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1. 发明授权

US5512627A Acrylic/lactam resin composition and method of production same 失效
标题翻译：丙烯酸/内酰胺树脂组合物及其生产方法相同
公开(公告)号：US5512627A
公开(公告)日：1996-04-30
申请号：US444606
申请日：1995-05-19
申请人： Bill R. Edwards
发明人： Bill R. Edwards
IPC分类号： C08F220/12 , C08J9/02 , C08K3/00 , C08K3/04 , C08G69/08 , C08G69/14
CPC分类号： C08J9/02 , C08F220/12 , C08K3/0008 , C08J2333/06
摘要： An acrylic/lactam monomer based polymeric resin is provided which has excellent weatherability, outstanding transparency and optical clarity, improved heath and solvent resistance, as well as improved impact strength. The acrylic/lactam monomer based polymeric resin is formulated by the catalytic activation at ambient temperature of a polymerization syrup which contains from about 300 to about 2970 parts by volume of an acrylic monomer, from about 30 to about 2700 parts by volume of a lactam monomer, from about 0.3 parts to about 40 parts by volume of a mercaptan chain transfer agent and from about 0.3 to about 40 parts by volume of a crosslinking agent capable of crosslinking the acrylic monomer and the lactam monomer. To prevent further polymerization of the polymeric constituents of the polymerization syrup, as well as to enhance the shelf life of the polymerization syrup, an effective amount of a polymerization inhibitor and an ultraviolet light stabilizer are incorporated into the polymerization syrup. The crosslinking of the acrylic monomer and the lactam monomer is carried out at ambient temperature and atmospheric pressure.
摘要翻译：提供了一种丙烯酸/内酰胺单体的聚合物树脂，其具有优异的耐候性，优异的透明度和光学透明度，改善的耐磨性和耐溶剂性以及改善的冲击强度。基于丙烯酸/内酰胺单体的聚合物树脂通过聚合糖浆的环境温度下的催化活化来配制，所述聚合糖浆含有约300至约2970体积份的丙烯酸单体，约30至约2700体积份的内酰胺单体，约0.3-约40体积份的硫醇链转移剂和约0.3-约40体积份的能够交联丙烯酸单体和内酰胺单体的交联剂。为了防止聚合糖浆的聚合物成分的进一步聚合，以及提高聚合糖浆的保存期限，将有效量的聚合抑制剂和紫外光稳定剂引入聚合糖浆中。丙烯酸单体和内酰胺单体的交联在环境温度和大气压下进行。

2. 发明授权

US5272230A Acrylic resin composition 失效
公开(公告)号：US5272230A
公开(公告)日：1993-12-21
申请号：US47690
申请日：1993-04-15
申请人： Bill R. Edwards
发明人： Bill R. Edwards
IPC分类号： C08F4/00 , C08F220/12 , C08F265/06
CPC分类号： C08F220/12 , C08F265/06
摘要： An acrylic resin is provided which has excellent weatherability, outstanding transparency and improved heat and solvent resistance, as well as improved impact strength. The acrylic resin comprises an intimate blend of a polymerization syrup and a catalytic amount of a polymerization catalyst capable of effecting polymerization of the syrup. The polymerization syrup, which has an improved shelf life and can be stored at ambient temperature and atmospheric pressure, consists essentially of:(a) from about 300 to about 1000 parts per volume of an acrylic monomer represented by the formula ##STR1## wherein R is an alkyl moiety containing 1 to about 18 carbon atoms; (b) from about 0.1 to about 1000 parts by volume of a non-peroxide oxygen donator, such as 2,2-bis(allyloxymethyl)-butan-1-ol or diallylphthalate;(c) from about 0.5 to about 5 parts by volume of a mercaptan; and(d) from about 0.3 to about 40 parts by volume of a crosslinking agent compatible with the acrylic monomer.The polymerization syrup can further contain from about 0.25 to about 100 parts by volume of a hydroxyalkyl methacrylate and from about 1 to about 100 parts by volume of a polycarbonate compound.

