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1. 发明申请

US20120329096A1 RECOVERY OF INORGANIC SALT DURING PROCESSING OF LIGNOCELLULOSIC FEEDSTOCKS 有权
标题翻译：无机盐处理过程中无机盐的回收
公开(公告)号：US20120329096A1
公开(公告)日：2012-12-27
申请号：US13569308
申请日：2012-08-08
申请人： Brian Foody , Jeffrey S. Tolan , Ziyad Rahme , Vijay Anand
发明人： Brian Foody , Jeffrey S. Tolan , Ziyad Rahme , Vijay Anand
IPC分类号： C12P7/10 , C12P19/00
CPC分类号： B01D61/147 , B01B1/005 , B01D15/1821 , B01D15/365 , B01D61/44 , C01C1/28 , C01D3/04 , C01D5/04 , C01D5/16 , C05B7/00 , C05C3/00 , C05D1/00 , C05D1/02 , C05D5/00 , C05F11/00 , C12P3/00 , C12P7/06 , C12P7/10 , C12P19/02 , C12P2201/00 , Y02E50/16 , Y02E50/17
摘要： A method for recovering inorganic salt during processing of a lignocellulosic feedstock is provided. The method comprises pretreating the lignocellulosic feedstock by adding an acid to the feedstock to produce a pretreated lignocellulosic feedstock. A soluble base is then added to the pretreated lignocellulosic feedstock to adjust the pH and produce a neutralized feedstock. The neutralized feedstock is then enzymatically hydrolyzed to produce an enzyme hydrolyzed feedstock and a sugar stream. Inorganic salt is recovered from either a stream obtained from the lignocellulosic feedstock prior to the step of pretreating, a stream obtained from the pretreated lignocellulosic feedstock, a stream obtained from the neutralized feedstock, a stream obtained from the sugar stream, or a combination of these streams. The inorganic salt may be concentrated, clarified, recovered and purified by crystallization, electrodialysis drying, or agglomeration and granulation, and then used as desired, for example as a fertilizer.
摘要翻译：提供了在木质纤维素原料的加工过程中回收无机盐的方法。该方法包括通过向原料中加入酸来预处理木质纤维素原料以产生预处理的木质纤维素原料。然后将可溶碱添加到预处理的木质纤维素原料中以调节pH并产生中和的原料。然后将中和的原料酶水解以产生酶水解原料和糖流。在预处理步骤之前从木质纤维素原料获得的物流中回收无机盐，从预处理的木质纤维素原料获得的物流，从中和原料获得的物流，从糖流获得的物流，或这些物质的组合流。无机盐可以通过结晶，电渗析干燥或附聚和造粒进行浓缩，澄清，回收和纯化，然后根据需要使用，例如作为肥料。

2. 发明申请

US20100221819A1 UPFLOW HYDROLYSIS REACTOR SYSTEM FOR HYDROLYZING CELLULOSE 审中-公开
标题翻译：用于水解纤维素的UPFLOW水解反应器系统
公开(公告)号：US20100221819A1
公开(公告)日：2010-09-02
申请号：US12762589
申请日：2010-04-19
申请人： Brian Foody , Ziyad Rahme , Jeffrey S. Tolan
发明人： Brian Foody , Ziyad Rahme , Jeffrey S. Tolan
IPC分类号： C12M1/00
CPC分类号： C12P19/14 , C12M45/09 , C12P19/02 , C12P19/04 , Y02E50/16 , Y02E50/17
摘要： A process for the enzymatic hydrolysis of cellulose to produce a hydrolysis product from a pre-treated cellulosic feedstock is provided. The process comprises introducing an aqueous slurry of the pre-treated cellulosic feedstock at the bottom of a hydrolysis reactor. Axial dispersion in the reactor is limited by avoiding mixing and maintaining an average slurry flow velocity of about 0.1 to about 20 feet per hour, such that the undissolved solids flow upward at a rate slower than that of the liquid. Cellulase enzymes are added to the aqueous slurry before or during the step of introducing. An aqueous stream comprising hydrolysis product and unhydrolyzed solids is removed from the hydrolysis reactor. Also provided are enzyme compositions which comprise cellulase enzymes and flocculents for use in the process. In addition, a kit comprising cellulase enzymes and flocculent is provided.
摘要翻译：提供了一种纤维素酶水解从预处理的纤维素原料产生水解产物的方法。该方法包括在水解反应器的底部引入预处理的纤维素原料的含水浆料。通过避免混合并保持约0.1至约20英尺/小时的平均浆料流速，使得未溶解的固体以比液体慢的速率向上流动，来限制反应器中的轴向分散。在引入步骤之前或期间，将纤维素酶加入到含水浆料中。从水解反应器中除去包含水解产物和未水解固体的水流。还提供了包含用于该方法的纤维素酶和絮凝剂的酶组合物。另外，提供了包含纤维素酶和絮状物的试剂盒。

