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1. 发明授权

US07744834B2 Method for manufacturing metal nanoparticles 有权
标题翻译：制造金属纳米粒子的方法
公开(公告)号：US07744834B2
公开(公告)日：2010-06-29
申请号：US11785094
申请日：2007-04-13
申请人： Kwi-Jong Lee , Jae-Woo Joung , Byung-Ho Jun
发明人： Kwi-Jong Lee , Jae-Woo Joung , Byung-Ho Jun
IPC分类号： C01G5/00 , C01G55/00 , C01G7/00 , C22B11/00 , C09D11/00 , C22C5/06 , C22C5/02 , C22C5/04
CPC分类号： C22B11/04 , B22F1/0018 , B22F9/24 , B82Y30/00 , C22B3/22 , C22B3/44 , Y02P10/234
摘要： A method for manufacturing metal nanoparticles, the method including forming a mixture by dissociating a metallic salt of a metal selected from the group consisting of Ag, Pd, Pt, Au and an alloy thereof as a metal precursor in fatty acid; and adding a metallic salt of a metal selected from the group consisting of Sn(NO3)2, Sn(CH3CO2)2, and Sn(acac)2 as a metallic catalyst into the mixture and mixing the mixture and the metallic salt. According to the method, metal nanoparticles have a uniform particle size distribution and a high yield by performing in a non-aqueous environment without using any organic solvent, and are environmentally friendly due to no use of a reducing agent.
摘要翻译：一种金属纳米粒子的制造方法，其特征在于，通过使选自Ag，Pd，Pt，Au及其合金的金属的金属盐作为金属前体在脂肪酸中分解而形成混合物，并将作为金属催化剂的选自Sn（NO 3）2，Sn（CH 3 CO 2）2和Sn（acac）2）的金属的金属盐加入混合物中，并将该混合物和金属盐混合。根据该方法，金属纳米粒子在不使用有机溶剂的情况下在非水环境中进行，具有均匀的粒度分布和高产率，并且由于不使用还原剂而是环境友好的。

2. 发明申请

US20080041270A1 Method for manufacturing metal nanoparticles 有权
标题翻译：制造金属纳米粒子的方法
公开(公告)号：US20080041270A1
公开(公告)日：2008-02-21
申请号：US11785094
申请日：2007-04-13
申请人： Kwi-Jong Lee , Jae-Woo Joung , Byung-Ho Jun
发明人： Kwi-Jong Lee , Jae-Woo Joung , Byung-Ho Jun
IPC分类号： C22B11/00 , C01G5/00 , C22B3/44 , C01G55/00
CPC分类号： C22B11/04 , B22F1/0018 , B22F9/24 , B82Y30/00 , C22B3/22 , C22B3/44 , Y02P10/234
摘要： The present invention relates to a method for manufacturing metal nanoparticles, more particularly, to a method for manufacturing metal nanoparticles, the method comprising: forming a mixture by dissociating a metal precursor in fatty acid; and adding a metallic salt of a metal selected from the group consisting of Sn, Mg and Fe as a metallic catalyst into the mixture and mixing the mixture and the metallic salt. According to the present invention, metal nanoparticles have a uniform particle size distribution and a high yield by performing in a non-aqueous environment without using any organic solvent, and may be environment-friendlily due to no use of a reducing agent.
摘要翻译：本发明涉及金属纳米粒子的制造方法，特别涉及金属纳米粒子的制造方法，该方法包括：通过使脂肪酸中的金属前体离解形成混合物; 并将作为金属催化剂的选自Sn，Mg和Fe的金属的金属盐加入混合物中，并将该混合物和金属盐混合。根据本发明，通过在非水环境中进行而不使用任何有机溶剂，金属纳米颗粒具有均匀的粒度分布和高产率，并且由于不使用还原剂而可能是环境友好的。

