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1. 发明授权

US3936437A Monoazo compounds derived from 2-hydroxymethyl-amino benzoic acids and 2,6-dihydroxypyridines 失效
标题翻译：衍生自2-羟甲基 - 氨基苯甲酸和2,6-二羟基吡啶的单偶氮化合物
公开(公告)号：US3936437A
公开(公告)日：1976-02-03
申请号：US425278
申请日：1973-12-17
申请人： Brian Ribbons Fishwick , Colin William Greenhalgh , Nigel Hughes
发明人： Brian Ribbons Fishwick , Colin William Greenhalgh , Nigel Hughes
IPC分类号： C07D213/69 , C07D213/77 , C07D213/80 , C07D213/82 , C07D213/85 , C09B29/42 , C09B29/36
CPC分类号： C07D213/69 , C07D213/77 , C07D213/80 , C07D213/82 , C07D213/85 , C09B29/3626
摘要： The disperse monoazo dyestuffs, free from sulphonic acid groups, which are represented by the formula: ##SPC1##Wherein X is alkyl, substituted alkyl, phenyl or optionally substituted carbamoyl; Y is a hydrogen atom or a substituent; and Z is a hydrogen atom or an optionally substituted alkyl, cycloalkyl, aryl or heterocyclic radical or an optionally substituted amino group, a process for the manufacture of the said dyestuffs and their use for coloring synthetic textile materials.
摘要翻译：不含磺酸基团的分散单偶氮染料，由下式表示：

2. 发明授权

US4030881A Coloration process 失效
标题翻译：着色过程
公开(公告)号：US4030881A
公开(公告)日：1977-06-21
申请号：US620694
申请日：1975-10-08
申请人： Violet Boyd , Brian Ribbons Fishwick , Brian Glover
发明人： Violet Boyd , Brian Ribbons Fishwick , Brian Glover
IPC分类号： D06P1/16 , C09B29/42 , D06P3/48 , D06P3/54 , D06P3/85 , D06P5/02 , D06P5/10 , C09B1/00 , C09B5/62
CPC分类号： D06P5/10 , C09B29/363 , D06P3/48 , D06P3/54 , Y10S8/921 , Y10S8/922
摘要： Process for the coloration of aromatic polyester or cellulose triacetate textile materials which comprises applying to the said textile material by an aqueous dyeing, padding or printing process a disperse dyestuff which contains at least two carboxylic acid ester groups and subsequently giving the colored textile material a treatment in an aqueous solution of an alkali having a pH above 8 and at a temperature between 50.degree. and 85.degree. C, whereby the textile materials are colored in a wide variety of shades possessing very good to excellent fastness properties.
摘要翻译：用于着色芳族聚酯或三醋酸纤维素纺织材料的方法，其包括通过水性染色，填充或印刷方法施加到所述纺织材料上的分散染料，所述分散染料含有至少两个羧酸酯基团，并随后将着色纺织材料给予处理在pH高于8且温度在50至85℃之间的碱的水溶液中，由此纺织材料以各种各样的色调着色，具有非常好至优异的牢度性能。

3. 发明授权

US4111956A Process for the manufacture of heterocyclic compounds 失效
标题翻译：制备杂环化合物的方法
公开(公告)号：US4111956A
公开(公告)日：1978-09-05
申请号：US764457
申请日：1977-01-31
申请人： David Boyd Baird , James Stanley Campbell , Brian Ribbons Fishwick , Robert David McClelland
发明人： David Boyd Baird , James Stanley Campbell , Brian Ribbons Fishwick , Robert David McClelland
IPC分类号： C07D333/38 , C07D333/44 , C07D333/36
CPC分类号： C07D333/38 , C07D333/44
摘要： Process for manufacture of the heterocyclic compounds of the formula: ##STR1## wherein X is cyano, acyl, alkylsulphonyl, arylsulphonyl, optionally substituted alkoxycarbonyl, nitro, phenyl or sulphamoyl, andY is hydrogen, optionally substituted alkyl or optionally substituted aryl, which comprises reacting a compound of the formula: ##STR2## with an acid halide in the presence of a compound of the formula ##STR3## and optionally in the presence of an aprotic solvent, and subjecting the resulting compound of the formula: ##STR4## or an acid salt thereof, to hydrolysis in acidic medium, wherein Z is hydrogen or an optionally substituted alkyl or aryl radical, and R.sup.2 and R.sup.3 each independently representing optionally substituted alkyl, cycloalkyl or aryl radicals, or R.sup.2 and R.sup.3 together form with the nitrogen atom a 5- or 6-membered nitrogen-containing heterocyclic ring.
摘要翻译：制备下式的杂环化合物的方法：其中X为氰基，酰基，烷基磺酰基，芳基磺酰基，任选取代的烷氧基羰基，硝基，苯基或氨磺酰基，Y为氢，任选取代的烷基或任选取代的芳基，使下式化合物反应：

