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1. 发明授权

US4233246A Manufacture of aliphatic hydroxycarbonyl compounds etherified with aliphatic groups 失效
标题翻译：用脂族基团醚化的脂族羟基羰基化合物的制备
公开(公告)号：US4233246A
公开(公告)日：1980-11-11
申请号：US971416
申请日：1978-12-20
申请人： Christian Dudeck , Gunter Lehmann , Norbert Petri , Hans Diem , Werner Fliege , Bernd Meissner , Karl-Heinz Ross , Wolfgang Muehlthaler
发明人： Christian Dudeck , Gunter Lehmann , Norbert Petri , Hans Diem , Werner Fliege , Bernd Meissner , Karl-Heinz Ross , Wolfgang Muehlthaler
IPC分类号： C07C47/198 , B01J23/00 , B01J23/50 , B01J23/72 , B01J27/14 , B01J35/02 , B01J37/02 , C07C45/00 , C07C45/29 , C07C45/37 , C07C45/38 , C07C45/39 , C07C49/175 , C07C67/00
CPC分类号： B01J23/50 , B01J23/72 , B01J27/14 , B01J35/02 , B01J37/0228 , C07C45/38 , C07C45/39
摘要： Aliphatic hydroxycarbonyl compounds etherified with aliphatic groups are prepared by oxidizing hydroxyalcohols in the presence of a metal catalyst which consists of one or more layers, each of a particular weight and each containing particles of a particular size, the catalyst bed also having a particular total thickness, and the catalyst components used being silver and copper, with or without added copper/tin/phosphorus or silver alone. The etherified hydroxyaldehydes and hydroxyketones obtainable by the process of the invention are valuable starting materials for the preparation of dyes, pesticides, plastics and scents.
摘要翻译：用脂族基团醚化的脂族羟基羰基化合物通过在金属催化剂存在下氧化羟基醇制备，金属催化剂由一层或多层组成，每层具有特定重量，每层含有特定尺寸的颗粒，催化剂床也具有特定的总厚度，所用的催化剂组分是银和铜，单独加入或不加入铜/锡/磷或银。通过本发明方法获得的醚化羟基醛和羟基酮是用于制备染料，农药，塑料和香料的有价值的原料。

2. 发明授权

US4229590A Preparation of alkyl pyruvates 失效
标题翻译：丙酮酸烷基酯的制备
公开(公告)号：US4229590A
公开(公告)日：1980-10-21
申请号：US10725
申请日：1979-02-08
申请人： Christian Dudeck , Gunter Lehmann , Bernd Meissner , Hans Diem , Werner Fliege , Norbert Petri , Karl-Heinz Ross
发明人： Christian Dudeck , Gunter Lehmann , Bernd Meissner , Hans Diem , Werner Fliege , Norbert Petri , Karl-Heinz Ross
IPC分类号： B01J23/00 , C07B61/00 , C07C69/716 , C07C67/30 , C07C67/42 , C07C69/67
CPC分类号： C07C69/716
摘要： Alkyl pyruvates are prepared by oxidizing alkyl lactates in the presence of a silver catalyst of a defined particle size, at from 450.degree. to 700.degree. C. The products are starting materials for the preparation of drugs, synthetic resins and plastics.
摘要翻译：丙烯酸烷基酯是通过在450-700℃下在规定粒度的银催化剂存在下，将乳酸烷基酯氧化来制备的。产物是用于制备药物，合成树脂和塑料的原料。

3. 发明授权

US4235823A Preparation of diketones 失效
标题翻译：二酮的制备
公开(公告)号：US4235823A
公开(公告)日：1980-11-25
申请号：US52103
申请日：1979-06-26
申请人： Christian Dudeck , Gunter Lehmann , Karl-Heinz Ross , Werner Fliege , Norbert Petri , Hans Diem , Bernd Meissner , Wolfgang Sauer
发明人： Christian Dudeck , Gunter Lehmann , Karl-Heinz Ross , Werner Fliege , Norbert Petri , Hans Diem , Bernd Meissner , Wolfgang Sauer
IPC分类号： C07C47/02 , B01J23/00 , B01J23/50 , B01J23/72 , C07B61/00 , C07C45/00 , C07C45/38 , C07C45/39 , C07C47/12 , C07C47/20 , C07C49/04 , C07C49/12 , C07C49/20 , C07C67/00
CPC分类号： C07C45/39 , C07C45/38
摘要： Diketones are prepared by oxidizing glycols in the presence of a silver catalyst and/or copper catalyst of a specific particle size, under specific temperature conditions and with a specific composition of the catalyst. The end products are starting materials for the preparation of dyes, drugs, plastics, scents, wrinkle-resist finishes and assistants for increasing the tear strength and resilience of fibrous materials, hardeners for use in the photographic industry, textile assistants for preventing shrinkage after washing, and paper assistants.
摘要翻译：在特定的温度条件下和特定的催化剂组成下，在特定粒径的银催化剂和/或铜催化剂存在下，氧化二醇制备二酮。最终产品是用于制备染料，药物，塑料，香料，抗皱整理剂和用于增加纤维材料的撕裂强度和弹性的助剂的原料，用于照相工业的硬化剂，用于防止洗涤后收缩的纺织助剂和纸张助理。