3. 发明授权

US07935169B2 Apparatus and method for manufacturing metal nanoparticles 有权
标题翻译：用于制造金属纳米粒子的装置和方法
公开(公告)号：US07935169B2
公开(公告)日：2011-05-03
申请号：US12149709
申请日：2008-05-07
申请人： Young-Il Lee , Jae-Woo Joung , Byung-Ho Jun , Joon-Rak Choi , Kwi-Jong Lee
发明人： Young-Il Lee , Jae-Woo Joung , Byung-Ho Jun , Joon-Rak Choi , Kwi-Jong Lee
IPC分类号： B22F9/24
CPC分类号： B22F9/24 , B22F2998/00 , Y10S977/896 , B22F1/0018 , B22F3/003
摘要： The present invention relates to an apparatus and a method of manufacturing metal nanoparticles, and more particularly to an apparatus including: a precursor supplying part which supplies a precursor solution of metal nanoparticles; a first heating part which is connected with the precursor supplying part, includes a reactor channel having a diameter of 1 to 50 mm, and is heated to the temperature range where any particle is not produced; a second heating part which is connected with the first heating part, includes a reactor channel having a diameter of 1 to 50 mm, and is heated to the temperature range where particles are produced; and a cooler which is connected with the second heating part and collects and cools metal nanoparticles produced at the second heating part which allows continuous mass production of metal nanoparticles.
摘要翻译：本发明涉及一种制造金属纳米颗粒的装置和方法，更具体地涉及一种装置，包括：提供金属纳米颗粒的前体溶液的前体供应部分; 与前体供给部连接的第一加热部包括直径为1〜50mm的反应器通道，并被加热到不产生任何粒子的温度范围; 与第一加热部连接的第二加热部包括直径为1〜50mm的反应器通道，并被加热到制造粒子的温度范围; 以及冷却器，其与第二加热部件连接并且收集和冷却在第二加热部件处产生的金属纳米颗粒，其允许连续大量生产金属纳米颗粒。

4. 发明授权

US07591872B1 Method for producing silver nanoparticles and conductive ink 失效
标题翻译：制备银纳米颗粒和导电油墨的方法
公开(公告)号：US07591872B1
公开(公告)日：2009-09-22
申请号：US11498837
申请日：2006-08-04
申请人： Byung-Ho Jun , Kwi-Jong Lee , Hye-Jin Cho , Jae-Woo Joung
发明人： Byung-Ho Jun , Kwi-Jong Lee , Hye-Jin Cho , Jae-Woo Joung
IPC分类号： B22F9/24
CPC分类号： H01B1/22 , B22F9/24 , B22F2998/00 , C08K3/08 , C09D7/62 , C09D7/67 , C09D11/38 , C09D11/52 , Y10S977/896 , Y10T428/2982 , B22F1/0018
摘要： A method of producing metal nanoparticles in a high yield rate and uniform shape and size, which is thus suitable for mass production. In addition, metal nanoparticles are provided that have superior dispersion stability when re-dispersed in various organic solvents, which thus suitable for use as a conductive ink having high conductivity. The method of producing nanoparticles includes mixing a metal precursor with a copper compound to a hydrocarbon based solvent, mixing an amine-based compound to the mixed solution of the metal precursor with copper compound and hydrocarbon based solvent, and mixing a compound including one or more atoms having at least one lone pair, selected from a group consisting of nitrogen, oxygen, sulfur and phosphorous to the mixed solution of the amine-based compound, metal precursor with a copper compound and hydrocarbon based solvent.
摘要翻译：以高产率和均匀的形状和尺寸制造金属纳米粒子的方法，因此适合批量生产。此外，提供了当重新分散在各种有机溶剂中时具有优异的分散稳定性的金属纳米颗粒，因此适合用作具有高导电性的导电油墨。制造纳米颗粒的方法包括将金属前体与铜化合物混合到烃类溶剂中，将胺类化合物与金属前体与铜化合物和烃类溶剂的混合溶液混合，并将包含一种或多种具有至少一个选自由氮，氧，硫和磷组成的组的孤对的原子与胺基化合物，金属前体与铜化合物和烃基溶剂的混合溶液。

