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1. 发明授权

US4404028A Nickel base alloys which contain boron and have been processed by rapid solidification process 失效
标题翻译：含有硼并经快速凝固工艺加工的镍基合金
公开(公告)号：US4404028A
公开(公告)日：1983-09-13
申请号：US257778
申请日：1981-04-27
申请人： Viswanathan Panchanathan , Ranjan Ray , Bill C. Giessen
发明人： Viswanathan Panchanathan , Ranjan Ray , Bill C. Giessen
IPC分类号： C22C45/04 , C22C19/08
CPC分类号： C22C45/04
摘要： New nickel rich metal alloys containing copper along with specific amounts of boron are disclosed. The alloys are subjected to rapid solidification processing (RSP) techniques which produce cooling rates between .about.10.sup.5 .degree. to 10.sup.7 .degree. C./sec. The as-quenched ribbon, powder, etc. consists primarily of a metastable crystalline solid solution phase. The metastable crystalline phases are subjected to suitable heat treatments so as to produce a transformation to a stable multiphase microstructure which includes borides. This heat treated alloy exhibits superior mechanical properties with good corrosion and/or oxidation resistance for numerous engineering applications.
摘要翻译：公开了含有铜的新的富含镍的金属合金以及特定量的硼。对这些合金进行快速凝固处理（RSP）技术，其产生105°至107℃/秒之间的冷却速率。淬火带，粉末等主要由亚稳态的结晶固溶相组成。对亚稳态结晶相进行适当的热处理，以产生包含硼化物的稳定的多相微结构的转变。该热处理合金在许多工程应用中表现出优异的机械性能和良好的耐腐蚀和/或抗氧化性能。

2. 发明授权

US4430115A Boron stainless steel powder and rapid solidification method 失效
标题翻译：硼不锈钢粉末和快速凝固法
公开(公告)号：US4430115A
公开(公告)日：1984-02-07
申请号：US153775
申请日：1980-05-27
申请人： Ranjan Ray , Donald E. Polk , Bill C. Giessen
发明人： Ranjan Ray , Donald E. Polk , Bill C. Giessen
IPC分类号： B22F9/00 , C22C33/02 , C22C45/02 , B22F1/00 , B22F1/04
CPC分类号： C22C45/02 , B22F9/008 , C22C33/0285
摘要： Alloys having composition similar to commercial precipitation-hardenable stainless steels, but modified by the addition of 1.4 to 2.4 wt % boron, are disclosed. The alloys are subjected to a rapid solidification processing (RSP) technique which produces cooling rates between .about.10.sup.5 -10.sup.7 .degree.C./sec. The as-quenched RSP ribbon or powder, etc., consists primarily of a metastable crystalline solid solution phase. The metastable crystalline phases are subjected to suitable heat treatments so as to produce a transformation to a stable multiphase microstructure, which includes borides; this heat treated alloy exhibits superior mechanical properties and thermal stability in conjunction with good corrosion and oxidation resistance.
摘要翻译：公开了具有与商业沉淀硬化性不锈钢相似的组成，但通过加入1.4至2.4重量％的硼而改性的合金。对合金进行快速凝固处理（RSP）技术，其产生的差异在105-107℃/秒之间。淬灭的RSP带或粉末等主要由亚稳态的结晶固溶体相组成。对亚稳结晶相进行适当的热处理，以产生包括硼化物在内的稳定多相微观结构的转变; 该热处理合金具有优异的机械性能和热稳定性以及良好的耐腐蚀和抗氧化性。

3. 发明授权

US4359352A Nickel base superalloys which contain boron and have been processed by a rapid solidification process 失效
标题翻译：含有硼的镍基超级合金，并通过快速凝固工艺加工
公开(公告)号：US4359352A
公开(公告)日：1982-11-16
申请号：US95382
申请日：1979-11-19
申请人： Ranjan Ray , Donald E. Polk , Bill C. Giessen
发明人： Ranjan Ray , Donald E. Polk , Bill C. Giessen
IPC分类号： C22C19/05 , C22C30/00
CPC分类号： C22C19/05 , Y10S75/952
摘要： Nickel and iron-nickel base alloys are described together with a rapid solidification process used in the preparation thereof to provide materials useful in the fabrication of parts subject to high temperature operating conditions. The alloys include commercial nickel base superalloys to which a specified amount of boron is added.
摘要翻译：镍和铁 - 镍基合金与其制备中使用的快速固化方法一起描述，以提供用于制造经受高温操作条件的部件的材料。合金包括商业镍基超级合金，其中加入了特定量的硼。

