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1. 发明授权

US09260593B2 Conjugated diene rubber modified with polar alkoxysilane, method and composition thereof 有权
标题翻译：用极性烷氧基硅烷改性的共轭二烯橡胶，其方法和组成
公开(公告)号：US09260593B2
公开(公告)日：2016-02-16
申请号：US13607450
申请日：2012-09-07
申请人： Chi-Chen Hsieh , Fu Lin , Chi-Ta Tsai , Hui-Kai Lin , Bo-Han Lin
发明人： Chi-Chen Hsieh , Fu Lin , Chi-Ta Tsai , Hui-Kai Lin , Bo-Han Lin
IPC分类号： C08C19/22 , C08L19/00 , C08F4/56 , C08F36/06 , C08F36/08 , C08F8/30 , C08C19/25 , C08C19/44 , C08F36/04
CPC分类号： C08L19/006 , C08C19/22 , C08C19/25 , C08C19/44 , C08F4/56 , C08F8/30 , C08F36/04 , C08F36/06 , C08F36/08
摘要： A modified conjugated diene rubber is disclosed. A method for producing the modified conjugated diene rubber includes providing an alkali metal ion-containing conjugated diene rubber; and reacting the alkali metal ion-containing conjugated diene rubber with an alkoxysilane to generate the modified conjugated diene rubber, the alkoxysilane being of the structural formula: wherein R1, R2, R3 are each independently selected from a group consisting of oxygen-containing C2-C12 group and nitrogen-containing C3-C12 group, the oxygen-containing C2-C12 group has a carbon atom directly connected to oxygen atom of the alkoxysilane, the nitrogen-containing C1-C12 group has a nitrogen atom directly connected to oxygen atom of the alkoxysilane, and R4 is selected from a group consisting of C3-C12 of alkyl, alkenyl, aryl, and alkoxy.
摘要翻译：公开了改性共轭二烯橡胶。改性共轭二烯橡胶的制造方法包括提供含碱金属离子的共轭二烯橡胶; 并使含有碱金属离子的共轭二烯橡胶与烷氧基硅烷反应以生成改性共轭二烯橡胶，该烷氧基硅烷具有以下结构式：其中R1，R2，R3各自独立地选自含氧C2- C12基和含氮C3-C12基，含氧C2-C12基具有与烷氧基硅烷的氧原子直接连接的碳原子，含氮C1-C12基具有与氧原子直接连接的氮原子烷氧基硅烷和R 4选自烷基，烯基，芳基和烷氧基的C 3 -C 12。

2. 发明申请

US20130150522A1 CONJUGATED DIENE RUBBER MODIFIED WITH POLAR ALKOXYSILANE, METHOD AND COMPOSITION THEREOF 有权
标题翻译：具有极性烷氧基硅烷改性的连接二烯橡胶，其方法和组合物
公开(公告)号：US20130150522A1
公开(公告)日：2013-06-13
申请号：US13607450
申请日：2012-09-07
申请人： Chi-Chen Hsieh , Fu Lin , Chi-Ta Tsai , Hui-Kai Lin , Bo-Han Lin
发明人： Chi-Chen Hsieh , Fu Lin , Chi-Ta Tsai , Hui-Kai Lin , Bo-Han Lin
IPC分类号： C08F236/10 , C08L9/06 , C08K3/36
CPC分类号： C08L19/006 , C08C19/22 , C08C19/25 , C08C19/44 , C08F4/56 , C08F8/30 , C08F36/04 , C08F36/06 , C08F36/08
摘要： A modified conjugated diene rubber is disclosed. A method for producing the modified conjugated diene rubber includes providing an alkali metal ion-containing conjugated diene rubber; and reacting the alkali metal ion-containing conjugated diene rubber with an alkoxysilane to generate the modified conjugated diene rubber, the alkoxysilane being of the structural formula: wherein R1, R2, R3 are each independently selected from a group consisting of oxygen-containing C2-C12 group and nitrogen-containing C3-C12 group, the oxygen-containing C2-C12 group has a carbon atom directly connected to oxygen atom of the alkoxysilane, the nitrogen-containing C1-C12 group has a nitrogen atom directly connected to oxygen atom of the alkoxysilane, and R4 is selected from a group consisting of C3-C12 of alkyl, alkenyl, aryl, and alkoxy.
摘要翻译：公开了改性共轭二烯橡胶。改性共轭二烯橡胶的制造方法包括提供含碱金属离子的共轭二烯橡胶; 并使含有碱金属离子的共轭二烯橡胶与烷氧基硅烷反应生成改性共轭二烯橡胶，该烷氧基硅烷具有以下结构式：其中R1，R2，R3各自独立地选自含氧C2- C12基和含氮C3-C12基，含氧C2-C12基具有与烷氧基硅烷的氧原子直接连接的碳原子，含氮C1-C12基具有与氧原子直接连接的氮原子烷氧基硅烷和R 4选自烷基，烯基，芳基和烷氧基的C 3 -C 12。

