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1. 发明授权

US5141970A Method of forming high-temperature resistant polymers 失效
标题翻译：形成高温耐热聚合物的方法
公开(公告)号：US5141970A
公开(公告)日：1992-08-25
申请号：US625574
申请日：1990-12-10
申请人： Ciaran B. McArdle , Joseph Burke , John G. Woods , Edward K. Welch, II
发明人： Ciaran B. McArdle , Joseph Burke , John G. Woods , Edward K. Welch, II
IPC分类号： C08F10/14 , C08F2/46 , C08F2/48 , C08F12/00 , C08F12/24 , C08F12/34 , C08F16/12 , C08F16/22 , C08F16/32 , C08F212/00 , C08F290/00 , C08F290/06 , C08F299/02 , C08J3/24 , C08L31/02 , C08L57/00
CPC分类号： C08F16/32 , C08F12/24 , C08F12/34 , C08F16/22
摘要： A method of forming high-temperature resistant polymers by a 2 step curing process comprising(a) curing a polymerizable composition at least one aromatic compound having alpha and/or beta instruction which is not substantially reactive under the curing condition of step a, particularly allyl or properyl, and(b) heating the cured composition of step a in the presence of acid to form a crosslinked resin.

2. 发明授权

US5084490A Styryloxy compounds and polymers thereof 失效
标题翻译：苯乙烯基化合物及其聚合物
公开(公告)号：US5084490A
公开(公告)日：1992-01-28
申请号：US625725
申请日：1990-12-10
申请人： Ciaran B. McArdle , Joseph Burke , John G. Woods
发明人： Ciaran B. McArdle , Joseph Burke , John G. Woods
IPC分类号： C08F2/50 , C07C43/215 , C08F2/46 , C08F2/48 , C08F12/34 , C08F16/32 , C08F290/00 , C08F299/02
CPC分类号： C07C43/215 , C08F12/34
摘要： Styryloxy compounds of the formula IV ##STR1## wherein R.sup.1 and R.sup.2 are H, or one of R.sup.1 and R.sup.2 is H and the other is methyl;R.sup.7 and R.sup.8 (which may be the same or different) are H, C.sub.1 -C.sub.5 alkyl or C.sub.1 -C.sub.5 alkenyl; or one of R.sup.7 and R.sup.8 may be --OR.sup.6 or C.sub.1 -C.sub.5 alkoxy or C.sub.1 -C.sub.5 alkenyloxy if R.sup.2 is not methyl;R.sup.6 is selected from the group consisting of: ##STR2## where R.sup.10 is C.sub.1 -C.sub.5 alkyl; and R.sup.11, R.sup.12 and R.sup.13, which may be the same or different, are H or C.sub.1 -C.sub.5 alkyl, are described as new low viscosity liquid styryloxy monomers which can be photocured and which form transparent polymers. They have an advantageous effect in a mixture with 4-allyloxystyrene, and this mixture has a synergistic effect in combination with divinyl ethers of a polyalkylene oxide.

3. 发明授权

US5200238A Liquid crystal display devices and method of manufacture 失效
标题翻译：液晶显示装置及制造方法
公开(公告)号：US5200238A
公开(公告)日：1993-04-06
申请号：US766492
申请日：1991-09-25
申请人： Ciaran B. McArdle , John G. Woods , Anthony F. Jacobine
发明人： Ciaran B. McArdle , John G. Woods , Anthony F. Jacobine
IPC分类号： G02F1/1337 , G02F1/139
CPC分类号： G02F1/133711 , G02F1/1397 , G02F2001/133746 , Y10T428/1005 , Y10T428/1014 , Y10T428/31663
摘要： A method of forming liquid crystal alignment layers of high tilt angle, said method comprising preparing a polymeric film of a monomer of the formula IV: ##STR1## wherein X and Y are strong electron withdrawing groups, optionally substituted with or containing Si or Ti, and A is --H or --CH.dbd.CH.sub.2 or, provided that X and Y are both --CN, A may be --R.sup.2 or --CH.dbd.CHR.sup.2 wherein R.sup.2 is hydrocarbyl, aryl or alkaryl; exposing said polymeric film to ultraviolet radiation for sufficient period of time to photochemically modify the polymer and, thereafter, subjecting the modified polymer to a heat treatment in the range of 100.degree.-400.degree. C. for at least 5 seconds.
摘要翻译：一种形成高倾斜角的液晶取向层的方法，所述方法包括制备式IV单体的聚合物膜：其中X和Y是强吸电子基团，任选被Si或Ti取代并且A是-H或-CH = CH 2，或者X和Y都是-CN，A可以是-R2或-CH = CHR2，其中R2是烃基，芳基或烷芳基; 将所述聚合物膜暴露于紫外线辐射足够的时间以光聚合改性聚合物，然后将改性聚合物在100-400℃范围内进行热处理至少5秒。