3. 发明申请

US20080102502A1 Inorganic salt recovery during processing of lignocellulosic feedstocks 失效
标题翻译：在木质纤维素原料加工过程中的无机盐回收
公开(公告)号：US20080102502A1
公开(公告)日：2008-05-01
申请号：US11586135
申请日：2006-10-25
申请人： Brian Foody , Jeffrey S. Tolan , Ziyad Rahme , Vijay Anand
发明人： Brian Foody , Jeffrey S. Tolan , Ziyad Rahme , Vijay Anand
IPC分类号： C12P7/06
CPC分类号： C12P19/02 , C08H8/00 , C12P7/10 , Y02E50/16 , Y02E50/17
摘要： A method for recovering inorganic salt during processing of a lignocellulosic feedstock is provided. The method comprises pretreating the lignocellulosic feedstock by adding an acid or a base to the feedstock to produce a pretreated lignocellulosic feedstock. A soluble base or acid is then added to the pretreated lignocellulosic feedstock to adjust the pH and produce a neutralized feedstock. The neutralized feedstock is then hydrolyzed to produce an hydrolyzed feedstock and a sugar stream. Inorganic salt is recovered from a wash stream obtained from the pretreated lignocellulosic feedstock, a stream obtained from the neutralized feedstock, a stream obtained from the sugar stream, or a combination of these streams. The inorganic salt may be concentrated, clarified, recovered and purified by crystallization, electrodialysis, drying, or agglomeration and granulation, and then used as desired, for example, as a fertilizer.
摘要翻译：提供了在木质纤维素原料的加工过程中回收无机盐的方法。该方法包括通过向原料中加入酸或碱来预处理木质纤维素原料以产生预处理的木质纤维素原料。然后将可溶性碱或酸加入到预处理的木质纤维素原料中以调节pH并产生中和的原料。然后将中和的原料水解以产生水解原料和糖流。从由预处理的木质纤维素原料获得的洗涤流，从中和的原料获得的物流，从糖流获得的物流或这些物流的组合从无机盐中回收无机盐。无机盐可以通过结晶，电渗析，干燥或附聚和造粒浓缩，澄清，回收和纯化，然后根据需要例如作为肥料使用。