4. 发明授权

US3993438A Process for coloring aromatic polyester-cellulose unions with a reactive dyestuff and a disperse dyestuff containing at least two carboxylic acid ester groups 失效
标题翻译：用活性染料和含有至少两个羧酸酯基的分散染料着色芳族聚酯 - 纤维素结合剂的方法
公开(公告)号：US3993438A
公开(公告)日：1976-11-23
申请号：US564899
申请日：1975-04-03
申请人： Brian Ribbons Fishwick , Violet Boyd , Brian Glover
发明人： Brian Ribbons Fishwick , Violet Boyd , Brian Glover
IPC分类号： C09B29/085 , C09B1/26 , C09B29/08 , C09B62/00 , C09B69/00 , D06P1/18 , D06P3/66 , D06P3/82 , D06P3/872 , D06P5/02
CPC分类号： D06P1/18 , C09B1/26 , C09B29/08 , C09B29/0816 , C09B62/00 , C09B69/00 , D06P3/66 , D06P3/8252 , Y10S8/922 , Y10S8/933 , Y10S8/937
摘要： An improved process for the continuous coloration of aromatic polyester/cellulose unions which comprises continuously applying to the said unions a reactive dyestuff and a disperse dyestuff containing at least two carboxylic acid ester groups, fixing the dyestuffs on the union, and thereafter subjecting the colored union to a treatment in an aqueous alkaline bath at a pH above 8.0 and at a temperature between 50.degree. and 85.degree. C, whereby the unions are padded or printed in a wide variety of shades possessing excellent fastness properties and there is little or no staining of any unprinted areas of the unions.
摘要翻译：一种用于连续着色芳族聚酯/纤维素接头的改进方法，其包括连续地向所述接合体施加活性染料和含有至少两个羧酸酯基团的分散染料，将染料固定在接头上，然后使着色接合体在pH 8.0以上，温度在50℃〜85℃之间的碱性水溶液中进行处理，由此将各种各样的色调填充或印刷，具有优异的牢固性，并且几乎没有染色任何未印刷的工会区域。

5. 发明授权

US4108867A 2-Aminothiophenes 失效
标题翻译： 2-氨基噻吩
公开(公告)号：US4108867A
公开(公告)日：1978-08-22
申请号：US466059
申请日：1974-05-01
申请人： David Boyd Baird , Alan Thomas Costello , Brian Ribbons Fishwick , Robert David McClelland , Peter Smith
发明人： David Boyd Baird , Alan Thomas Costello , Brian Ribbons Fishwick , Robert David McClelland , Peter Smith
IPC分类号： C07D333/36 , C07D333/38 , C07D333/44 , C09B29/00 , C09B29/06 , C09B29/08 , C09B29/36 , C07D333/24 , A01N9/00 , C09B27/00
CPC分类号： C09B29/3695 , C07D333/36 , C07D333/38 , C07D333/44 , C09B29/0059 , C09B29/06 , C09B29/08
摘要： The compounds of the formula ##STR1## wherein X is a lower alkylsulphonyl, phenylsulphonyl, cyano, carbonamido, carboxylic acid or carboxylic acid ester group;Y is hydrogen, lower alkyl, phenyl or nitrophenyl; andZ is nitro, cyano or carbonamido.
摘要翻译：其中X为低级烷基磺酰基，苯基磺酰基，氰基，碳酰氨基，羧酸或羧酸酯基团的式（Ⅰ）化合物; Y是氢，低级烷基，苯基或硝基苯基; Z为硝基，氰基或碳酰氨基。

6. 发明授权

US3992410A Process for manufacturing thiophene derivatives 失效
标题翻译：制造噻吩衍生物的方法
公开(公告)号：US3992410A
公开(公告)日：1976-11-16
申请号：US583764
申请日：1975-06-04
申请人： David Boyd Baird , Brian Ribbons Fishwick , Ian Knowles Barben , John Murray Holland, deceased
发明人： David Boyd Baird , Brian Ribbons Fishwick , Ian Knowles Barben , John Murray Holland, deceased
IPC分类号： C07D333/36 , C07D333/66 , C07D333/72 , C07D333/78 , C07D409/04 , C07D333/00
CPC分类号： C07D333/66 , C07D333/36 , C07D333/72 , C07D333/78
摘要： Process for the manufacture of salts of 2-aminothiophenes having the formula: ##SPC1##Wherein R, X and Y are each independently a hydrogen atom, an alkyl radical or an optionally substituted aryl radical, or a thienyl or furyl radical or either R and X or X and Y together form a chain or methylene groups to form a 5- or 6- membered fused ring system, which comprises treating the corresponding compound of the formula: ##EQU1## with hydrogen sulphide in the presence of an acid and in the presence of an organic solvent, and the use of the said salts as diazo components in the manufacture of azo dyestuffs.
摘要翻译：制备具有下式的2-氨基噻吩盐的方法：

