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1. 发明授权

US07550537B2 Organo-dilithium compound and process for preparing the same 有权
标题翻译：有机 - 二锂化合物及其制备方法
公开(公告)号：US07550537B2
公开(公告)日：2009-06-23
申请号：US11876596
申请日：2007-10-22
申请人： Carl L. Willis , Daniel E. Goodwin , Grant W. Haddix , Pierre N. Tutunjian , Joy P. Cocchiara , Harvey E. Atwood , Craig A. Stevens
发明人： Carl L. Willis , Daniel E. Goodwin , Grant W. Haddix , Pierre N. Tutunjian , Joy P. Cocchiara , Harvey E. Atwood , Craig A. Stevens
IPC分类号： C08F25/02
CPC分类号： C08F36/04 , C07F1/02 , C08F4/488
摘要： Disclosed is an anionic diinitiator prepared using a diisopropenyl benzene compound and an organo lithium compound having primary polymerization sites. The anionic diinitiators are prepared by admixing a diisopropenyl benzene compound with diethyl ether, ethylene, an organo lithium compound, and a solvent under reaction conditions sufficient to prepare a diinitiator having primary lithium alkyl reactive sites. The diinitiators are particularly useful in preparing block copolymers.
摘要翻译：公开了使用二异丙烯基苯化合物和具有一次聚合位点的有机锂化合物制备的阴离子二引发剂。通过将二异丙烯基苯化合物与二乙醚，乙烯，有机锂化合物和溶剂混合制备阴离子二引发剂，该反应条件足以制备具有伯烷基反应活性位点的二引发剂。二引发剂在制备嵌段共聚物中特别有用。

2. 发明申请

US20080111256A1 ANIONIC POLYMERIZATION DIINITIATOR AND PROCESS FOR PREPARING SAME 有权
标题翻译：阴离子聚合反应器及其制备方法
公开(公告)号：US20080111256A1
公开(公告)日：2008-05-15
申请号：US11876596
申请日：2007-10-22
申请人： Carl L. Willis , Daniel E. Goodwin , Grant W. Haddix , Pierre N. Tutunjian , Joy P. Cocchiara , Harvey E. Atwood , Craig A. Stevens
发明人： Carl L. Willis , Daniel E. Goodwin , Grant W. Haddix , Pierre N. Tutunjian , Joy P. Cocchiara , Harvey E. Atwood , Craig A. Stevens
IPC分类号： C07F1/02
CPC分类号： C08F36/04 , C07F1/02 , C08F4/488
摘要： Disclosed is an anionic diinitiator prepared using a diisopropenyl benzene compound and an organo lithium compound having primary polymerization sites. The anionic diinitiators are prepared by admixing a diisopropenyl benzene compound with diethyl ether, ethylene, an organo lithium compound, and a solvent under reaction conditions sufficient to prepare a diinitiator having primary lithium alkyl reactive sites. The diinitiators are particularly useful in preparing block copolymers.
摘要翻译：公开了使用二异丙烯基苯化合物和具有一次聚合位点的有机锂化合物制备的阴离子二引发剂。通过将二异丙烯基苯化合物与二乙醚，乙烯，有机锂化合物和溶剂混合制备阴离子二引发剂，该反应条件足以制备具有伯烷基反应活性位点的二引发剂。二引发剂在制备嵌段共聚物中特别有用。

3. 发明授权

US07285596B2 Anionic polymerization diinitiator and process for preparing same 有权
标题翻译：阴离子聚合二引发剂及其制备方法
公开(公告)号：US07285596B2
公开(公告)日：2007-10-23
申请号：US10947011
申请日：2004-09-22
申请人： Carl L. Willis , Daniel E. Goodwin , Grant W. Haddix , Pierre N. Tutunjian , Joy P. Cocchiara , Harvey E. Atwood , Craig A. Stevens
发明人： Carl L. Willis , Daniel E. Goodwin , Grant W. Haddix , Pierre N. Tutunjian , Joy P. Cocchiara , Harvey E. Atwood , Craig A. Stevens
IPC分类号： C08F25/02
CPC分类号： C08F36/04 , C07F1/02 , C08F4/488
摘要： Disclosed is an anionic diinitiator prepared using a diisopropenyl benzene compound and an organo lithium compound having primary polymerization sites. The anionic diinitiators are prepared by admixing a diisopropenyl benzene compound with diethyl ether, ethylene, an organo lithium compound, and a solvent under reaction conditions sufficient to prepare a diinitiator having primary lithium alkyl reactive sites. The diinitiators are particularly useful in preparing block copolymers.
摘要翻译：公开了使用二异丙烯基苯化合物和具有一次聚合位点的有机锂化合物制备的阴离子二引发剂。通过将二异丙烯基苯化合物与二乙醚，乙烯，有机锂化合物和溶剂混合制备阴离子二引发剂，该反应条件足以制备具有伯烷基反应活性位点的二引发剂。二引发剂在制备嵌段共聚物中特别有用。