4. 发明授权

US08911979B2 Recovery of inorganic salt during processing of lignocellulosic feedstocks 有权
标题翻译：在木质纤维素原料加工过程中回收无机盐
公开(公告)号：US08911979B2
公开(公告)日：2014-12-16
申请号：US13569308
申请日：2012-08-08
申请人： Brian Foody , Jeffrey S. Tolan , Ziyad Rahme , Vijay Anand
发明人： Brian Foody , Jeffrey S. Tolan , Ziyad Rahme , Vijay Anand
IPC分类号： C12P7/08 , C12P7/12 , C13K1/02 , C13K1/06 , B01D61/14 , B01B1/00 , B01D15/18 , B01D15/36 , B01D61/44 , C05B7/00 , C05C3/00 , C05D1/00 , C05D1/02 , C05D5/00 , C05F11/00 , C12P3/00 , C12P7/06 , C12P7/10 , C12P19/02
CPC分类号： B01D61/147 , B01B1/005 , B01D15/1821 , B01D15/365 , B01D61/44 , C01C1/28 , C01D3/04 , C01D5/04 , C01D5/16 , C05B7/00 , C05C3/00 , C05D1/00 , C05D1/02 , C05D5/00 , C05F11/00 , C12P3/00 , C12P7/06 , C12P7/10 , C12P19/02 , C12P2201/00 , Y02E50/16 , Y02E50/17
摘要： A method for recovering inorganic salt during processing of a lignocellulosic feedstock is provided. The method comprises pretreating the lignocellulosic feedstock by adding an acid to the feedstock to produce a pretreated lignocellulosic feedstock. A soluble base is then added to the pretreated lignocellulosic feedstock to adjust the pH and produce a neutralized feedstock. The neutralized feedstock is then enzymatically hydrolyzed to produce an enzyme hydrolyzed feedstock and a sugar stream. Inorganic salt is recovered from either a stream obtained from the lignocellulosic feedstock prior to the step of pretreating, a stream obtained from the pretreated lignocellulosic feedstock, a stream obtained from the neutralized feedstock, a stream obtained from the sugar stream, or a combination of these streams. The inorganic salt may be concentrated, clarified, recovered and purified by crystallization, electrodialysis drying, or agglomeration and granulation, and then used as desired, for example as a fertilizer.
摘要翻译：提供了在木质纤维素原料的加工过程中回收无机盐的方法。该方法包括通过向原料中加入酸来预处理木质纤维素原料以产生预处理的木质纤维素原料。然后将可溶碱添加到预处理的木质纤维素原料中以调节pH并产生中和的原料。然后将中和的原料酶水解以产生酶水解原料和糖流。在预处理步骤之前从木质纤维素原料获得的物流中回收无机盐，从预处理的木质纤维素原料获得的物流，从中和原料获得的物流，从糖流获得的物流，或这些物质的组合流。无机盐可以通过结晶，电渗析干燥或附聚和造粒进行浓缩，澄清，回收和纯化，然后根据需要使用，例如作为肥料。

5. 发明授权

US08247203B2 Recovery of inorganic salt during processing of lignocellulosic feedstocks 有权
标题翻译：在木质纤维素原料加工过程中回收无机盐
公开(公告)号：US08247203B2
公开(公告)日：2012-08-21
申请号：US12539645
申请日：2009-08-12
申请人： Brian Foody , Jeffrey S. Tolan , Ziyad Rahme , Vijay Anand
发明人： Brian Foody , Jeffrey S. Tolan , Ziyad Rahme , Vijay Anand
IPC分类号： C12P7/08 , C12P7/12 , C13K1/02 , C13K1/06
CPC分类号： B01D61/147 , B01B1/005 , B01D15/1821 , B01D15/365 , B01D61/44 , C01C1/28 , C01D3/04 , C01D5/04 , C01D5/16 , C05B7/00 , C05C3/00 , C05D1/00 , C05D1/02 , C05D5/00 , C05F11/00 , C12P3/00 , C12P7/06 , C12P7/10 , C12P19/02 , C12P2201/00 , Y02E50/16 , Y02E50/17
摘要： A method for recovering inorganic salt during processing of a lignocellulosic feedstock is provided. The method comprises pretreating the lignocellulosic feedstock by adding an acid to the feedstock to produce a pretreated lignocellulosic feedstock. A soluble base is then added to the pretreated lignocellulosic feedstock to adjust the pH and produce a neutralized feedstock. The neutralized feedstock is then enzymatically hydrolyzed to produce an enzyme hydrolyzed feedstock and a sugar stream. Inorganic salt is recovered from either a stream obtained from the lignocellulosic feedstock prior to the step of pretreating, a stream obtained from the pretreated lignocellulosic feedstock, a stream obtained from the neutralized feedstock, a stream obtained from the sugar stream, or a combination of these streams. The inorganic salt may be concentrated, clarified, recovered and purified by crystallization, electrodialysis drying, or agglomeration and granulation, and then used as desired, for example as a fertilizer.
摘要翻译：提供了在木质纤维素原料的加工过程中回收无机盐的方法。该方法包括通过向原料中加入酸来预处理木质纤维素原料以产生预处理的木质纤维素原料。然后将可溶碱添加到预处理的木质纤维素原料中以调节pH并产生中和的原料。然后将中和的原料酶水解以产生酶水解原料和糖流。在预处理步骤之前从木质纤维素原料获得的物流中回收无机盐，从预处理的木质纤维素原料获得的物流，从中和原料获得的物流，从糖流获得的物流，或这些物质的组合流。无机盐可以通过结晶，电渗析干燥或团聚和造粒进行浓缩，澄清，回收和纯化，然后根据需要使用，例如作为肥料。