4. 发明授权

US4242282A Preparation of glyoxal 失效
标题翻译：乙二醛的制备
公开(公告)号：US4242282A
公开(公告)日：1980-12-30
申请号：US2331
申请日：1979-01-10
申请人： Hans Diem , Christian Dudeck , Gunter Lehmann , Guenther Matthias , Norbert Petri
发明人： Hans Diem , Christian Dudeck , Gunter Lehmann , Guenther Matthias , Norbert Petri
IPC分类号： C07C47/127 , B01J23/00 , C07C45/00 , C07C45/38 , C07C67/00 , C07C45/29
CPC分类号： C07C45/38
摘要： Glyoxal is prepared by oxidizing glycol in the presence of a silver catalyst of a defined particle size and under defined conditions of temperature, residence time and inert gas concentration.The glyoxal obtainable by the process of the invention may be used in wrinkle-resist finishing, as an assistant for increasing the tensile strength and resilience of fibrous materials, a tanning agent, a hardener in the photographic industry, and a starting material for the manufacture of synthetic resins, textile auxiliaries, for example to prevent shrinkage after washing, paper additives, for example for increasing the wet strength, and plastics.
摘要翻译：乙二醛通过在具有规定粒度的银催化剂存在下和在限定的温度，停留时间和惰性气体浓度条件下氧化二醇来制备。通过本发明的方法可获得的乙二醛可用于抗皱整理中，作为用于提高纤维材料，鞣制剂，照相工业中的硬化剂的拉伸强度和回弹性的助剂以及用于制造的原料的合成树脂，纺织助剂，例如用于防止洗涤后的收缩，纸添加剂，例如用于增加湿强度，以及塑料。

5. 发明授权

US4224254A Preparation of aromatic and araliphatic aldehydes 失效
标题翻译：芳烃和芳脂醛的制备
公开(公告)号：US4224254A
公开(公告)日：1980-09-23
申请号：US24830
申请日：1979-03-28
申请人： Wolfgang Sauer , Werner Fliege , Christian Dudeck , Norbert Petri
发明人： Wolfgang Sauer , Werner Fliege , Christian Dudeck , Norbert Petri
IPC分类号： B01J23/00 , B01J35/00 , C07C45/00 , C07C45/38 , C07C47/20 , C07C47/52 , C07C67/00 , C07C213/00 , C07C223/00 , C07C45/16
CPC分类号： C07C45/38 , B01J35/00
摘要： Aromatic and araliphatic aldehydes are prepared by oxidizing corresponding alcohols with oxygen in the presence of a silver catalyst of a defined particle size, and under defined temperature conditions. The products are starting materials for the preparation of dyes, pesticides, plastics and scents.
摘要翻译：芳族和芳脂族醛通过在具有规定粒径的银催化剂存在下和在规定的温度条件下用氧氧化相应的醇来制备。该产品是用于制备染料，农药，塑料和香料的起始原料。