4. 再颁专利

USRE39559E1 Butadiene polymers having terminal functional groups 有权
标题翻译：具有末端官能团的丁二烯聚合物
公开(公告)号：USRE39559E1
公开(公告)日：2007-04-10
申请号：US10657064
申请日：2003-09-05
申请人： Dale L. Handlin, Jr. , Daniel E. Goodwin , Carl L. Willis , David J. St. Clair , John D. Wilkey , Michael J. Modic , Craig A. Stevens
发明人： Dale L. Handlin, Jr. , Daniel E. Goodwin , Carl L. Willis , David J. St. Clair , John D. Wilkey , Michael J. Modic , Craig A. Stevens
IPC分类号： C08F8/00
CPC分类号： C08L19/006 , C08C19/44 , C08F136/06 , C08G18/0823 , C08G18/6208 , C08G18/8175 , C08G63/00 , C08G64/18 , C08G69/00 , C08G81/024 , C08L15/00 , C08F4/488 , C08G18/62
摘要： Hydrogenated butadiene polymers having terminal functional groups have minimum viscosity at any molecular weight when the 1,2-addition is between 30% and 70%. Hydrogenated butadiene polymers having about two terminal hydroxyl groups per molecule have surprisingly lower viscosities at 30% to 70% 1,2-addition than similar polymers having either higher or lower amounts of 1,2-addition. The polymers are useful in making coatings, sealants, binders, and block copolymers with polyesters, polyamides, and polycarbonates.
摘要翻译：具有末端官能团的氢化丁二烯聚合物在1,2-加成量在30％至70％之间时具有任何分子量下的最小粘度。每分子具有约两个末端羟基的氢化丁二烯聚合物具有比具有更高或更低量1,2-加成的类似聚合物在30％至70％1,2-加成中具有惊人的较低粘度。聚合物可用于制备涂料，密封剂，粘合剂和与聚酯，聚酰胺和聚碳酸酯的嵌段共聚物。

5. 发明授权

US5405911A Butadiene polymers having terminal functional groups 失效
标题翻译：具有末端官能团的丁二烯聚合物
公开(公告)号：US5405911A
公开(公告)日：1995-04-11
申请号：US306552
申请日：1994-09-15
申请人： Dale L. Handlin, Jr. , Daniel E. Goodwin , Carl L. Willis , David J. St. Clair , John D. Wilkey , Michael J. Modic , Craig A. Stevens
发明人： Dale L. Handlin, Jr. , Daniel E. Goodwin , Carl L. Willis , David J. St. Clair , John D. Wilkey , Michael J. Modic , Craig A. Stevens
IPC分类号： C08C19/44 , C08F136/06 , C08G18/08 , C08G18/62 , C08G18/81 , C08G63/00 , C08G64/18 , C08G69/00 , C08G81/02 , C08L15/00 , C08L19/00 , C08F8/00
CPC分类号： C08L19/006 , C08C19/44 , C08F136/06 , C08G18/0823 , C08G18/6208 , C08G18/8175 , C08G63/00 , C08G64/18 , C08G69/00 , C08G81/024 , C08L15/00
摘要： Hydrogenated butadiene polymers having terminal functional groups have minimum viscosity at any molecular weight when the 1,2-addition is between 30% and 70% Hydrogenated butadiene polymers having about two terminal hydroxyl groups per molecule have surprisingly lower viscosities at 30% to 70% 1,2-addition than similar polymers having either higher or lower amounts of 1,2-addition. The polymers are useful in making coatings, sealants, binders, and block copolymers with polyesters, polyamides, and polycarbonates.
摘要翻译：具有末端官能团的氢化丁二烯聚合物在1,2-加成量为30％至70％时具有任何分子量的最小粘度。每分子具有约两个末端羟基的氢化丁二烯聚合物具有30％至70％1的令人惊奇的较低粘度，比具有更高或更低量的1,2-加成的类似聚合物进行2-加成。聚合物可用于制备涂料，密封剂，粘合剂和与聚酯，聚酰胺和聚碳酸酯的嵌段共聚物。