3. 发明授权

US5045613A Acrylic resin composition 失效
标题翻译：丙烯酸树脂组合物
公开(公告)号：US5045613A
公开(公告)日：1991-09-03
申请号：US568194
申请日：1990-08-15
申请人： Bill R. Edwards
发明人： Bill R. Edwards
IPC分类号： C08F220/12 , C08F265/06
CPC分类号： C08F220/12 , C08F265/06
摘要： An acrylic resin is provided which has excellent weatherability, outstanding transparency and improved heat and solvent resistance, as well as improved impact strength. The acrylic resin comprises an intimate blend of a polymerization syrup and a catalytic amount of a polymerization catalyst capable of effecting polymerization of the syrup. The polymerization syrup, which has an improved shelf life and can be stored at ambient temperature and atmospheric pressure, consists essentially of:(a) from about 300 to about 1000 parts per volume of an acrylic monomer represented by the formula ##STR1## wherein R is an alkyl moiety containing 1 to about 18 carbon atoms; (b) from about 0.1 to about 1 part by volume of diallylphthalate;(c) from about 0.5 to about 5 parts by volume of mercaptan; and(d) from about 0.3 to about 40 parts by volume of a crosslinking agent compatible with the acrylic monomer.The polymerization syrup can further contain from about 1 to about 100 parts by volume of a polycarbonate compound.
摘要翻译：提供了具有优异的耐候性，优异的透明性和改善的耐热和耐溶剂性以及改善的冲击强度的丙烯酸树脂。丙烯酸树脂包括聚合糖浆和催化量的能够实现糖浆聚合的聚合催化剂的紧密共混物。具有改善的保质期并且可以在环境温度和大气压下储存的聚合糖浆基本上由以下组成：（a）约300至约1000份/体积的由式“IMAGE”表示的丙烯酸单体，其中R 是含有1至约18个碳原子的烷基部分; （b）约0.1至约1份（体积）邻苯二甲酸二烯丙酯; （c）约0.5至约5体积份的硫醇; 和（d）约0.3至约40体积份的与丙烯酸类单体相容的交联剂。聚合糖浆还可含有约1至约100体积份的聚碳酸酯化合物。

4. 发明授权

US5508339A Acrylic/lactam resin compositions and method of producing same 失效
公开(公告)号：US5508339A
公开(公告)日：1996-04-16
申请号：US445326
申请日：1995-05-19
申请人： Bill R. Edwards
发明人： Bill R. Edwards
IPC分类号： C08F220/12 , C08J9/02 , C08K3/00 , C08G69/08 , C08G69/14
CPC分类号： C08J9/02 , C08F220/12 , C08K3/0008 , C08J2333/06
摘要： An acrylic/lactam monomer based polymeric resin is provided which has excellent weatherability, outstanding transparency and optical clarity, improved heath and solvent resistance, as well as improved impact strength. The acrylic/lactam monomer based polymeric resin is formulated by the catalytic activation at ambient temperature of a polymerization syrup which contains from about 300 to about 2970 parts by volume of an acrylic monomer, from about 30 to about 2700 parts by volume of a lactam monomer, from about 0.3 parts to about 40 parts by volume of a mercaptan chain transfer agent and from about 0.3 to about 40 parts by volume of a crosslinking agent capable of crosslinking the acrylic monomer and the lactam monomer. To prevent further polymerization of the polymeric constituents of the polymerization syrup, as well as to enhance the shelf life of the polymerization syrup, an effective amount of a polymerization inhibitor and an ultraviolet light stabilizer are incorporated into the polymerization syrup. The crosslinking of the acrylic monomer and the lactam monomer is carried out at ambient temperature and atmospheric pressure.