4. 发明授权

US06231714B1 Allylic phenyl ether (meth)acrylate compositions and novel allylic phenyl ether (meth)acrylate monomers 失效
标题翻译：烯丙基苯基醚（甲基）丙烯酸酯组合物和新型烯丙基苯基醚（甲基）丙烯酸酯单体
公开(公告)号：US06231714B1
公开(公告)日：2001-05-15
申请号：US09198536
申请日：1998-11-24
申请人： John G. Woods , Susanne Morrill , Ciaran B. McArdle
发明人： John G. Woods , Susanne Morrill , Ciaran B. McArdle
IPC分类号： B32B3100
CPC分类号： C08F290/062 , C07C69/54 , C08F16/26 , C08F20/30 , C08F22/105
摘要： Curable compositions include at least one monomer compound having both (meth)acrylic ester functionality and an allylic phenyl ether functional group on the same molecule, the allylic phenyl ether functional group having at least one unsubstituted position on the phenyl ring which is ortho or para to the allylic ether group, and a free radical catalyst system. The composition may also includes a latent thermally activated acid generator. Claisen Rearrangement of radically polymerized polymers produced from the compositions may be induced at temperatures of about 100° C. or more to give crosslinked products of improved thermal resistance. Novel monomers which may be used in such compositions are characterized by formulas I and II: where R1 is H or methyl; R2 is a direct bond, a group of the formula —NCnH2n-, or a group of the formula —(OCnH2n—)m— which when taken with the phenyl group to which it is attached forms a phenyl ether; n is 1-4 and m is 1-10; R3 is —CH2CH═CH2, —CH2C(CH3)═CH2, —CH2CH═CH(CH3), —CH2C(CH3)═CH(CH3), —CH2CH═C(CH3)2 or —CH2 CH═CH(C6H5); and R4 is a divalent allylic group, and wherein the compound is optionally substituted on a phenyl group thereof by an alkyl, alkoxy or halo group, provided that relative to the respective —OR3 or —OR4O — groups, at least one unsubstituted ortho or para position remains on an adjacent phenyl ring.
摘要翻译：可固化组合物包括在同一分子上具有（甲基）丙烯酸酯官能团和烯丙基苯基醚官能团的至少一种单体化合物，所述烯丙基苯基醚官能团在苯环上具有至少一个未取代的位置，烯丙基醚基团和自由基催化剂体系。组合物还可以包括潜热热活化酸产生剂。 Claisen从组合物制备的自由基聚合聚合物的重排可以在约100℃或更高的温度下诱导，得到具有改善的耐热性的交联产物。可用于这些组合物中的新单体由式I和II表征：其中R 1是H或甲基; R2是直接键，式-NC n H 2n - 或式 - （OC n H 2n - ）m - 的基团，当与其连接的苯基取代时形成苯基醚; n为1-4，m为1-10; R3是-CH2CH = CH2，-CH2C（CH3）= CH2，-CH2CH = CH（CH3），-CH2C（CH3）= CH（CH3），-CH2CH = C（CH3）2或-CH2CH = CH（C6H5 ）; 并且R 4是二价烯丙基，并且其中所述化合物任选地在其苯基上被烷基，烷氧基或卤素取代，条件是相对于相应的-OR 3或-OR 4 O-基团，至少一个未取代的邻位或对位的位置保留在相邻的苯环上。