6. 发明授权

US07727746B2 Upflow reactor for enzymatic hydrolysis of cellulose 失效
标题翻译：用于纤维素酶水解的上流式反应器
公开(公告)号：US07727746B2
公开(公告)日：2010-06-01
申请号：US11303424
申请日：2005-12-16
申请人： Brian Foody , Ziyad Rahme , Jeffrey S. Tolan
发明人： Brian Foody , Ziyad Rahme , Jeffrey S. Tolan
IPC分类号： C12P19/14
CPC分类号： C12P19/14 , C12M45/09 , C12P19/02 , C12P19/04 , Y02E50/16 , Y02E50/17
摘要： A process for the enzymatic hydrolysis of cellulose to produce a hydrolysis product from a pre-treated cellulosic feedstock is provided. The process comprises introducing an aqueous slurry of the pre-treated cellulosic feedstock at the bottom of a hydrolysis reactor. Axial dispersion in the reactor is limited by avoiding mixing and maintaining an average slurry flow velocity of about 0.1 to about 20 feet per hour, such that the undissolved solids flow upward at a rate slower than that of the liquid. Cellulase enzymes are added to the aqueous slurry before or during the step of introducing. An aqueous stream comprising hydrolysis product and unhydrolyzed solids is removed from the hydrolysis reactor. Also provided are enzyme compositions which comprise cellulase enzymes and flocculents for use in the process. In addition, a kit comprising cellulase enzymes and flocculent is provided.
摘要翻译：提供了一种纤维素酶水解从预处理的纤维素原料产生水解产物的方法。该方法包括在水解反应器的底部引入预处理的纤维素原料的含水浆料。通过避免混合并保持约0.1至约20英尺/小时的平均浆料流速，使得未溶解的固体以比液体慢的速率向上流动，来限制反应器中的轴向分散。在引入步骤之前或期间，将纤维素酶加入到含水浆料中。从水解反应器中除去包含水解产物和未水解固体的水流。还提供了包含用于该方法的纤维素酶和絮凝剂的酶组合物。此外，提供了包含纤维素酶和絮状物的试剂盒。

7. 发明授权

US07670813B2 Inorganic salt recovery during processing of lignocellulosic feedstocks 失效
标题翻译：在木质纤维素原料加工过程中的无机盐回收
公开(公告)号：US07670813B2
公开(公告)日：2010-03-02
申请号：US11586135
申请日：2006-10-25
申请人： Brian Foody , Jeffrey S. Tolan , Ziyad Rahme , Vijay Anand
发明人： Brian Foody , Jeffrey S. Tolan , Ziyad Rahme , Vijay Anand
IPC分类号： C12P19/02 , C12P3/00 , C12P7/06 , C12P7/08
CPC分类号： C12P19/02 , C08H8/00 , C12P7/10 , Y02E50/16 , Y02E50/17
摘要： A method for recovering inorganic salt during processing of a lignocellulosic feedstock is provided. The method comprises pretreating the lignocellulosic feedstock by adding an acid or a base to the feedstock to produce a pretreated lignocellulosic feedstock. A soluble base or acid is then added to the pretreated lignocellulosic feedstock to adjust the pH and produce a neutralized feedstock. The neutralized feedstock is then hydrolyzed to produce an hydrolyzed feedstock and a sugar stream. Inorganic salt is recovered from a wash stream obtained from the pretreated lignocellulosic feedstock, a stream obtained from the neutralized feedstock, a stream obtained from the sugar stream, or a combination of these streams. The inorganic salt may be concentrated, clarified, recovered and purified by crystallization, electrodialysis, drying, or agglomeration and granulation, and then used as desired, for example, as a fertilizer.
摘要翻译：提供了在木质纤维素原料的加工过程中回收无机盐的方法。该方法包括通过向原料中加入酸或碱来预处理木质纤维素原料以产生预处理的木质纤维素原料。然后将可溶性碱或酸加入到预处理的木质纤维素原料中以调节pH并产生中和的原料。然后将中和的原料水解以产生水解原料和糖流。从由预处理的木质纤维素原料获得的洗涤流，从中和的原料获得的物流，从糖流获得的物流或这些物流的组合从无机盐中回收无机盐。无机盐可以通过结晶，电渗析，干燥或附聚和造粒浓缩，澄清，回收和纯化，然后根据需要例如作为肥料使用。