3. 发明授权

US09109071B2 Process for producing conjugated diene rubber and composite of the same rubber 有权
标题翻译：共轭二烯橡胶的制造方法和相同橡胶的复合体
公开(公告)号：US09109071B2
公开(公告)日：2015-08-18
申请号：US13326109
申请日：2011-12-14
申请人： Chi-Chen Hsieh , Fu Lin , Chi-Ta Tsai
发明人： Chi-Chen Hsieh , Fu Lin , Chi-Ta Tsai
IPC分类号： C08J5/14 , C08F36/04 , C08F36/06 , C08F136/04 , C08F136/06 , C08C19/44
CPC分类号： C08F36/04 , C08C19/44 , C08F36/06 , C08F136/04 , C08F136/06
摘要： A process for producing conjugated diene rubber and its composite includes polymerizing a conjugated diene or a conjugated diene and a vinyl aromatic hydrocarbon in a hydrocarbon solution by anionic polymerization to obtain conjugated diene rubber containing alkali metal in the polymer chain end reacting with at least one organic silane compound to become a modified conjugated diene rubber. After or during the modified conjugated diene rubber contacting with large amount of water, solvent and water content are removed from the modified conjugated diene by applicable hot sources, wherein coupling ratio of modified conjugated diene rubber is less than 40%, coupling ratio of modified conjugated diene rubber after contact with water is at least 50% The conjugated diene rubber and composite exhibit storage stability.
摘要翻译：共轭二烯橡胶及其复合体的制造方法包括通过阴离子聚合在烃溶液中使共轭二烯或共轭二烯和乙烯基芳烃聚合，得到在聚合物链末端含有碱金属的共轭二烯橡胶，其与至少一种有机硅烷化合物成为改性共轭二烯橡胶。在与大量水接触的改性共轭二烯橡胶之后或之后，通过适用的热源从改性共轭二烯中除去溶剂和水分，其中改性共轭二烯橡胶的偶合比小于40％，改性共轭二烯橡胶的偶合比二烯橡胶与水接触后至少为50％。共轭二烯橡胶和复合材料具有保存稳定性。

4. 发明申请

US20130053472A1 PROCESS FOR PRODUCING CONJUGATED DIENE RUBBER AND COMPOSITE OF THE SAME RUBBER 有权
标题翻译：生产混合二烯橡胶和相同橡胶复合材料的方法
公开(公告)号：US20130053472A1
公开(公告)日：2013-02-28
申请号：US13326109
申请日：2011-12-14
申请人： Chi-Chen Hsieh , Fu Lin , Chi-Ta Tsai
发明人： Chi-Chen Hsieh , Fu Lin , Chi-Ta Tsai
IPC分类号： C08J5/14 , C08F8/00
CPC分类号： C08F36/04 , C08C19/44 , C08F36/06 , C08F136/04 , C08F136/06
摘要： A process for producing conjugated diene rubber and its composite includes polymerizing a conjugated diene or a conjugated diene and a vinyl aromatic hydrocarbon in a hydrocarbon solution by anionic polymerization to obtain conjugated diene rubber containing alkali metal in the polymer chain end reacting a with at least one organic silane compound to become a modified conjugated diene rubber. After or during the modified conjugated diene rubber contacting with large amount of water, solvent and water content are removed from the modified conjugated diene by applicable hot sources, wherein coupling ratio of modified conjugated diene rubber is less than 40%, coupling ratio of modified conjugated diene rubber after contact with water is at least 50% The conjugated diene rubber and composite exhibit storage stability.
摘要翻译：共轭二烯橡胶及其复合体的制造方法包括通过阴离子聚合在烃溶液中使共轭二烯或共轭二烯和乙烯基芳烃聚合，得到在聚合物链末端含有碱金属的共轭二烯橡胶与至少一种有机硅烷化合物成为改性共轭二烯橡胶。在与大量水接触的改性共轭二烯橡胶之后或之后，通过适用的热源从改性共轭二烯中除去溶剂和水分，其中改性共轭二烯橡胶的偶合比小于40％，改性共轭二烯橡胶的偶合比二烯橡胶与水接触后至少为50％。共轭二烯橡胶和复合材料具有保存稳定性。

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