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1. 发明申请

US20150108412A1 METAL PHOSPHATE CONTAINING MANGANESE AND METHOD FOR ITS PRODUCTION 有权
标题翻译：含锰金属磷酸盐及其生产方法
公开(公告)号：US20150108412A1
公开(公告)日：2015-04-23
申请号：US14367531
申请日：2012-12-21
申请人： Chemische Fabrik Budenheim KG
发明人： Gunnar Buehler , Christian Graf , Andreas Jazdanian , Killian Schwarz , Michael Rapphahn
IPC分类号： H01M4/58 , H01M4/62 , C01B25/45
CPC分类号： H01M4/5825 , C01B25/377 , C01B25/45 , C01P2002/52 , C01P2002/54 , C01P2002/72 , C01P2002/77 , C01P2004/04 , C01P2004/20 , C01P2004/32 , C01P2004/40 , C01P2006/40 , H01M4/625
摘要： A manganese(Mn)-bearing monometal phosphate of the type Mn3(PO4)2.3H2O or mixed-metal phosphate of the type (Mnx, Mety)3(PO4)2.3H2O, wherein x+y=1 and Met represents one or more metals selected from Fe, Co, Ni, Sc, Ti, V, Cr, Cu, Zn, Be, Mg, Ca, Sr, Ba, Al, Zr, Hf, Re, Ru, La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb and Lu, characterised in that in the X-ray powder diffraction diagram the phosphate has peaks at 10.96±0.05, 12.78±0.17, 14.96±0.13, 17.34±0.15, 18.98±0.18, 21.75±0.21, 22.07±0.11, 22.97±0.10, 25.93±0.25, 26.95±0.30, 27.56±0.10, 29.19±0.12, 29.84±0.21, 30.27±0.12, 34.86±0.21, 35.00±0.20, 35.33±0.30, 35.58±0.10, 35.73±0.12, 42.79±0.45, 43.37±0.45, 44.70±0.15 and 44.93±0.20 degrees two-theta, based on CuKα-radiation.
摘要翻译： Mn3（PO4）2.3H2O型锰（Mn） - 单金属磷酸盐或类型（Mnx，Mety）3（PO4）2.3H2O的混合金属磷酸盐，其中x + y = 1，Met表示一种或多种选自Fe，Co，Ni，Sc，Ti，V，Cr，Cu，Zn，Be，Mg，Ca，Sr，Ba，Al，Zr，Hf，Re，Ru，La，Ce，Pr，Nd，Sm ，Eu，Gd，Tb，Dy，Ho，Er，Tm，Yb和Lu，其特征在于在X射线粉末衍射图中，磷酸盐在10.96±0.05,12.78±0.17,14.96±0.13,17.34±0.15 ，18.98±0.18，21.75±0.21,22.07±0.11,22.97±0.10,25.93±0.25,26.95±0.30,27.56±0.10,29.19±0.12,29.84±0.21,30.27±0.12,34.86±0.21,35.00±0.20,35.33 基于CuKα辐射，±0.30,35.58±0.10,35.73±0.12,42.79±0.45,43.37±0.45,4.70±0.15和44.93±0.20度2-θ。

2. 发明申请

US20150001446A1 METAL PHOSPHATES AND PROCESS FOR THE PREPARATION THEREOF 有权
标题翻译：金属磷酸盐及其制备方法
公开(公告)号：US20150001446A1
公开(公告)日：2015-01-01
申请号：US14367534
申请日：2012-12-21
申请人： Chemische Fabrik Budenheim KG
发明人： Gunnar Buehler , Christian Graf , Andreas Jazdanian , Killian Schwarz , Michael Rapphahn
IPC分类号： H01M4/58 , C01B25/38 , C01B25/45
CPC分类号： H01M4/5825 , C01B25/37 , C01B25/375 , C01B25/377 , C01B25/38 , C01B25/45 , H01B1/06 , H01M10/0525 , H01M2220/20
摘要： A process for producing a phosphate by: introducing oxidic metal(II)-, metal(III)-metal(FV) or compounds with mixed oxide stages selected from hydroxides, oxides, oxide-hydroxides, oxide-hydrates, carbonates and hydroxide carbonates, of at least one of the metals Mn, Fe, Co and Ni with the elemental forms or alloys of at least one of the metals Mn, Fe, Co and/or Ni into an aqueous medium containing phosphoric acid, and reacting the oxidic metal compounds with elemental forms or alloys of the metals to obtain divalent metal ions, removing solid substances, producing an alkali metal phosphate receiver solution with a pH-value of 5 to 8 and metering the aqueous solution into the receiver solution and at the same time metering a basic aqueous alkali hydroxide solution that the pH-value of the resulting reaction mixture is kept in the region of 5 to 8 to precipitate the desired phosphate.
摘要翻译：通过以下方式制备磷酸盐的方法：将氧化金属（II） - ，金属（III） - 金属（FV）或具有选自氢氧化物，氧化物，氧化物 - 氢氧化物，氧化物 - 水合物，碳酸盐和氢氧化碳酸盐的混合氧化物阶段的化合物引入，的金属Mn，Fe，Co和Ni中的至少一种与至少一种金属Mn，Fe，Co和/或Ni的元素形式或合金混合到含有磷酸的水性介质中，并使氧化金属化合物用金属的元素形式或合金形成二价金属离子，去除固体物质，制备pH值为5〜8的碱金属磷酸盐接收溶液，并将水溶液计量到接收溶液中，同时计量将所得反应混合物的pH值保持在5至8的范围内以沉淀所需磷酸盐的碱性碱性氢氧化碱水溶液。

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