4. 发明授权

US4347076A Aluminum-transition metal alloys made using rapidly solidified powers and method 失效
标题翻译：使用快速固化的功率和方法制备的铝 - 过渡金属合金
公开(公告)号：US4347076A
公开(公告)日：1982-08-31
申请号：US193417
申请日：1980-10-03
申请人： Ranjan Ray , Donald E. Polk , Bill C. Giessen
发明人： Ranjan Ray , Donald E. Polk , Bill C. Giessen
IPC分类号： B22F9/00 , C22C1/04 , C22C45/08
CPC分类号： B22F9/00 , B22F9/008 , C22C1/0416 , C22C45/08
摘要： A method of fabricating aluminum alloys containing finely dispersed aluminum-transition metal intermetallic phases is disclosed. The alloys are subjected to melt spinning to form a brittle filament consisting in large measure of a metastable face-centered cubic solid solution; this is then pulverized to a staple or powder configuration; the power or staple is consolidated using conventional techniques. Upon heat treatment, the solid solution decomposes into a structure consisting of an aluminum alloy matrix of conventional composition containing a fine uniform dispersion of the intermetallic phase, the heat-treated alloy being ductile. The heat-treated alloys possess high strength, especially at elevated temperatures. Preferred alloys are disclosed which contain 10 to 15 wt % Fe.
摘要翻译：公开了一种制造含有细分散的铝 - 过渡金属金属间相的铝合金的方法。将合金进行熔融纺丝以形成由大量亚稳的面心立方固溶体组成的脆性长丝; 然后将其粉碎成短纤维或粉末构型; 使用常规技术来整合动力或装订。通过热处理，固溶体分解成由包含金属间相的细均匀分散体的常规组合物的铝合金基体组成的结构，热处理的合金是延展性的。热处理的合金具有高强度，特别是在高温下。公开了含有10至15重量％Fe的优选合金。

5. 发明授权

US5677265A Process for oxygenation of ceramic high T.sub.c superconductors 失效
标题翻译：陶瓷高Tc超导体氧化工艺
公开(公告)号：US5677265A
公开(公告)日：1997-10-14
申请号：US398289
申请日：1995-03-03
申请人： Bill C. Giessen , Robert S. Markiewicz , Bala Maheswaran , Thomas R. Gilbert
发明人： Bill C. Giessen , Robert S. Markiewicz , Bala Maheswaran , Thomas R. Gilbert
IPC分类号： C04B35/64 , H01L39/24 , C04B35/638 , C04B35/76
CPC分类号： C04B35/64 , H01L39/2464 , Y10S505/728 , Y10S505/785
摘要： A process for the oxygenation of ceramic high T.sub.c superconductors is disclosed. The superconductor is formed from a sintered powdered ceramic. Microchannels are formed in the ceramic material by embedding in the powder a plurality of wires or fibers formed of a material which is thermally removable during the sintering process to leave thin, continuous, tubular channels. After sintering, the ceramic is exposed to oxygen in a high temperature, high pressure environment. The microchannels aid in the transport of oxygen into the interior of the material by providing passages along which the oxygen travels prior to diffusing into the material. The lengths of the diffusion paths in the material are thereby greatly shortened. In another embodiment, the channels are formed after sintering and prior to oxygenation by drilling, punching, or etching.
摘要翻译：公开了一种用于陶瓷高Tc超导体氧合的方法。超导体由烧结陶瓷粉末形成。在陶瓷材料中形成微通道，通过在粉末中埋入由在烧结过程中可热去除的材料形成的多根线或纤维，以留下薄而连续的管状通道。烧结后，陶瓷在高温，高压环境下暴露于氧气。微通道有助于通过在扩散到材料中之前提供氧气在其中行进的通道将氧气输送到材料的内部。因此，材料中的扩散路径的长度大大缩短。在另一个实施方案中，通道在烧结之后并且在通过钻孔，冲压或蚀刻进行氧合之前形成。