5. 发明授权

US5073587A Polymeric composition and method of producing same 失效
标题翻译：聚合物组合物及其制备方法
公开(公告)号：US5073587A
公开(公告)日：1991-12-17
申请号：US464945
申请日：1990-01-16
申请人： Bill R. Edwards
发明人： Bill R. Edwards
IPC分类号： C08F2/44 , C08K3/00
CPC分类号： C08F2/44 , C08K3/0033
摘要： An acrylic-based particulate filled polymeric composition is provided which is curable at atmospheric pressure and ambient temperature and has a pour to pull time of less than about 4 hours. The acrylic-based particulate filled polymeric composition comprises an intimate blend of a polymerization syrup, a filler, and minor effective amount of crosslinking agent, a polymerization catalyst, a quaternary compound and a polymerization initiator. To enhance and reduce the pour to pull time of articles molded or cast from the acrylic-based particular filled polymeric composition, an effective miner amount of a reaction modifier, such as trimethylpropane triacrylate, can be incorporated into the polymeric composition. The polymerization syrup employed in formulating an acrylic-based particulate filled polymeric composition consist essentially of from about 300 to about 1,000 parts by volume of an acrylic monomer, from about 0.01 to about 1 part by volume of peroxide-free oxygen donator, from about 0.5 to about 5 parts by volume of a mercaptan, and from about 0.3 to about 40 parts by volume of a crosslinking agent compatible with the acrylic monomer.
摘要翻译：提供了一种基于丙烯酸的颗粒填充的聚合物组合物，其在大气压和环境温度下是可固化的，并且具有少于约4小时的倾倒时间。基于丙烯酸的颗粒填充的聚合物组合物包含聚合糖浆，填料和少量有效量的交联剂，聚合催化剂，季铵化合物和聚合引发剂的紧密共混物。为了增强和减少由丙烯酸基特殊填充的聚合物组合物模塑或铸造的制品的倾倒时间，可以将有效的矿粉量的反应调节剂如三丙基丙烷三丙烯酸酯引入聚合物组合物中。用于配制基于丙烯酸的颗粒填充的聚合物组合物的聚合糖浆基本上由约300至约1,000体积份的丙烯酸类单体，约0.01至约1体积份的无过氧化物的氧气供体，约0.5 至约5体积份的硫醇，和约0.3至约40体积份的与丙烯酸类单体相容的交联剂。

6. 发明授权

US4208915A Method of determining foreign material in food products using ultrasonic sound 失效
标题翻译：使用超声波测定食品中异物的方法
公开(公告)号：US4208915A
公开(公告)日：1980-06-24
申请号：US7984
申请日：1979-01-31
申请人： Bill R. Edwards
发明人： Bill R. Edwards
IPC分类号： G01N29/12 , G01N29/28 , G01N33/02 , G01N29/00 , B07C5/34
CPC分类号： G01N33/02 , G01N29/12 , G01N29/28 , G01N2291/2698
摘要： A method of determining foreign material such as metal and bone particles in food products, the method using ultrasonic sound frequencies from a plurality of transducers disposed in a rotatable cylinder having a liquid copulant. The cylinder having a surrounding flexible wall which is compressed on top of the surface of the food products. The sound frequencies are transmitted through the food products and received back by a receiver in the transducers for monitoring any variance in the frequency indicating foreign material in the food products.
摘要翻译：一种确定食品中异物如金属和骨颗粒的方法，该方法使用设置在具有液体共混物的可旋转圆筒中的多个换能器的超声波声频。圆筒具有围绕柔性壁的压缩在食品表面的顶部。声音频率通过食品传播，并由传感器中的接收器回传，用于监测指示食品中异物的频率变化。