7. 发明授权

US3935232A Process for manufacturing heterocyclic compounds 失效
标题翻译：制备杂环化合物的方法
公开(公告)号：US3935232A
公开(公告)日：1976-01-27
申请号：US514319
申请日：1974-10-11
申请人： David Boyd Baird , Ronald Baker , Brian Ribbons Fishwick , Robert David McClelland
发明人： David Boyd Baird , Ronald Baker , Brian Ribbons Fishwick , Robert David McClelland
IPC分类号： C07D333/24
摘要： A process for the manufacture of the heterocyclic compounds of the formula: ##SPC1##Wherein R is a hydrogen atom or a hydrocarbon radical, which comprises decarboxylating and dinitrating a compound of the formula: ##SPC2##Wherein R has the meaning stated above, and finally hydrolysing off the acyl group, and the use of the said heterocyclic compounds as diazo components in the production of azo dyestuffs.
摘要翻译：制备下式杂环化合物的方法：

8. 发明授权

US4119624A Disperse monoazo dyestuffs 失效
标题翻译：分散单偶氮染料
公开(公告)号：US4119624A
公开(公告)日：1978-10-10
申请号：US567404
申请日：1975-04-11
申请人： Violet Boyd , Brian Ribbons Fishwick , David John Watson
发明人： Violet Boyd , Brian Ribbons Fishwick , David John Watson
IPC分类号： C09B29/08
摘要： The disperse monoazo dyestuffs of the formula:- ##STR1## wherein U is hydrogen, chlorine, bromine, cyano, lower alkyl, lower alkoxy or a group of the formula --CONT.sup.1 T.sup.2, --COOT.sup.3 or --SO.sub.2 T.sup.3 ;V is hydrogen, chlorine, bromine, cyano or lower alkoxycarbonyl;W is hydrogen, cyano, nitro, thiocyano, chlorine, bromine or a group of the formula --SO.sub.2 NT.sup.1 T.sup.2, --COOT.sup.3 or --SO.sub.2 T.sup.3 ;Q is hydrogen, chlorine, bromine, lower alkoxy or a --COOT.sup.3 group;R is cyano lower alkyl;A and A.sup.1 each independently represent a lower alkylene radical;X is cyano, lower alkoxy, lower alkoxy lower alkoxy, lower alkoxy lower alkoxy lower alkoxy, chlorine, bromine, lower alkoxycarbonyl, lower alkylcarbonyl, optionally substituted phenoxy carbonyl or optionally substituted phenoxy;Y is lower alkoxycarbonyl, lower alkylcarbonyl, optionally substituted phenylcarbonyl, optionally substituted phenoxycarbonyl, phenyl lower alkoxycarbonyl, lower alkylsulphonyl, optionally substituted phenylsulphonyl or N-optionally substituted aminocarbonyl;T.sup.1 is hydrogen or alkyl;T.sup.2 is hydrogen, alkyl, phenyl, phenylalkyl or cycloalkyl; and T.sup.3 is alkyl, phenyl, phenylalkyl or cycloalkyl, a process for the manufacture of the said dyestuffs and their use for coloring synthetic textile materials. The said dyestuffs have excellent build-up properties on polyester textile material so that heavy depths of shade can be readily obtained and the resulting colorations have excellent fastness to light, to wet treatments and to dry heat treatments.
摘要翻译：其中U是氢，氯，溴，氰基，低级烷基，低级烷氧基或式-CONT1T2，-COOT3或-SO2T3的基团的下式的分散单偶氮染料： V是氢，氯，溴，氰基或低级烷氧基羰基; W是氢，氰基，硝基，硫氰基，氯，溴或式-SO2NT1T2，-COOT3或-SO2T3的基团; Q是氢，氯，溴，低级烷氧基或-COOT3基团; R为氰基低级烷基; A和A1各自独立地表示低级亚烷基; X为氰基，低级烷氧基，低级烷氧基低级烷氧基，低级烷氧基低级烷氧基低级烷氧基，氯，溴，低级烷氧基羰基，低级烷基羰基，任意取代的苯氧基羰基或任意取代的苯氧基; Y是低级烷氧基羰基，低级烷基羰基，任选取代的苯基羰基，任意取代的苯氧基羰基，苯基低级烷氧基羰基，低级烷基磺酰基，任选取代的苯基磺酰基或N-任选取代的氨基羰基; T1是氢或烷基; T 2是氢，烷基，苯基，苯基烷基或环烷基; 并且T3是烷基，苯基，苯基烷基或环烷基，制备所述染料的方法及其用于着色合成纺织材料的用途。所述染料在聚酯纺织材料上具有优异的聚集性能，因此可以容易地获得很深的色调，并且所得到的着色具有优异的耐光牢度，湿法处理和干热处理。