6. 发明授权

US5593514A Amorphous metal alloys rich in noble metals prepared by rapid solidification processing 失效
标题翻译：通过快速固化处理制备富含贵金属的无定形金属合金
公开(公告)号：US5593514A
公开(公告)日：1997-01-14
申请号：US348017
申请日：1994-12-01
申请人： Bill C. Giessen , Sunil V. Gokhale , Krassimir G. Marchev
发明人： Bill C. Giessen , Sunil V. Gokhale , Krassimir G. Marchev
IPC分类号： C22C45/00 , C22C5/02 , C22C5/04 , C22C5/06
CPC分类号： C22C45/003
摘要： Amorphous metal alloys rich in noble metals prepared by rapid solidification processing are disclosed. The alloys have at least a ternary composition having the formula M.sub.a G1.sub.b G2.sub.c, wherein M is at least one element selected from the group consisting of Ag, Au, Ru, Os, Rh, Ir, Pd, and Pt, and G1 is at least one element selected from the group consisting of B, C, Cu, Ni, Si, and Be, and G2 is at least one element selected from the group consisting of Y, the lanthanides, Zr, Hf, Ca, Mg, Ti, Nb, and Ta. The subscripts a, b, and c are atomic percentages; a ranges from 70 to 90 percent, and b and c range from 5 to 15 percent each. Preferably, a is at least 80 percent and b and c are generally equal. The amorphous metal alloys are readily glass forming and thermally stable at room temperatures.
摘要翻译：公开了通过快速凝固处理制备的富含贵金属的无定形金属合金。该合金具有至少一种具有式MaG1bG2c的三元组合物，其中M是选自Ag，Au，Ru，Os，Rh，Ir，Pd和Pt中的至少一种元素，G1是至少一种元素选自由B，C，Cu，Ni，Si和Be组成的组中的至少一种元素，G 2是选自Y，镧系元素，Zr，Hf，Ca，Mg，Ti，Nb和 Ta 下标a，b和c是原子百分比; a范围从70％到90％，b和c范围从5％到15％。优选地，a为至少80％，b和c通常相等。非晶态金属合金在室温下易于形成玻璃并具有热稳定性。

7. 发明授权

US4540546A Method for rapid solidification processing of multiphase alloys having large liquidus-solidus temperature intervals 失效
标题翻译：用于液相线 - 固相线温度较高的多相合金的快速凝固加工方法
公开(公告)号：US4540546A
公开(公告)日：1985-09-10
申请号：US558612
申请日：1983-12-06
申请人： Bill C. Giessen
发明人： Bill C. Giessen
IPC分类号： B22D11/06 , B22F9/00 , B22F9/10 , C22C1/10 , C22C45/00 , C22C1/02 , C21C5/56
CPC分类号： B22D11/0611 , B22F9/008 , B22F9/10 , C22C1/1042 , C22C45/00 , Y10S75/956
摘要： Rapid solidification processing by liquid quenching is made practical for multiphase alloys having relatively large liquidus-solidus temperature intervals by a new processing technique termed "melt mix reaction" involving chemically reacting two starting alloys in a mixing nozzle in which a melt mix reaction takes place between the chemically reactable components of the starting alloys to form submicron particles of the resultant compound in the final alloy. The mixing and chemical reaction is performed at a temperature which is at or above the highest liquidus temperature of the starting alloys but which is also substantially below the liquidus temperature of the final alloy, and as close to the solidus temperature of the final alloy as possible. Rapid solidification may be accomplished through the utilization of a melt spinning wheel or may be accomplished through the utilization of an atomizing nozzle configuration, with the rapidly solidified alloy containing a matrix with a microdispersion or a precipitate of the resulting compound contained therein. Heat treatment of the rapidly solidified final alloy may be additionally employed to produce precipitate hardening of the final alloy should such microdispersed precipitates not be formed or be formed incompletely during the rapid solidification process.
摘要翻译：通过液体淬火的快速凝固处理对于具有相对较大的液相线 - 固相线温度间隔的多相合金是实用的，通过称为“熔融混合反应”的新的加工技术，包括在混合喷嘴中使两种起始合金化学反应，其中发生熔融混合反应起始合金的化学反应成分，以在最终合金中形成所得化合物的亚微米颗粒。混合和化学反应在等于或高于原始合金的最高液相线温度的温度下进行，但也大大低于最终合金的液相线温度，并且尽可能接近最终合金的固相线温度。可以通过利用熔融纺丝轮来实现快速凝固，或者可以通过利用雾化喷嘴构型来实现快速凝固的合金，其中含有微分散体的基质或其中所含的所得化合物的沉淀物。如果这种微分散的沉淀物在快速凝固过程中不形成或不完全形成，则可以另外使用快速固化的最终合金的热处理来产生最终合金的沉淀硬化。