6. 再颁专利

USRE39617E1 Butadiene polymers having terminal functional groups 有权
标题翻译：具有末端官能团的丁二烯聚合物
公开(公告)号：USRE39617E1
公开(公告)日：2007-05-08
申请号：US10655988
申请日：2003-09-05
申请人： Dale L. Handlin, Jr. , Daniel E. Goodwin , Carl L. Willis , David J. St. Clair , John D. Wilkey , Michael J. Modic , Craig A. Stevens
发明人： Dale L. Handlin, Jr. , Daniel E. Goodwin , Carl L. Willis , David J. St. Clair , John D. Wilkey , Michael J. Modic , Craig A. Stevens
IPC分类号： C08F8/00
CPC分类号： C08L19/006 , C08C19/44 , C08F136/06 , C08G18/0823 , C08G18/6208 , C08G18/8175 , C08G63/00 , C08G64/18 , C08G69/00 , C08G81/024 , C08L15/00 , C08F4/488 , C08G18/62
摘要： Hydrogenated butadiene polymers having terminal functional groups have minimum viscosity at any molecular weight when the 1,2-addition is between 30% and 70% Hydrogenated butadiene polymers having about two terminal hydroxyl groups per molecule have surprisingly lower viscosities at 30% to 70% 1,2-addition than similar polymers having either higher or lower amounts of 1,2-addition. The polymers are useful in making coatings, sealants, binders, and block copolymers with polyesters, polyamides, and polycarbonates.
摘要翻译：具有末端官能团的氢化丁二烯聚合物在1,2-加成量为30％至70％时具有任何分子量的最小粘度。每分子具有约两个末端羟基的氢化丁二烯聚合物具有30％至70％1的令人惊奇的较低粘度，比具有更高或更低量的1,2-加成的类似聚合物进行2-加成。聚合物可用于制备涂料，密封剂，粘合剂和与聚酯，聚酰胺和聚碳酸酯的嵌段共聚物。

7. 发明授权

US5393843A Butadiene polymers having terminal functional groups 失效
标题翻译：具有末端官能团的丁二烯聚合物
公开(公告)号：US5393843A
公开(公告)日：1995-02-28
申请号：US938917
申请日：1992-08-31
申请人： Dale L. Handlin, Jr. , Daniel E. Goodwin , Carl L. Willis , David J. St. Clair , John D. Wilkey , Michael J. Modic , Craig A. Stevens
发明人： Dale L. Handlin, Jr. , Daniel E. Goodwin , Carl L. Willis , David J. St. Clair , John D. Wilkey , Michael J. Modic , Craig A. Stevens
IPC分类号： C08C19/44 , C08F136/06 , C08G18/08 , C08G18/62 , C08G18/81 , C08G63/00 , C08G64/18 , C08G69/00 , C08G81/02 , C08L15/00 , C08L19/00 , C08F8/00
CPC分类号： C08L19/006 , C08C19/44 , C08F136/06 , C08G18/0823 , C08G18/6208 , C08G18/8175 , C08G63/00 , C08G64/18 , C08G69/00 , C08G81/024 , C08L15/00
摘要： Hydrogenated butadiene polymers having terminal functional groups have minimum viscosity at any molecular weight when the 1,2-addition is between 30% and 70%. Hydrogenated butadiene polymers having about two terminal hydroxyl groups per molecule have surprisingly lower viscosities at 30% to 70% 1,2-addition than similar polymers having either higher or lower amounts of 1,2-addition. The polymers are useful in making coatings, sealants, binders, and block copolymers with polyesters, polyamides, and polycarbonates.
摘要翻译：具有末端官能团的氢化丁二烯聚合物在1,2-加成量在30％至70％之间时具有任何分子量下的最小粘度。每分子具有约两个末端羟基的氢化丁二烯聚合物具有比具有更高或更低量1,2-加成的类似聚合物在30％至70％1,2-加成中具有惊人的较低粘度。聚合物可用于制备涂料，密封剂，粘合剂和与聚酯，聚酰胺和聚碳酸酯的嵌段共聚物。

8. 发明授权

US5151475A Termination of anionic polymerization 失效
标题翻译：阴离子聚合的终止
公开(公告)号：US5151475A
公开(公告)日：1992-09-29
申请号：US685111
申请日：1991-04-15
申请人： Craig A. Stevens , Carma J. Gibler , Linda R. Chamberlain , Thomas F. Brownscombe
发明人： Craig A. Stevens , Carma J. Gibler , Linda R. Chamberlain , Thomas F. Brownscombe
IPC分类号： C08C19/44 , C08F2/38 , C08F2/42
CPC分类号： C08C19/44 , C08F2/42
摘要： This is an improvement upon a process which comprises anionically polymerizing monomers with an anionic polymerization initiator in a suitable solvent thereby creating a living polymer. The improvement comprises terminating the polymerization by the addition of a terminating agent selected from the group consisting of boranes, ammonia, halogens, hydrocarbons containing a C-H group where the carbon is connected directly to a triply-bound carbon or to two doubly-bound carbons and silanes.
摘要翻译：这是对包括阴离子聚合单体与阴离子聚合引发剂在合适溶剂中的方法的改进，从而产生活性聚合物。改进包括通过加入选自硼烷，氨，卤素，含有CH基团的碳的终止剂终止聚合，其中碳直接连接到三键结合的碳或两个双键结合的碳上，以及硅烷

