e.g. in the discharge extruder of the separator which is provided with rotating built-in components, through one or more degassing zones, optionally by the additional admixture of entraining media, such as inert gas or steam, for example.
摘要翻译：本发明涉及一种由聚合物溶液制备粒状聚合物材料的方法，其中聚合物溶液的有机溶剂在热交换器中蒸发，任选地与蒸汽混合，或在具有蒸汽混合物的保持管中蒸发，浓缩溶液，溶剂蒸气和任选的冷凝蒸汽的糊状混合物在具有旋转的内置部件的隔板中分离，用于清洁壁。通过加热隔离壁或旋转的内置部件以及旋转的内置部件的剪切能量，将预浓缩的聚合物溶液进一步浓缩在隔板中。在造粒前进行溶剂的残留脱气，例如在具有旋转内置部件的分离器的排出挤出机中，通过一个或多个脱气区，任选地通过例如惰性气体或蒸汽的夹带介质的附加混合物。

2. 发明授权

US5830977A Process for the isolation of partially crystalline polycarbonate powder 失效
标题翻译：用于分离部分结晶的聚碳酸酯粉末的方法
公开(公告)号：US5830977A
公开(公告)日：1998-11-03
申请号：US778654
申请日：1997-01-03
申请人： Claus Wulff , Gottfried Zaby , Clemens Casper , Klemens Kohlgruber , Hugo Obermann , Steffen Kuhling
发明人： Claus Wulff , Gottfried Zaby , Clemens Casper , Klemens Kohlgruber , Hugo Obermann , Steffen Kuhling
IPC分类号： C08G64/40 , C08J3/14 , C08G64/00
CPC分类号： C08J3/14 , C08G64/403 , C08J2369/00
摘要： The present invention provides a process for the isolation of partially crystalline polycarbonate powder or oligocarbonate powder from solutions thereof, in which process the organic solvent of a polycarbonate solution is vaporized in a heat exchanger, optionally with incorporation of steam, or in a holding tube with incorporation of steam and the pasty mixture of concentrated solution, solvent vapor and optionally water is separated in a separator. In this process, the solvent vapor is condensed in a heat exchanger downstream from the separator. The solvent is vaporized in the heat exchanger by indirect input of heat through the heat exchanger walls and vaporization may be promoted by preheating the polycarbonate or oligocarbonate solution in an upstream heat exchanger or by introducing steam or both.
摘要翻译：本发明提供从其溶液中分离部分结晶的聚碳酸酯粉末或低聚碳酸酯粉末的方法，其中聚碳酸酯溶液的有机溶剂在热交换器中蒸发，任选地加入蒸汽，或在具有在分离器中分离蒸汽和浓缩溶液，溶剂蒸气和任选的水的糊状混合物。在该方法中，溶剂蒸汽在分离器下游的热交换器中冷凝。溶剂在热交换器中通过热交换器壁的间接输入而蒸发，并且通过在上游热交换器中预热聚碳酸酯或低聚碳酸溶液或通过引入蒸汽或两者来促进蒸发。

3. 发明授权

US5786445A Process for drying polymeric powders and polymeric agglomerates 失效
标题翻译：干燥聚合物粉末和聚合物附聚物的方法
公开(公告)号：US5786445A
公开(公告)日：1998-07-28
申请号：US724931
申请日：1996-10-02
申请人： Claus Wulff , Gottfried Zaby , Thomas Bamberger , Klemens Kohlgruber , Hugo Obermann , Stefaan De Vos , Gabriel Denecker , Johan Vaes , Tony Van Osselaer
发明人： Claus Wulff , Gottfried Zaby , Thomas Bamberger , Klemens Kohlgruber , Hugo Obermann , Stefaan De Vos , Gabriel Denecker , Johan Vaes , Tony Van Osselaer
IPC分类号： F26B11/14 , B29B13/02 , B29B13/06 , B29K55/02 , B29K69/00 , F26B5/04 , F26B17/20 , C08F6/00
CPC分类号： B29B13/065 , F26B17/20 , F26B5/041
摘要： The invention relates to a process for drying polymeric powders and polymeric agglomerates, in particular thermoplastic aromatic polycarbonate or other thermoplastic polymers such as, for example, acrylonitrile-butadiene-styrene copolymer, in the melt, whereby thermoplastic polymeric powders or polymeric agglomerates containing water or solvent or both are freed from adhering moisture and contained solvent, accompanied by melting, in an apparatus provided with rotating baffles for cleaning the walls of the apparatus and for distribution and transport of the material being dried, by heat input through the walls or through the rotating baffles or both as well as by heat input as a result of shearing action. The process of drying and that of melting for the subsequent granulation are thereby combined.
摘要翻译：本发明涉及在熔体中干燥聚合物粉末和聚合物附聚物，特别是热塑性芳族聚碳酸酯或其它热塑性聚合物例如丙烯腈 - 丁二烯 - 苯乙烯共聚物的方法，由此将含有水或聚合物的热塑性聚合物粉末或聚合物附聚物溶剂或两者在具有用于清洁设备的壁的旋转挡板的设备中并且随着熔化而被包含溶剂并且包含溶剂，并且通过壁的热输入或通过壁的热输入以及用于分配和输送待干燥的材料旋转挡板或两者以及作为剪切作用的结果的热输入。由此组合干燥过程和熔化后续制粒。