7. 发明授权

US5492940A Acrylic/lactam resin compositions and method of producing same 失效
公开(公告)号：US5492940A
公开(公告)日：1996-02-20
申请号：US444605
申请日：1995-05-19
申请人： Bill R. Edwards
发明人： Bill R. Edwards
IPC分类号： C08F220/12 , C08J9/02 , C08K3/00 , C08J9/06 , C08J9/08
CPC分类号： C08J9/02 , C08F220/12 , C08K3/0008 , C08J2333/06
摘要： An acrylic/lactam monomer based polymeric resin is provided which has excellent weatherability, outstanding transparency and optical clarity, improved heath and solvent resistance, as well as improved impact strength. The acrylic/lactam monomer based polymeric resin is formulated by the catalytic activation at ambient temperature of a polymerization syrup which contains from about 300 to about 2970 parts by volume of an acrylic monomer, from about 30 to about 2700 parts by volume of a lactam monomer, from about 0.3 parts to about 40 parts by volume of a mercaptan chain transfer agent and from about 0.3 to about 40 parts by volume of a crosslinking agent capable of crosslinking the acrylic monomer and the lactam monomer. To prevent further polymerization of the polymeric constituents of the polymerization syrup, as well as to enhance the shelf life of the polymerization syrup, an effective amount of a polymerization inhibitor and an ultraviolet light stabilizer are incorporated into the polymerization syrup. The crosslinking of the acrylic monomer and the lactam monomer is carried out at ambient temperature and atmospheric pressure.

8. 发明授权

US5399593A Acrylic/lactam resin compositions and method of producing same 失效
标题翻译：丙烯酸/内酰胺树脂组合物及其制备方法
公开(公告)号：US5399593A
公开(公告)日：1995-03-21
申请号：US136632
申请日：1993-10-14
申请人： Bill R. Edwards
发明人： Bill R. Edwards
IPC分类号： C08F220/12 , C08J9/02 , C08K3/00
CPC分类号： C08J9/02 , C08F220/12 , C08K3/0008 , C08J2333/06
摘要： An acrylic/lactam monomer based polymeric resin is provided which has excellent weatherability, outstanding transparency and optical clarity, improved heath and solvent resistance, as well as improved impact strength. The acrylic/lactam monomer based polymeric resin is formulated by the catalytic activation at ambient temperature of a polymerization syrup which contains from about 300 to about 2970 parts by volume of an acrylic monomer, from about 30 to about 2700 parts by volume of a lactam monomer, from about 0.3 parts to about 40 parts by volume of a mercaptan chain transfer agent and from about 0.3 to about 40 parts by volume of a crosslinking agent capable of crosslinking the acrylic monomer and the lactam monomer. To prevent further polymerization of the polymeric constituents of the polymerization syrup, as well as to enhance the shelf life of the polymerization syrup, an effective amount of a polymerization inhibitor and an ultraviolet light stabilizer are incorporated into the polymerization syrup. The crosslinking of the acrylic monomer and the lactam monomer is carried out at ambient temperature and atmospheric pressure.
摘要翻译：提供了一种丙烯酸/内酰胺单体的聚合物树脂，其具有优异的耐候性，优异的透明度和光学透明度，改善的耐磨性和耐溶剂性以及改善的冲击强度。基于丙烯酸/内酰胺单体的聚合物树脂通过聚合糖浆的环境温度下的催化活化来配制，所述聚合糖浆含有约300至约2970体积份的丙烯酸单体，约30至约2700体积份的内酰胺单体，约0.3-约40体积份的硫醇链转移剂和约0.3-约40体积份的能够交联丙烯酸单体和内酰胺单体的交联剂。为了防止聚合糖浆的聚合物成分的进一步聚合，以及提高聚合糖浆的保存期限，将有效量的聚合抑制剂和紫外光稳定剂引入聚合糖浆中。丙烯酸单体和内酰胺单体的交联在环境温度和大气压下进行。