9. 发明授权

US06349522B1 Brick block and process and apparatus therefor 失效
标题翻译：砖块及其工艺和设备
公开(公告)号：US06349522B1
公开(公告)日：2002-02-26
申请号：US09557949
申请日：2000-04-24
申请人： Craig A. Stevens
发明人： Craig A. Stevens
IPC分类号： E04G910
CPC分类号： E04C1/395 , B28B7/0061 , B28B7/0073 , B28B7/10
摘要： An apparatus and process for the manufacture of brick block, i.e. a concrete chimney or wall block, with an impressed brick grout pattern on the face thereof, comprises a mold adapted to fit a known concrete block manufacturing machine. The mold has grout bars to impress a simulated laid brick pattern onto at least one vertical face of the block, the grout bar moveable in and out from a wall of the mold by hydraulic components. The hydraulic components utilize a unique multi-piston hydraulic block.
摘要翻译：用于制造砖块，即混凝土烟囱或墙体砖的装置和方法，其表面上具有压痕砖灌浆图案，包括适于装配已知混凝土块制造机器的模具。模具具有灌浆棒，以将模拟的铺设的砖图案压印在块的至少一个垂直面上，水泥浆杆通过液压组件可移动进出模具的壁。液压元件采用独特的多活塞液压块。

10. 发明授权

US5543472A Concurrent epoxidation and catalyst residue extraction 失效
标题翻译：并行环氧化和催化剂残渣萃取
公开(公告)号：US5543472A
公开(公告)日：1996-08-06
申请号：US442520
申请日：1995-05-16
申请人： Craig A. Stevens , Bhaskar P. Rao , Cary A. Veith , James R. Erickson
发明人： Craig A. Stevens , Bhaskar P. Rao , Cary A. Veith , James R. Erickson
IPC分类号： C08C2/04 , C08C19/06 , C08F8/08
CPC分类号： C08C2/04 , C08C19/06
摘要： A process for the concurrent epoxidation of, and catalyst residue extraction from, anionically polymerized diene-containing polymers which have been hydrogenated using a Group VIII metal catalyst, said process comprising:(a) introducing a catalyst residue-containing diene-containing polymer cement into a reactor,(b) heating the polymer cement to a temperature of 25.degree. to 65.degree. C.,(c) contacting the polymer cement with a caustic solution,(d) contacting the polymer cement with a peracid solution,(e) mixing the polymer, caustic, and acid at 25.degree. to 65.degree. C. for 1/2 to 3 hours,(f) optionally adding sufficient caustic solution to neutralize excess acid while continuing the mixing,(g) adding sufficient water such that the aqueous/organic phase weight ratio is from 0.2:1 to 1:1 while continuing the mixing,(h) allowing the phases to settle for 5 to 90 minutes,(i) removing the aqueous phase from the reactor,(j) optionally repeating steps (g), (h), and (i) until the catalyst residue contents are less than 10 ppm, and(k) removing the polymer cement from the reactor and removing the solvent to recover the epoxidized polymer.
摘要翻译：一种使用VIII族金属催化剂进行氢化的阴离子聚合的含二烯烃聚合物的并行环氧化和催化剂残余物萃取的方法，所述方法包括：（a）将含催化剂残余物的含二烯烃的聚合物水泥引入反应器，（b）将聚合物粘合剂加热到25℃至65℃的温度，（c）使聚合物粘合剂与苛性碱溶液接触，（d）使聚合物粘合剂与过酸溶液接触，（e）混合 25℃至65℃的聚合物，苛性碱和酸，+ E，1/2 + EE至3小时，（f）任选地加入足够的苛性碱溶液以中和过量的酸，同时继续混合，（g）加入足够的水使得水/有机相重量比为0.2:1至1:1，同时继续混合，（h）允许相沉降5至90分钟，（i）从反应器中除去水相，（j）任选地重复步骤（g），（h）和（i）直到cata st渣残渣含量小于10ppm，（k）从反应器中除去聚合物粘合剂并除去溶剂以回收环氧化聚合物。

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