8. 发明申请

US20100003733A1 RECOVERY OF INORGANIC SALT DURING PROCESSING OF LIGNOCELLULOSIC FEEDSTOCKS 有权
标题翻译：无机盐处理过程中无机盐的回收
公开(公告)号：US20100003733A1
公开(公告)日：2010-01-07
申请号：US12539645
申请日：2009-08-12
申请人： Brian Foody , Jeffrey S. Tolan , Ziyad Rahme , Vijay Anand
发明人： Brian Foody , Jeffrey S. Tolan , Ziyad Rahme , Vijay Anand
IPC分类号： C12P7/10 , C12P3/00
CPC分类号： B01D61/147 , B01B1/005 , B01D15/1821 , B01D15/365 , B01D61/44 , C01C1/28 , C01D3/04 , C01D5/04 , C01D5/16 , C05B7/00 , C05C3/00 , C05D1/00 , C05D1/02 , C05D5/00 , C05F11/00 , C12P3/00 , C12P7/06 , C12P7/10 , C12P19/02 , C12P2201/00 , Y02E50/16 , Y02E50/17
摘要： A method for recovering inorganic salt during processing of a lignocellulosic feedstock is provided. The method comprises pretreating the lignocellulosic feedstock by adding an acid to the feedstock to produce a pretreated lignocellulosic feedstock. A soluble base is then added to the pretreated lignocellulosic feedstock to adjust the pH and produce a neutralized feedstock. The neutralized feedstock is then enzymatically hydrolyzed to produce an enzyme hydrolyzed feedstock and a sugar stream. Inorganic salt is recovered from either a stream obtained from the lignocellulosic feedstock prior to the step of pretreating, a stream obtained from the pretreated lignocellulosic feedstock, a stream obtained from the neutralized feedstock, a stream obtained from the sugar stream, or a combination of these streams. The inorganic salt may be concentrated, clarified, recovered and purified by crystallization, electrodialysis drying, or agglomeration and granulation, and then used as desired, for example as a fertilizer.
摘要翻译：提供了在木质纤维素原料的加工过程中回收无机盐的方法。该方法包括通过向原料中加入酸来预处理木质纤维素原料以产生预处理的木质纤维素原料。然后将可溶碱添加到预处理的木质纤维素原料中以调节pH并产生中和的原料。然后将中和的原料酶水解以产生酶水解原料和糖流。在预处理步骤之前从木质纤维素原料获得的物流中回收无机盐，从预处理的木质纤维素原料获得的物流，从中和原料获得的物流，从糖流获得的物流，或这些物质的组合流。无机盐可以通过结晶，电渗析干燥或附聚和造粒进行浓缩，澄清，回收和纯化，然后根据需要使用，例如作为肥料。