5. 发明申请

US20110060157A1 APPARATUS AND METHODS FOR CONTROLLED RADICAL POLYMERIZATION 有权
标题翻译：控制辐射聚合的装置和方法
公开(公告)号：US20110060157A1
公开(公告)日：2011-03-10
申请号：US12946895
申请日：2010-11-16
申请人： David M. Glaser , Roderick Coffey , John G. Woods , Anthony F. Jacobine
发明人： David M. Glaser , Roderick Coffey , John G. Woods , Anthony F. Jacobine
IPC分类号： C07C67/347
CPC分类号： C08F220/18 , B01J14/005 , B01J16/005 , B01J19/0066 , B01J19/1881 , B01J2219/00063 , B01J2219/00069 , B01J2219/00094 , B01J2219/00162 , B01J2219/002 , B01J2219/00213 , B01J2219/00231 , B01J2219/00238 , C08F2/00 , C08F293/005 , C08F2438/01
摘要： A method of conducting controlled radical polymerization, including: (a) providing a mixture of at least one monomer; at least one monomer solvent; at least one compound metal coordinating capable; and at least one initiator; (b) directing the mixture at a rate over a solid catalyst surface contained in an external chamber to the vessel, the catalyst including a metal or metal compound capable of at least two oxidation states; (c) monitoring the reaction vessel temperature; (d) adjusting the flow rate when the temperature is outside a selected temperature range; and (e) allowing the polymerization to proceed to desired conversion level.
摘要翻译：一种进行受控自由基聚合的方法，包括：（a）提供至少一种单体的混合物; 至少一种单体溶剂; 至少一种配位的复合金属; 和至少一个引发剂; （b）以混合物的速率将包含在外部室中的固体催化剂表面的速率引导至容器，所述催化剂包括能够具有至少两种氧化态的金属或金属化合物; （c）监测反应容器的温度; （d）当温度在选定的温度范围之外时调节流量; 和（e）允许聚合进行到所需的转化水平。

6. 发明授权

US07728092B1 Anaerobically curable compositions 有权
标题翻译：厌氧可固化组合物
公开(公告)号：US07728092B1
公开(公告)日：2010-06-01
申请号：US11279661
申请日：2006-04-13
申请人： Anthony F. Jacobine , Joel D. Schall , John G. Woods
发明人： Anthony F. Jacobine , Joel D. Schall , John G. Woods
IPC分类号： C08F20/06
CPC分类号： C09J4/00 , C08F220/06 , C08F222/06 , C08F222/1006 , C08F222/40 , C08K5/098
摘要： The present invention relates to anaerobically curable compositions based on (meth)acrylate-functionalized poly(acrylate) polymers.
摘要翻译：本发明涉及基于（甲基）丙烯酸酯官能化的聚（丙烯酸酯）聚合物的厌氧可固化组合物。

7. 发明授权

US07671114B2 Adhesive of substituted oxirane or oxetane compound with silver-based, lead-free solder 有权
标题翻译：取代环氧乙烷或氧杂环丁烷化合物与银基，无铅焊料的粘合剂
公开(公告)号：US07671114B2
公开(公告)日：2010-03-02
申请号：US12176729
申请日：2008-07-21
申请人： John G. Woods , Yuhshi Lu , Bruce C. B. Chan , Philip T. Klemarczyk , Andrew D. Messana
发明人： John G. Woods , Yuhshi Lu , Bruce C. B. Chan , Philip T. Klemarczyk , Andrew D. Messana
IPC分类号： C08K3/08 , C08L63/00 , C08L71/00
CPC分类号： H01L21/563 , C08G59/1455 , C08G59/1494 , C08K5/5435 , C09J163/00 , H01L23/293 , H01L2224/73203 , H01L2924/01004 , H01L2924/01077 , H01L2924/01079
摘要： In accordance with the present invention, it has now been found that glycidyl epoxy resins containing substitution on the epoxide ring can be used with conventional epoxy curing agents and fluxing agents to produce underfill adhesives that are suitable for use with silver-based alloys. Owing to the structural similarity of the new materials to conventional epoxy resins, physical and material properties of the invention formulations are altered little, if at all, relative to products currently in use, and so are highly compatible with existing processes.
摘要翻译：根据本发明，已经发现在环氧化物环上含有取代基的缩水甘油基环氧树脂可以与常规的环氧固化剂和助熔剂一起使用，以生产适用于银基合金的底部填充粘合剂。由于新材料与常规环氧树脂的结构相似性，本发明制剂的物理和材料性能相对于目前使用的产品而言几乎没有改变，因此与现有方法高度兼容。