8. 发明授权

US4362553A Tool steels which contain boron and have been processed using a rapid solidification process and method 失效
标题翻译：含有硼的工具钢，并使用快速固化方法和方法进行处理
公开(公告)号：US4362553A
公开(公告)日：1982-12-07
申请号：US275629
申请日：1981-06-22
申请人： Ranjan Ray , Donald E. Polk , Bill C. Giessen
发明人： Ranjan Ray , Donald E. Polk , Bill C. Giessen
IPC分类号： B22F9/00 , C22C33/02 , C22C38/12 , C22C38/32 , C22C38/22 , C22C38/24 , C22C38/26
CPC分类号： B22F9/008 , C22C33/0257 , C22C38/12 , C22C38/32
摘要： Iron base alloys containing chromium and refractory metals as well as 0.8 to 1.3 wt % boron are disclosed. The alloys are subjected to a rapid solidification processing (RSP) technique, producing cooling rates of about 10.sup.5 to 10.sup.7 .degree. C./sec. The as-quenched RSP ribbon, or powder, etc., consists primarily of a single phase with a body centered cubic structure. After appropriate heat treatments, the rapidly solidified alloys have a microstructure consisting of ultrafine hard particles of metallic carbides and borides and mixtures thereof dispersed in an iron-rich matrix. These alloys exhibit excellent corrosion resistance combined with high hardness, wear resistance and high temperature stability. These heat treated alloys have superior properties which make them suitable for many applications, where high strength and corrosion resistance are required, in particular at elevated temperature, e.g. high temperature bearings.
摘要翻译：公开了含有铬和难熔金属的铁基合金以及0.8至1.3重量％的硼。对合金进行快速凝固处理（RSP）技术，产生约105至107℃/秒的冷却速率。淬火后的RSP带或粉末等主要由具有体心立方结构的单相组成。在适当的热处理之后，快速固化的合金具有由分散在富铁基质中的金属碳化物和硼化物的超细硬质颗粒及其混合物组成的显微组织。这些合金表现出优异的耐腐蚀性，结合高硬度，耐磨性和高温稳定性。这些热处理的合金具有优异的性能，使得它们适用于需要高强度和耐腐蚀性的许多应用，特别是在升高的温度下。高温轴承。

9. 发明授权

US08349093B2 Method of plasma nitriding of alloys via nitrogen charging 有权
标题翻译：通过氮气充填等离子体氮化合金的方法
公开(公告)号：US08349093B2
公开(公告)日：2013-01-08
申请号：US12479904
申请日：2009-06-08
申请人： Clark VanTine Cooper , Krassimir G. Marchev , Bill C. Giessen
发明人： Clark VanTine Cooper , Krassimir G. Marchev , Bill C. Giessen
IPC分类号： C23C8/24
CPC分类号： C23C8/26 , C23C8/02 , C23C8/80 , Y10T428/12 , Y10T428/12458
摘要： A nitrided metal includes a metal core with a first microstructure and a nitrogen-containing solid solution region on the metal core. The nitrogen-containing solid solution region is free of nitride compounds and includes a second microstructure which is equivalent to the first microstructure. The first microstructure and the second microstructure are a tetragonal crystal structure.
摘要翻译：氮化金属包括在金属芯上具有第一微结构和含氮固溶体区域的金属芯。含氮固溶体区域不含氮化物，并且包括与第一微结构相当的第二微结构。第一微结构和第二微结构是四方晶体结构。

10. 发明申请

US20090246551A1 METHOD OF PLASMA NITRIDING OF ALLOYS VIA NITROGEN CHARGING 有权
标题翻译：通过氮素充填法合成氮等离子体的方法
公开(公告)号：US20090246551A1
公开(公告)日：2009-10-01
申请号：US12479904
申请日：2009-06-08
申请人： Clark VanTine Cooper , Krassimir G. Marchev , Bill C. Giessen
发明人： Clark VanTine Cooper , Krassimir G. Marchev , Bill C. Giessen
IPC分类号： B32B5/14 , B32B15/04
CPC分类号： C23C8/26 , C23C8/02 , C23C8/80 , Y10T428/12 , Y10T428/12458
摘要： A method of nitriding a metal includes transforming a surface region of a generally nitrogen-free metal into a nitrogen-containing solid solution surface region. A first heating process heats the surface region at a first temperature in the presence of a nitrogen gas partial pressure to form a nitrogen-charged surface portion on the surface region. A second heating process heats the surface region and nitrogen-charged surface portion at a second temperature for a predetermined time to interstitially diffuse nitrogen from the nitrogen-charged surface portion a depth into the surface region. Coincident with the second heating process, an ionized inert or reducing gas removes the nitrogen-charged surface portion. The resulting nitrogen-containing solid solution surface region has a gradual transition in nitrogen concentration.
摘要翻译：金属氮化的方法包括将一般无氮金属的表面区域转化为含氮固溶体表面区域。在氮气分压的存在下，第一加热工艺在第一温度下加热表面区域，以在表面区域上形成带氮表面部分。第二加热过程在第二温度下将表面区域和带氮表面部分加热预定时间，从而将含氮表面部分的氮气间隙地扩散到表面区域。与第二加热方法一致，电离的惰性或还原气体除去带氮的表面部分。所得到的含氮固溶体表面区域的氮浓度逐渐变化。

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