5. 发明申请

US20090223410A1 METHOD FOR PRODUCING SILVER NANOPARTICLES AND CONDUCTIVE INK 失效
标题翻译：生产银纳米颗粒和导电油墨的方法
公开(公告)号：US20090223410A1
公开(公告)日：2009-09-10
申请号：US11498837
申请日：2006-08-04
申请人： Byung-Ho Jun , Kwi-Jong Lee , Hye-Jin Cho , Jae-Woo Joung
发明人： Byung-Ho Jun , Kwi-Jong Lee , Hye-Jin Cho , Jae-Woo Joung
IPC分类号： C09D11/00 , B22F9/20 , B32B15/02
CPC分类号： H01B1/22 , B22F9/24 , B22F2998/00 , C08K3/08 , C09D7/62 , C09D7/67 , C09D11/38 , C09D11/52 , Y10S977/896 , Y10T428/2982 , B22F1/0018
摘要： A method of producing metal nanoparticles in a high yield rate and uniform shape and size, which is thus suitable for mass production. In addition, metal nanoparticles are provided that have superior dispersion stability when re-dispersed in various organic solvents, which thus suitable for use as a conductive ink having high conductivity. The method of producing nanoparticles includes mixing a metal precursor with a copper compound to a hydrocarbon based solvent, mixing an amine-based compound to the mixed solution of the metal precursor with copper compound and hydrocarbon based solvent, and mixing a compound including one or more atoms having at least one lone pair, selected from a group consisting of nitrogen, oxygen, sulfur and phosphorous to the mixed solution of the amine-based compound, metal precursor with a copper compound and hydrocarbon based solvent.
摘要翻译：以高产率和均匀的形状和尺寸制造金属纳米粒子的方法，因此适合批量生产。此外，提供了当重新分散在各种有机溶剂中时具有优异的分散稳定性的金属纳米颗粒，因此适合用作具有高导电性的导电油墨。制造纳米颗粒的方法包括将金属前体与铜化合物混合到烃类溶剂中，将胺类化合物与金属前体与铜化合物和烃类溶剂的混合溶液混合，并将包含一种或多种具有至少一个选自由氮，氧，硫和磷组成的组的孤对的原子与胺基化合物，金属前体与铜化合物和烃基溶剂的混合溶液。

6. 发明申请

US20080138643A1 Method for manufacturing copper nanoparticles and copper nanoparticles manufactured using the same 审中-公开
标题翻译：制造使用其的铜纳米粒子和铜纳米粒子的制造方法
公开(公告)号：US20080138643A1
公开(公告)日：2008-06-12
申请号：US11902238
申请日：2007-09-20
申请人： Kwi-Jong Lee , Jae-Woo Joung , Young-Il Lee , Byung-Ho Jun
发明人： Kwi-Jong Lee , Jae-Woo Joung , Young-Il Lee , Byung-Ho Jun
IPC分类号： B22F1/02 , B22F9/16
CPC分类号： B22F9/30 , B22F1/0018 , B22F9/24 , B82Y30/00 , Y10T428/12181
摘要： The present invention relates to a method for manufacturing copper nanoparticles and copper nanoparticles thus manufactured, in particular, to a method for manufacturing copper nanoparticles, wherein the method includes producing mixture by mixing one or more copper salt selected from a group consisting of CuCl2, Cu(NO3)2, CuSO4, (CH3COO)2Cu and Cu(acac)2 (copper acetyloacetate) with fatty acid and dissociating; and reacting the mixture by heating and copper nanoparticle.According to the present invention, copper nanoparticles can be synthesized in a uniform size and a high concentration using general copper salt as a copper precursor material in non-aqueous system without designing precursor material. The present invention is not only environment-friendly, but also economical as highly expensive equipment is not demanded.
摘要翻译：本发明涉及一种制造铜纳米颗粒的方法，特别涉及一种制造铜纳米颗粒的方法，其中该方法包括通过混合一种或多种选自CuCl