8. 发明申请

US20090018239A1 UNDERFILL ADHESIVES 有权
标题翻译：不良胶粘剂
公开(公告)号：US20090018239A1
公开(公告)日：2009-01-15
申请号：US12176729
申请日：2008-07-21
申请人： John G. Woods , Yuhshi Luh , Bruce C.B. Chan , Philip T. Klemarczyk , Andrew D. Messana
发明人： John G. Woods , Yuhshi Luh , Bruce C.B. Chan , Philip T. Klemarczyk , Andrew D. Messana
IPC分类号： C08K5/00
CPC分类号： H01L21/563 , C08G59/1455 , C08G59/1494 , C08K5/5435 , C09J163/00 , H01L23/293 , H01L2224/73203 , H01L2924/01004 , H01L2924/01077 , H01L2924/01079
摘要： In accordance with the present invention, it has now been found that glycidyl epoxy resins containing substitution on the epoxide ring can be used with conventional epoxy curing agents and fluxing agents to produce underfill adhesives that are suitable for use with silver-based alloys. Owing to the structural similarity of the new materials to conventional epoxy resins, physical and material properties of the invention formulations are altered little, if at all, relative to products currently in use, and so are highly compatible with existing processes.
摘要翻译：根据本发明，已经发现在环氧化物环上含有取代基的缩水甘油基环氧树脂可以与常规的环氧固化剂和助熔剂一起使用，以生产适用于银基合金的底部填充粘合剂。由于新材料与常规环氧树脂的结构相似性，本发明制剂的物理和材料性能相对于目前使用的产品而言几乎没有改变，因此与现有方法高度兼容。

9. 发明申请

US20090000732A1 Bonded Fuel Cell Assembly, Methods, Systems and Sealant Compositions for Producing the Same 审中-公开
标题翻译：用于生产燃料电池组合件，方法，系统和密封剂组合物
公开(公告)号：US20090000732A1
公开(公告)日：2009-01-01
申请号：US12161173
申请日：2007-01-17
申请人： Anthony F. Jacobine , John G. Woods , Steven Thomas Nakos , Matthew Peter Burdzy , Brian Russel Einsla , Kevin James Welch
发明人： Anthony F. Jacobine , John G. Woods , Steven Thomas Nakos , Matthew Peter Burdzy , Brian Russel Einsla , Kevin James Welch
IPC分类号： B32B37/06 , B32B37/12 , B32B38/18 , B29C35/08 , B29C65/14
CPC分类号： H01M8/0284 , H01M8/0267 , H01M8/0271 , H01M8/0286 , H01M8/241 , H01M8/242 , H01M8/2457 , H01M2008/1095 , Y10T156/1798
摘要： A fuel cell, having improved sealing against leakage, includes a sealant disposed over the peripheral portions a membrane electrode assembly such that the cured sealant penetrates a gas diffusion layer of the membrane electrode assembly. The sealant is applied through liquid injection molding techniques to form cured sealant composition at the peripheral portions of the membrane electrode assembly. The sealant may be thermally cured at low temperatures, for example 130° C. or less, or may be cured at room temperature through the application of actinic radiation. The sealant may be a one-part or a two-part sealant. The sealant includes a polymerizable material, such as a polymerizable monomer, oligomer, telechelic polymer, functional polymer and combinations thereof functionalized with a group selected from epoxy, allyl, vinyl, (meth)acrylate, imide, amide, urethane and combinations thereof. Useful fuel cell components to be bonded include a cathode flow field plate, an anode flow field plate, a resin frame, a gas diffusion layer, an anode catalyst layer, a cathode catalyst layer, a membrane electrolyte, a membrane-electrode-assembly frame, and combinations thereof.
摘要翻译：具有改善的泄漏密封性的燃料电池包括设置在周边部分上的膜电极组件的密封剂，使得固化的密封剂渗透膜电极组件的气体扩散层。通过液体注射成型技术施加密封剂，以在膜电极组件的周边部分形成固化的密封剂组合物。密封剂可以在低温例如130℃或更低温度下热固化，或者可以通过施加光化辐射在室温下固化。密封剂可以是一部分或两部分密封剂。密封剂包括聚合性材料，例如可聚合单体，低聚物，遥爪聚合物，官能聚合物及其与选自环氧基，烯丙基，乙烯基，（甲基）丙烯酸酯，酰亚胺，酰胺，氨基甲酸酯及其组合的基团官能化的组合。有待燃料电池组件包括阴极流场板，阳极流场板，树脂框架，气体扩散层，阳极催化剂层，阴极催化剂层，膜电解质，膜 - 电极 - 组件框架，及其组合。