9. 发明授权

US07585652B2 Recovery of inorganic salt during processing of lignocellulosic feedstocks 有权
标题翻译：在木质纤维素原料加工过程中回收无机盐
公开(公告)号：US07585652B2
公开(公告)日：2009-09-08
申请号：US11104698
申请日：2005-04-13
申请人： Brian Foody , Jeffrey S. Tolan , Ziyad Rahme , Vijay Anand
发明人： Brian Foody , Jeffrey S. Tolan , Ziyad Rahme , Vijay Anand
IPC分类号： C12P7/08 , C12P7/12 , C13K1/02 , C13K1/06
CPC分类号： B01D61/147 , B01B1/005 , B01D15/1821 , B01D15/365 , B01D61/44 , C01C1/28 , C01D3/04 , C01D5/04 , C01D5/16 , C05B7/00 , C05C3/00 , C05D1/00 , C05D1/02 , C05D5/00 , C05F11/00 , C12P3/00 , C12P7/06 , C12P7/10 , C12P19/02 , C12P2201/00 , Y02E50/16 , Y02E50/17
摘要： A method for recovering inorganic salt during processing of a lignocellulosic feedstock is provided. The method comprises pretreating the lignocellulosic feedstock by adding an acid to the feedstock to produce a pretreated lignocellulosic feedstock. A soluble base is then added to the pretreated lignocellulosic feedstock to adjust the pH and produce a neutralized feedstock. The neutralized feedstock is then enzymatically hydrolyzed to produce an enzyme hydrolyzed feedstock and a sugar stream. Inorganic salt is recovered from either a stream obtained from the lignocellulosic feedstock prior to the step of pretreating, a stream obtained from the pretreated lignocellulosic feedstock, a stream obtained from the neutralized feedstock, a stream obtained from the sugar stream, or a combination of these streams. The inorganic salt may be concentrated, clarified, recovered and purified by crystallization, electrodialysis drying, or agglomeration and granulation, and then used as desired, for example as a fertilizer.
摘要翻译：提供了在木质纤维素原料的加工过程中回收无机盐的方法。该方法包括通过向原料中加入酸来预处理木质纤维素原料以产生预处理的木质纤维素原料。然后将可溶碱添加到预处理的木质纤维素原料中以调节pH并产生中和的原料。然后将中和的原料酶水解以产生酶水解原料和糖流。在预处理步骤之前从木质纤维素原料获得的物流中回收无机盐，从预处理的木质纤维素原料获得的物流，从中和原料获得的物流，从糖流获得的物流，或这些物质的组合流。无机盐可以通过结晶，电渗析干燥或附聚和造粒进行浓缩，澄清，回收和纯化，然后根据需要使用，例如作为肥料。

10. 发明授权

US09102951B2 Process for recovering salt during a lignocellulosic conversion process 有权
标题翻译：在木质纤维素转化过程中回收盐的方法
公开(公告)号：US09102951B2
公开(公告)日：2015-08-11
申请号：US14241133
申请日：2012-08-24
申请人： Robert Griffin , Ziyad Rahme , Patricia Dawn MacLean , Brian Foody
发明人： Robert Griffin , Ziyad Rahme , Patricia Dawn MacLean , Brian Foody
IPC分类号： C12P3/00 , F23G5/04 , C05D9/00 , F23G7/10 , C02F9/00 , C02F1/52 , C02F1/04 , D21C11/00 , B01D3/00 , C05F5/00 , F22B1/18 , C12P7/10 , C22B26/22
CPC分类号： C05B9/00 , B01D3/002 , B01D9/00 , C02F1/04 , C02F1/52 , C02F9/00 , C05D9/00 , C05F5/008 , C10L1/1988 , C10L2200/0469 , C10L2250/04 , C10L2290/24 , C10L2290/26 , C10L2290/543 , C12P3/00 , C12P7/10 , C22B26/22 , D21C11/0007 , F22B1/18 , F23G5/04 , F23G7/10 , Y02A40/212 , Y02E50/16 , Y02E50/343 , Y02W30/47
摘要： The present invention relates to a process for generating steam and recovering salts during a lignocellulosic conversion process. The process comprises de-salting a still bottoms stream; incinerating a stream comprising lignin and the de-salted still bottoms stream in an incinerator; and utilizing the heat generated from said incinerating to produce steam. Further provided is a process that comprises feeding a concentrated still bottoms stream to a crystallizer and forming insoluble solids therein comprising salts. Furthermore, the invention relates to a process for recovering salts from a lignocellulosic conversion process, which process comprises the addition of solvent to a still bottoms stream to precipitate salts therefrom. Also provided is a still bottoms composition, a fertilizer product and a composition for incineration.
摘要翻译：本发明涉及在木质纤维素转化过程中产生蒸汽和回收盐的方法。该方法包括对仍然底部物流进行脱盐; 在焚烧炉中焚烧包含木质素和脱盐的塔底流的物流; 并且利用从所述焚化产生的热产生蒸汽。还提供了一种方法，其包括将浓缩的残留物流送入结晶器并在其中形成其中包含盐的不溶性固体。此外，本发明涉及一种从木质纤维素转化方法中回收盐的方法，该方法包括将溶剂加入至塔底馏分料流中以从其中沉淀出盐。还提供了还有底部组合物，肥料产品和用于焚化的组合物。

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