6. 发明授权

US4584412A Preparation of formaldehyde 失效
公开(公告)号：US4584412A
公开(公告)日：1986-04-22
申请号：US693864
申请日：1985-01-23
申请人： Albrecht Aicher , Gunter Lehmann , Norbert Petri , Walter Pitteroff , Gunter Reuss , Hans Schreiber , Robert Sebastian
发明人： Albrecht Aicher , Gunter Lehmann , Norbert Petri , Walter Pitteroff , Gunter Reuss , Hans Schreiber , Robert Sebastian
IPC分类号： B01J23/00 , B01J23/50 , C07B61/00 , C07C45/00 , C07C45/38 , C07C45/78 , C07C45/80 , C07C45/81 , C07C47/055 , C07C67/00 , C07C45/29
CPC分类号： C07C45/80 , C07C45/38 , C07C45/78 , C07C45/81
摘要： Formaldehyde is prepared by (a) passing a mixture of methanol and water with a concentration of between 50 and 90% by weight, based on the total weight of the two substances, of methanol into a packed column which possesses a packing having a total layer thickness of not less than 50 cm and a total surface area of not less than 0.5 cm.sup.2 per cm.sup.3 of packing, a liquid circulation of from 15 to 90 g/min per g/min of methanol fed to the column, and a concentration of from 10 to 45% by weight of methanol in the recycle liquid, the temperature at the point of entry of the recycle liquid in the column being from 50.degree. to 86.degree. C. and the bottom temperature being 10.degree.-25.degree. C. lower than this, i.e. from 40.degree. to 70.degree. C., (b) separating off methanol and water from the column by stripping with air, an inert gas and/or exit gas, the throughput being from 0.5 to 3 tonnes of methanol and water per hour per m.sup.2 of column cross-section, (c) converting the gaseous mixture of methanol, water, air, inert gas and/or exit gas at a space velocity of from 0.5 to 3 tonnes of methanol per m.sup.2 of catalyst bed cross-section per hour, in the presence of a silver catalyst at from 550.degree. to 750.degree. C. and (d) finally, cooling and absorbing the hot reaction gases, and using the resulting heat of absorption and, if desired, the heat of reaction and/or the heat of condensation partially or completely for heating the recycle liquid, methanol containing impurities being used if desired and, after the stages (a) and (b) and before the stages (c) and (d), the measures of a stage (e) being carried out, wherein the gaseous mixture formed is passed through two layers of wire filter having a wire diameter of from 0.1 to 0.5 mm and a free layer volume of from 90 to 99.5 vol. %, based on the total volume of one wire layer, at a flow rate of from 7 to 13 m/sec in the first layer, and from 1 to 4 m/sec in the second layer.The formaldehyde obtainable by the process of the invention is a disinfectant, tanning agent, reducing agent and a useful starting material for the preparation of synthetic resins, adhesives and plastics.

7. 发明授权

US4227021A Production of adipic acid from acidic wash waters 失效
标题翻译：从酸性洗涤水中生产己二酸
公开(公告)号：US4227021A
公开(公告)日：1980-10-07
申请号：US901235
申请日：1978-04-28
申请人： Otto-Alfred Grosskinsky , Norbert Petri , Johannes Hein , Hans Leitner
发明人： Otto-Alfred Grosskinsky , Norbert Petri , Johannes Hein , Hans Leitner
IPC分类号： C07C55/14 , C07C51/00 , C07C51/42 , C07C51/487 , C07C67/00 , C07C51/24
CPC分类号： C07C51/487
摘要： An improved process for producing adipic acid from the acidic wash waters which arise in the process for oxidizing cyclohexane with air, by treatment with nitric acid at from 10.degree. to 50.degree. C., with removal of the heat of reaction by external cooling, wherein the reaction mixture is led, at a flow velocity of at least 2.0 m/sec, as a thin layer spirally in counter-current to the coolant, under conditions which do not perturb the flow of the reaction mixture.
摘要翻译：通过在10℃至50℃下用硝酸处理，通过外部冷却除去反应热而在由空气氧化环己烷的过程中产生的酸性洗涤水中生产己二酸的改进方法，其中在不干扰反应混合物的流动的条件下，反应混合物以至少2.0m / sec的流速被引导为与冷却剂逆流螺旋形的薄层。

8. 发明授权

US3954736A Production of lactams 失效
标题翻译：生产内酰胺
公开(公告)号：US3954736A
公开(公告)日：1976-05-04
申请号：US84546
申请日：1970-10-27
申请人： Norbert Petri
发明人： Norbert Petri
IPC分类号： B01J8/24 , C07B61/00 , C07D201/04
CPC分类号： C07D201/04
摘要： Continuous production of lactams by rearrangement of cycloalkanone oximes at from 210.degree. to 450.degree.C in contact with a supported catalyst in a fluidized bed wherein from 0.01 to 1 kg of steam is introduced above the fluidized bed for each kg of cycloalkanone oxime supplied. Lactams are starting materials for the production of synthetic polyamides suitable for fibers.
摘要翻译：通过在210℃至450℃下重新排列与负载型催化剂接触的流化床中连续生产内酰胺，其中在流化床上将0.01至1kg蒸汽引入每kg供应的环烷酮肟。内酰胺是用于生产适用于纤维的合成聚酰胺的起始原料。

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