10. 发明授权

US07193016B1 Epoxy-extended polyacrylate toughening agent 失效
标题翻译：环氧延伸聚丙烯酸酯增韧剂
公开(公告)号：US07193016B1
公开(公告)日：2007-03-20
申请号：US10692935
申请日：2003-10-27
申请人： John G. Woods , Mark M. Konarski , Kyra M. Kozak , Yuhshi Luh
发明人： John G. Woods , Mark M. Konarski , Kyra M. Kozak , Yuhshi Luh
IPC分类号： C08F8/08 , C08L63/00 , C08L63/02
CPC分类号： C09J163/00 , C08F8/14 , C08F2810/40 , C08F20/16
摘要： In accordance with the present invention, there are provided toughening agents which are useful for improving the performance properties of epoxy-based adhesive formulations. For example, epoxidized polybutylacrylates have been found to be useful toughening agents of component level underfill adhesive compositions. Invention materials are generally liquid rubbers which provided improved fracture toughness while maintaining satisfactory capillary flow properties. Invention materials can be synthesized in neat (solventless) reactions from readily available low-cost raw materials and isolated in high yields. They have a branched telechelic structure with terminal epoxide functional groups. The polyacrylate is typically obtained as a mixture of epoxidized polymer, chain extended polyoligomer and unreacted monomer. Invention materials are compatible with common epoxy formulations and may be used without purification. At low levels of incorporation, they provide adhesives that meet the minimum fracture toughness (Gq>2.0 lb/in) and capillary flow specifications (flow time
摘要翻译：根据本发明，提供了可用于改善环氧基粘合剂制剂的性能的增韧剂。例如，已经发现环氧化的聚丁基丙烯酸酯是组分级底部填充粘合剂组合物的有用的增韧剂。发明材料通常是液体橡胶，其提供改善的断裂韧性同时保持令人满意的毛细管流动性能本发明材料可以从易于获得的低成本原料的纯（无溶剂）反应中合成并以高收率分离。它们具有末端环氧官能团的分子遥爪结构。聚丙烯酸酯通常以环氧化聚合物，链延长多元寡聚物和未反应单体的混合物形式获得。本发明材料与普通的环氧配方相容，可以不经纯化地使用。在低掺量下，它们提供了许多商业底层填充应用的粘合剂，其满足最小断裂韧性（Gq> 2.0lb / in）和毛细管流动规格（流动时间<180秒）。根据本发明的另一个实施方案，提供了包含本发明化合物的粘合剂组合物及其使用方法。在本发明的另外的实施方案中，提供了制备本发明增韧剂的方法，用于将装置粘附到基底上的方法以及包括附着到第二制品上的第一制品的组件。

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