9. 发明授权

US5250596A Acrylic resin composition 失效
标题翻译：丙烯酸树脂组合物
公开(公告)号：US5250596A
公开(公告)日：1993-10-05
申请号：US47795
申请日：1993-04-15
申请人： Bill R. Edwards
发明人： Bill R. Edwards
IPC分类号： C08F2/38 , C08F220/12 , C08F265/06 , C08K5/42
CPC分类号： C08F220/12 , C08F265/06
摘要： An acrylic resin is provided which has excellent weatherability, outstanding transparency and improved heat and solvent resistance, as well as improved impact strength. The acrylic resin comprises an intimate blend of a polymerization syrup and a catalytic amount of a polymerization catalyst capable of effecting polymerization of the syrup. The polymerization syrup, which has an improved shelf life and can be stored at ambient temperature and atmospheric pressure, consists essentially of:(a) from about 300 to about 1000 parts per volume of an acrylic monomer represented by the formula ##STR1## wherein R is an alkyl moiety containing 1 to about 18 carbon atoms; (b) from about 0.1 to about 1000 parts by volume of a non-peroxide oxygen donator, such as 2,2-bis(allyloxymethyl)-butan-1-ol or diallylphthalate;(c) from about 0.5 to about 5 parts by volume of a mercaptan; and(d) from about 0.3 to about 40 parts by volume of a crosslinking agent compatible with the acrylic monomer.The polymerization syrup can further contain from about 0.25 to about 100 parts by volume of a hydroxyalkyl methacrylate and from about 1 to about 100 parts by volume of a polycarbonate compound.
摘要翻译：提供了具有优异的耐候性，优异的透明性和改善的耐热和耐溶剂性以及改善的冲击强度的丙烯酸树脂。丙烯酸树脂包括聚合糖浆和催化量的能够实现糖浆聚合的聚合催化剂的紧密共混物。具有改善的保质期并且可以在环境温度和大气压下储存的聚合糖浆基本上由以下组成：（a）约300至约1000份/体积的由式“IMAGE”表示的丙烯酸单体，其中R 是含有1至约18个碳原子的烷基部分; （b）约0.1至约1000体积份的非过氧化物供氧子，例如2,2-双（烯丙氧基甲基） - 丁-1-醇或邻苯二甲酸二烯丙酯; （c）约0.5至约5体积份的硫醇; 和（d）约0.3至约40体积份的与丙烯酸类单体相容的交联剂。聚合糖浆还可含有约0.25至约100体积份的甲基丙烯酸羟烷基酯和约1至约100体积份的聚碳酸酯化合物。

10. 发明授权

US5023313A Acrylic resin composition 失效
标题翻译：丙烯酸树脂组合物
公开(公告)号：US5023313A
公开(公告)日：1991-06-11
申请号：US528728
申请日：1990-05-23
申请人： Bill R. Edwards
发明人： Bill R. Edwards
IPC分类号： C08F2/38 , C08F220/12 , C08F265/06
CPC分类号： C08F220/12 , C08F265/06
摘要： An acrylic resin is provided which has excellent weatherability, outstanding transparency and improved heat and solvent resistance, as well as improved impact strength. The acrylic resin comprises an intimate blend of a polymerization syrup and a catalytic amount of a polymerization catalyst capable of effecting polymerization of the syrup. The polymerization syrup, which has an improved shelf life and can be stored at ambient temperature and atmospheric pressure, consists essentially of:(a) from about 300 to about 1000 parts per volume of an acrylic monomer represented by the formula ##STR1## wherein R is an alkyl moiety containing 1 to about 18 carbon atoms; (b) from about 0.1 to about 1 parts by volume of 2,2-bis(allyl-oxymethyl)-butan-1-ol;(c) from about 0.5 to about 5 parts by volume of a mercaptan; and(d) from about 0.3 to about 40 parts by volume of a crosslinking agent compatible with the acrylic monomer.The polymerization syrup can further contain from about 1 to about 100 parts by volume of a polycarbonate compound.
摘要翻译：提供了具有优异的耐候性，优异的透明性和改善的耐热和耐溶剂性以及改善的冲击强度的丙烯酸树脂。丙烯酸树脂包括聚合糖浆和催化量的能够实现糖浆聚合的聚合催化剂的紧密共混物。具有改善的保质期并且可以在环境温度和大气压下储存的聚合糖浆基本上由以下组成：（a）约300至约1000份/体积的由式“IMAGE”表示的丙烯酸单体，其中R 是含有1至约18个碳原子的烷基部分; （b）约0.1至约1体积份的2,2-双（烯丙基 - 氧甲基） - 丁-1-醇; （c）约0.5至约5体积份的硫醇; 和（d）约0.3至约40体积份的与丙烯酸类单体相容的交联剂。聚合糖浆还可含有约1至约100体积份的聚碳酸酯化合物。

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