4. 发明授权

US5852157A Process for the production of polycarbonate agglomerate 失效
标题翻译：生产聚碳酸酯聚集体的方法
公开(公告)号：US5852157A
公开(公告)日：1998-12-22
申请号：US810263
申请日：1997-03-03
申请人： Gottfried Zaby , Clemens Casper , Klemens Kohlgruber , Hugo Obermann
发明人： Gottfried Zaby , Clemens Casper , Klemens Kohlgruber , Hugo Obermann
IPC分类号： C08J3/14 , B01J2/02 , C08G64/40 , C08G64/00
CPC分类号： B01J2/02
摘要： This invention relates to a process for the production of polycarbonate agglomerate of high bulk density from polycarbonate solutions, in which the organic solvent is stripped from a solution of polycarbonate by means of steam, and which is characterised in that the resulting suspension of polycarbonate particles, condensed water and water- and solvent vapor is fed in a tube or tubular heat exchanger to a separator which is partially filled with water and which is under elevated pressure. The polycarbonate agglomerates are discharged, together with part of the water, via a pressure lock at the bottom of the separator.
摘要翻译：本发明涉及由聚碳酸酯溶液制备高堆积密度的聚碳酸酯聚集体的方法，其中有机溶剂通过蒸汽从聚碳酸酯溶液中剥离，其特征在于所得的聚碳酸酯颗粒悬浮液，冷凝水和水和溶剂蒸汽在管或管式热交换器中进料到部分被水填充并且处于升高压力下的分离器中。聚碳酸酯附聚物与部分水一起通过分离器底部的压力锁定排出。

5. 发明授权

US5767224A Two-step process for the production of thermoplastic polycarbonate 失效
标题翻译：生产热塑性聚碳酸酯的两步法
公开(公告)号：US5767224A
公开(公告)日：1998-06-16
申请号：US823792
申请日：1997-03-24
申请人： Steffen Kuhling , Klaus Schebesta , Uwe Hucks , Martin Ullrich , Heinrich Schuchardt , Rolf Bachmann , Thomas Fischer , Klemens Kohlgruber , Franz Ferdinand Rhiel , Gottfried Zaby
发明人： Steffen Kuhling , Klaus Schebesta , Uwe Hucks , Martin Ullrich , Heinrich Schuchardt , Rolf Bachmann , Thomas Fischer , Klemens Kohlgruber , Franz Ferdinand Rhiel , Gottfried Zaby
IPC分类号： C08G64/30 , C08G64/00
CPC分类号： C08G64/307
摘要： The invention relates to a two-step melt process for the production of thermoplastic, solvent-free, low-branching polycarbonates with low --OH terminal group content using a self-cleaning high-viscosity reactor.
摘要翻译：本发明涉及使用自清洁高粘度反应器生产具有低-OH端基含量的热塑性，无溶剂，低支化聚碳酸酯的两步熔融方法。

6. 发明授权

US5726228A Use of carbonates as demoulding agents for thermoplastic polycarbonates 失效
标题翻译：使用碳酸酯作为热塑性聚碳酸酯的脱模剂
公开(公告)号：US5726228A
公开(公告)日：1998-03-10
申请号：US759951
申请日：1996-12-03
申请人： Ralf Kaufmann , Wolfgang Ebert , Hartmut Lower , Jurgen Kadelka , Claus Wulff , Gottfried Zaby
发明人： Ralf Kaufmann , Wolfgang Ebert , Hartmut Lower , Jurgen Kadelka , Claus Wulff , Gottfried Zaby
IPC分类号： C08K5/15 , C08K5/00 , C08K5/156 , C08L69/00 , G11B7/2534 , C08K5/10
CPC分类号： G11B7/2534 , C08K5/156
摘要： The present invention relates to the use of cyclic carbonates as demoulding agents for thermoplastic polycarbonates, and to the incorporation of these cyclic carbonates into the thermoplastic polycarbonates.
摘要翻译：本发明涉及使用环状碳酸酯作为热塑性聚碳酸酯的脱模剂，以及将这些环状碳酸酯引入到热塑性聚碳酸酯中。