7. 发明授权

US07988761B2 Method for manufacturing metal nanoparticles comprising rod-shaped nanoparticles 失效
标题翻译：制造包含棒状纳米粒子的金属纳米粒子的方法
公开(公告)号：US07988761B2
公开(公告)日：2011-08-02
申请号：US11987182
申请日：2007-11-28
申请人： Byung-Ho Jun , Jae-Woo Joung
发明人： Byung-Ho Jun , Jae-Woo Joung
IPC分类号： B22F9/16 , B22F9/18 , B22F9/20
CPC分类号： B22F1/0025 , B22F9/24 , B22F2998/00 , B82Y30/00 , Y10S977/773 , Y10S977/775 , Y10S977/777 , Y10S977/81 , B22F2301/10
摘要： The present invention relates to a method for manufacturing metal nanoparticles containing rod-shaped nanoparticles, the method including: producing metal oxide nanoparticle intermediates having at least rod-shaped metal oxide nanoparticles by heating a mixture of a nonpolar solvent, a metal precursor and an amine including secondary amine at 60-300° C.; producing metal nanoparticles by adding a capping molecule and a reducing agent to the mixture and heating the result mixture at 90-150° C.; and recovering the metal nanoparticles. According to the present invention, the shape of metal nanoparticle can be controlled by mixing primary amines or secondary amines as proper ratio without using apparatus additionally, as well as, the size of metal nanoparticle can be controlled to several nm.
摘要翻译：本发明涉及一种制造含有棒状纳米颗粒的金属纳米颗粒的方法，所述方法包括：通过加热非极性溶剂，金属前体和胺的混合物来生产至少具有棒状金属氧化物纳米颗粒的金属氧化物纳米颗粒中间体包括在60-300℃的仲胺。通过向混合物中加入封端分子和还原剂制备金属纳米颗粒，并将结果混合物在90-150℃下加热。并回收金属纳米粒子。根据本发明，金属纳米颗粒的形状可以通过混合伯胺或仲胺作为适当比例而不使用另外的装置，以及金属纳米颗粒的尺寸可以控制到几nm来控制。

8. 发明授权

US07935170B2 Method for manufacturing copper-based nanoparticles 有权
标题翻译：铜基纳米粒子的制造方法
公开(公告)号：US07935170B2
公开(公告)日：2011-05-03
申请号：US11987162
申请日：2007-11-28
申请人： Byung-Ho Jun , Jae-Woo Joung , Joon-Rak Choi
发明人： Byung-Ho Jun , Jae-Woo Joung , Joon-Rak Choi
IPC分类号： B22F9/24
CPC分类号： C01G3/02 , B22F9/20 , B22F2998/00 , B82Y30/00 , C01P2004/04 , C01P2004/64 , Y10S977/896 , B22F2301/10
摘要： The present invention relates to a method for manufacturing copper-based nanoparticles, in particular, to a method for manufacturing copper-based nanoparticles, wherein the method includes producing CuO nanoparticles by mixing CuO micropowder and alkylamine in a nonpolar solvent and heating the mixture at 60-300° C.; and producing copper-based nanoparticles by mixing a capping molecule and a reducing agent with the CuO nanoparticles and heating the mixture at 60-120° C.According to the present invention, copper-based nanoparticles can be synthesized using CuO, but not requiring any inorganic reducing agent, in a high yield and a high concentration, so that it allows mass production and easy controlling to desired oxidation number of nanoparticles.
摘要翻译：本发明涉及一种铜基纳米粒子的制造方法，特别涉及一种铜基纳米粒子的制造方法，其特征在于，该方法包括通过将CuO微粉末和烷基胺混合在非极性溶剂中并在60℃加热混合物来制备CuO纳米粒子 -300°C。并通过将封端分子和还原剂与CuO纳米颗粒混合并在60-120℃下加热混合物来生产铜基纳米颗粒。根据本发明，可以使用CuO合成铜基纳米颗粒，但不需要任何无机还原剂，以高产率和高浓度，使得其允许批量生产并容易控制纳米颗粒的所需氧化数。