9. 发明授权

US4079050A Disperse monoazo dyestuffs containing a thiophene residue 失效
标题翻译：分散含有噻吩残留物的单偶氮染料
公开(公告)号：US4079050A
公开(公告)日：1978-03-14
申请号：US654170
申请日：1976-02-02
申请人： David Boyd Baird , Alan Thomas Costello , Brian Ribbons Fishwick , Robert David McClelland , Peter Smith
发明人： David Boyd Baird , Alan Thomas Costello , Brian Ribbons Fishwick , Robert David McClelland , Peter Smith
IPC分类号： C07D333/38 , C07D333/44 , C09B29/00 , C09B29/06 , C09B29/08 , C09B29/26
CPC分类号： C07D333/38 , C07D333/44 , C09B29/00 , C09B29/06 , C09B29/0807
摘要： The water-insoluble monoazo dyestuffs, free from sulphonic acid and carboxylic acid groups, which are of the formula: ##STR1## wherein Y is hydrogen, lower alkyl, optionally substituted phenyl or nitro; Z is nitro, cyano, optionally substituted phenyl, optionally substituted lower alkoxycarbonyl or carbonamido; T is hydrogen, optionally substituted lower alkyl or optionally substituted lower alkoxy;W is an acylamino group of the formula: ##STR2## wherein X.sup.1 is hydrogen or lower alkyl, X.sup.2 is hydrogen or an optionally substituted hydrocarbon or heterocyclic radical, and A is a direct link or --0-- or ##STR3## and R.sup.1 and R.sup.2 each independently represent a hydrogen atom or an optionally substituted alkyl radical or R.sup.1 and R.sup.2 together form with the nitrogen atom N a 5- or 6-membered nitrogen-containing heterocyclic ring, a process for the manufacture of the said dyestuffs by diazotization and coupling, and the use of the said dyestuffs for coloring synthetic textile materials, in particular aromatic polyester textile materials which they color in violet to green shades possessing excellent fastness to light, to wet treatments and to dry heat treatments.
摘要翻译：不溶于磺酸和羧酸基的水不溶性单偶氮染料，其具有下式：其中Y为氢，低级烷基，任选取代的苯基或硝基; Z是硝基，氰基，任选取代的苯基，任选取代的低级烷氧基羰基或碳酰氨基; T是氢，任选取代的低级烷基或任选取代的低级烷氧基; W是下式的酰氨基，其中X 1是氢或低级烷基，X 2是氢或任选取代的烃或杂环基，A是直链或-O-或R 1和R 2 各自独立地表示氢原子或任选取代的烷基，或者R 1和R 2与氮原子一起一起形成5-或6-元含氮杂环，通过重氮化和偶联制备所述染料的方法，以及所述染料用于着色合成纺织材料，特别是紫色的芳族聚酯纺织材料，具有优异的耐光牢度的绿色色调，湿法处理和干热处理。

10. 发明授权

US4029469A Coloring process for synthetic textile materials 失效
标题翻译：合成纺织材料着色工艺
公开(公告)号：US4029469A
公开(公告)日：1977-06-14
申请号：US620692
申请日：1975-10-08
申请人： Violet Boyd , Brian Ribbons Fishwick , Brian Glover
发明人： Violet Boyd , Brian Ribbons Fishwick , Brian Glover
IPC分类号： C09B29/085 , C09B29/08 , C09B29/42 , D06P3/48 , D06P3/54 , D06P5/10 , C09B27/00 , D06P1/02
CPC分类号： D06P5/10 , C09B29/08 , C09B29/0817 , C09B29/363 , D06P3/48 , D06P3/54 , Y10S8/922
摘要： Process for coloring aromatic polyester textile materials which comprises applying to the said textile material by an aqueous dyeing, padding or printing process an aqueous dispersion of a water-insoluble monoazo dyestuff of the formula:- ##STR1## wherein X is hydrogen or methyl, Y and Z are each independently chlorine or bromine, and R is lower alkyl, and subsequently subjecting the colored textile material to a treatment in an aqueous solution of sodium hydrosulphite whereby the aromatic polyester textile materials are colored in brown shades of excellent fastness properties.
摘要翻译：用于着色芳族聚酯纺织材料的方法，其包括通过水性染色，填充或印刷方法将所述纺织材料施用于下式的水不溶性单偶氮染料的水分散体：其中X是氢或甲基，Y 和Z各自独立地为氯或溴，R为低级烷基，随后将着色纺织品进行在亚硫酸氢钠水溶液中的处理，由此使芳族聚酯纺织品以具有优异坚牢性的棕色色调着色。

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