7. 发明授权

US5921089A Method for the transport and storage of phenol 失效
标题翻译：苯酚运输和储存方法
公开(公告)号：US5921089A
公开(公告)日：1999-07-13
申请号：US942613
申请日：1997-10-02
申请人： Werner Kleinloh , Otto Schnurr , Tony Van Osselaer , Claus Wulff , Gottfried Zaby
发明人： Werner Kleinloh , Otto Schnurr , Tony Van Osselaer , Claus Wulff , Gottfried Zaby
IPC分类号： C07C37/88 , C07C39/04 , C07C39/16 , F17C11/00
CPC分类号： C07C37/88
摘要： The transportation and storage of phenol is enhanced by additions of up to 70% by weight of acetone to liquid phenol.
摘要翻译：通过向液体苯中加入高达70重量％的丙酮来增强苯的输送和储存。

8. 发明授权

US5652313A Two-stage process for the manufacture of thermoplastic polycarbonate 失效
标题翻译：用于制造热塑性聚碳酸酯的两阶段工艺
公开(公告)号：US5652313A
公开(公告)日：1997-07-29
申请号：US594688
申请日：1996-01-31
申请人： Steffen Kuhling , Uwe Hucks , Gottfried Zaby , Claus Wulff
发明人： Steffen Kuhling , Uwe Hucks , Gottfried Zaby , Claus Wulff
IPC分类号： C08F2/00 , C08G64/20 , C08G64/30
CPC分类号： C08G64/307
摘要： The present invention provides a two-stage melt process for the manufacture of thermoplastic, solvent-free, low-branched polycarbonates with low OH end-group contents with the use of ammonium or phophonium catalysts in the first stage and alkali and alkaline earth catalysts in the second stage.
摘要翻译：本发明提供了一种两阶段熔融法，用于制造具有低OH末端含量的热塑性无溶剂的低支化聚碳酸酯，在第一阶段使用铵或磷鎓催化剂，碱和碱土金属催化剂在第二阶段

9. 发明授权

US4380593A Intumescent compositions 失效
标题翻译：膨胀成分
公开(公告)号：US4380593A
公开(公告)日：1983-04-19
申请号：US351687
申请日：1982-02-24
申请人： Wulf von Bonin , Gottfried Zaby
发明人： Wulf von Bonin , Gottfried Zaby
IPC分类号： C08G18/00 , C08G18/38 , C08G18/50 , C09D5/18 , C09K21/14 , C08G18/14
CPC分类号： C09D5/185 , C08G18/3838 , C08G18/3851 , C08G18/3889 , C08G18/509 , C09K21/14
摘要： Optionally-foamed intumescent compositions obtained by reacting(a) polyisocyanates with(b) phosphorus-containing condensation products having at least 2 hydroxyl groups and obtained by condensing primary or secondary monoamines and/or polyamines optionally containing OH-groups, carbonyl compounds and dialkyl phosphites, optionally followed by alkoxylation, and(c) more than bifunctional polyethers having an average OH-number of from 150 to 500 which have been obtained by the addition of alkylene oxides, of which from 50 to 100% by weight consist of ethylene oxide, with low molecular weight starters, and(d) cyanuric acid and/or cyanuric acid derivatives, and(e) optionally water and(f) optionally other organic compounds containing isocyanate-reactive hydrogen atoms,are used, for example, as cavity-filling, gap-sealing or coating materials.
摘要翻译：通过使（a）多异氰酸酯与（b）具有至少2个羟基的含磷缩合产物并通过使任选含有OH基，羰基化合物和亚磷酸二烷基酯的伯或仲单胺和/或多胺缩合获得的任选发泡膨胀组合物，任选地随后进行烷氧基化，和（c）通过加入环氧烷烃获得的具有150-500的平均OH-数的双官能团聚醚，其中50-100重量％由环氧乙烷组成，（d）氰尿酸和/或氰尿酸衍生物，和（e）任选的水和（f）任选地含有异氰酸酯反应性氢原子的其它有机化合物，例如作为空腔填充物，间隙密封或涂层材料。

10. 发明授权

US5831111A Process for the continuous production of aryl carbonates 失效
标题翻译：连续生产碳酸芳基酯的方法
公开(公告)号：US5831111A
公开(公告)日：1998-11-03
申请号：US850474
申请日：1997-05-05
申请人： Pieter Ooms , Eric Bischof , Hans-Josef Buysch , Steffen Kuhling , Gottfried Zaby , Wolfgang Jakob , Jurgen Dahmer , Norbert Schon
发明人： Pieter Ooms , Eric Bischof , Hans-Josef Buysch , Steffen Kuhling , Gottfried Zaby , Wolfgang Jakob , Jurgen Dahmer , Norbert Schon
IPC分类号： B01J21/04 , C07B61/00 , C07C68/02 , C07C69/96
CPC分类号： C07C68/02
摘要： The present invention relates to a process for the continuous production of carbonates having aromatic ester groups by reacting aromatic hydroxy compounds with phosgene in the gas phase in the presence of heterogeneous catalysts.
摘要翻译：本发明涉及一种在非均相催化剂存在下，通过气相中芳族羟基化合物与光气反应连续生产具有芳族酯基的碳酸酯的方法。

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