9. 发明申请

US20100319489A1 APPARATUS AND METHOD FOR MANUFACTURING METAL NANOPARTICLES 失效
标题翻译：用于制造金属纳米颗粒的装置和方法
公开(公告)号：US20100319489A1
公开(公告)日：2010-12-23
申请号：US12850276
申请日：2010-08-04
申请人： Young-Il LEE , Jae-Woo Joung , Byung-Ho Jun , Joon-Rak Choi , Kwi-Jong Lee
发明人： Young-Il LEE , Jae-Woo Joung , Byung-Ho Jun , Joon-Rak Choi , Kwi-Jong Lee
IPC分类号： B22F9/16
CPC分类号： B22F9/24 , B22F2998/00 , Y10S977/896 , B22F1/0018 , B22F3/003
摘要： The present invention relates to an apparatus and a method of manufacturing metal nanoparticles, and more particularly to an apparatus including: a precursor supplying part which supplies a precursor solution of metal nanoparticles; a first heating part which is connected with the precursor supplying part, includes a reactor channel having a diameter of 1 to 50 mm, and is heated to the temperature range where any particle is not produced; a second heating part which is connected with the first heating part, includes a reactor channel having a diameter of 1 to 50 mm, and is heated to the temperature range where particles are produced; and a cooler which is connected with the second heating part and collects and cools metal nanoparticles produced at the second heating part which allows continuous mass production of metal nanoparticles.
摘要翻译：本发明涉及一种制造金属纳米颗粒的装置和方法，更具体地涉及一种装置，包括：提供金属纳米颗粒的前体溶液的前体供应部分; 与前体供给部连接的第一加热部包括直径为1〜50mm的反应器通道，并被加热到不产生任何粒子的温度范围; 与第一加热部连接的第二加热部包括直径为1〜50mm的反应器通道，并被加热到制造粒子的温度范围; 以及冷却器，其与第二加热部件连接并且收集和冷却在第二加热部件处产生的金属纳米颗粒，其允许连续大量生产金属纳米颗粒。

10. 发明申请

US20100282022A1 Method for manufaturing copper-based nanoparticles 有权
标题翻译：铜基纳米粒子的制备方法
公开(公告)号：US20100282022A1
公开(公告)日：2010-11-11
申请号：US11987162
申请日：2007-11-28
申请人： Byung-Ho Jun , Jae-Woo Joung , Joon-Rak Choi
发明人： Byung-Ho Jun , Jae-Woo Joung , Joon-Rak Choi
IPC分类号： B22F9/18
CPC分类号： C01G3/02 , B22F9/20 , B22F2998/00 , B82Y30/00 , C01P2004/04 , C01P2004/64 , Y10S977/896 , B22F2301/10
摘要： The present invention relates to a method for manufacturing copper-based nanoparticles, in particular, to a method for manufacturing copper-based nanoparticles, wherein the method includes producing CuO nanoparticles by mixing CuO micropowder and alkylamine in a nonpolar solvent and heating the mixture at 60-300° C.; and producing copper-based nanoparticles by mixing a capping molecule and a reducing agent with the CuO nanoparticles and heating the mixture at 60-120° C.According to the present invention, copper-based nanoparticles can be synthesized using CuO, but not requiring any inorganic reducing agent, in a high yield and a high concentration, so that it allows mass production and easy controlling to desired oxidation number of nanoparticles.
摘要翻译：本发明涉及一种铜基纳米粒子的制造方法，特别涉及一种铜基纳米粒子的制造方法，其特征在于，该方法包括通过将CuO微粉末和烷基胺混合在非极性溶剂中并在60℃加热混合物来制备CuO纳米粒子 -300°C。并通过将封端分子和还原剂与CuO纳米颗粒混合并在60-120℃下加热混合物来生产铜基纳米颗粒。根据本发明，可以使用CuO合成铜基纳米颗粒，但不需要任何无机还原剂，以高产率和高浓度，使得其允许批量生产并容易控制纳米颗粒的所需氧化数。

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