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1. 发明授权

US5652030A Vapor phase chemical infiltration process of a material into a porous substrate at controlled surface temperature 失效
标题翻译：将材料的气相化学渗透过程控制在表面温度下进入多孔基材
公开(公告)号：US5652030A
公开(公告)日：1997-07-29
申请号：US635933
申请日：1996-04-25
申请人： Bernard Delperier , Christian Robin-Brosse , Jean-Luc Domblides , Gilles Bondieu
发明人： Bernard Delperier , Christian Robin-Brosse , Jean-Luc Domblides , Gilles Bondieu
IPC分类号： C04B35/52 , C04B35/80 , C04B35/83 , C04B35/84 , C23C16/52 , C23C8/00
CPC分类号： C04B35/806 , C04B35/83 , Y10S427/10
摘要： The substrate (10) is placed in an enclosure (12) and is heated so as to establish therein a temperature gradient such that the substrate has a higher temperature in portions that are remote from its exposed surfaces than at its exposed surfaces. A reaction gas constituting a precursor for the material to be infiltrated is admitted into the enclosure, with formation of the material being enhanced in those portions of the substrate that are at higher temperature. At the beginning of the infiltration process, and at least during the major portion thereof, substrate heating is controlled in such a manner as to maintain the temperature of its exposed surfaces at a value that is no greater than the minimum temperature for the reaction gas to deposit the material that is to be infiltrated, while portions of the substrate that are remote from its exposed surfaces are at a temperature that is greater than the minimum temperature for deposition.
摘要翻译： PCT No.PCT / FR94 / 01090 Sec。 371日期：1996年4月25日 102（e）日期1996年4月25日PCT 1994年9月20日PCT公布。公开号WO95 / 11868 日期1995年5月4日将衬底（10）放置在外壳（12）中并被加热以便在其中建立温度梯度，使得衬底在远离其暴露表面的部分中比在其暴露表面处具有更高的温度。构成待渗透材料的前体的反应气体被允许进入外壳，在衬底的处于较高温度的部分中材料的形成被增强。在渗透过程开始时，并且至少在其主要部分期间，基板加热被控制为将其暴露表面的温度保持在不大于反应气体的最低温度的值沉积要渗透的材料，而远离其暴露表面的基底的部分处于大于沉积最低温度的温度。

2. 发明授权

US06410088B1 CVI (chemical vapor infiltration) densification of porous structures 失效
标题翻译：多孔结构的CVI（化学气相渗透）致密化
公开(公告)号：US06410088B1
公开(公告)日：2002-06-25
申请号：US09420428
申请日：1999-10-19
申请人： Christian Robin-Brosse , Jacques Thebault , Yves Patrigeon , Gilles Bondieu , Jean-Luc Domblides
发明人： Christian Robin-Brosse , Jacques Thebault , Yves Patrigeon , Gilles Bondieu , Jean-Luc Domblides
IPC分类号： C23C1626
CPC分类号： C04B41/009 , C04B35/83 , C04B41/5001 , C04B41/85 , C23C16/045 , C23C16/26 , C04B41/4531 , C04B41/4554 , C04B30/02
摘要： The present invention provides a method of densifying porous structures by chemical vapor infiltration. In characteristic manner, said densification method is implemented using toluene as a precursor for carbon. Said toluene is generally used mixed with at least one carrier gas.
摘要翻译：本发明提供一种通过化学气相渗透致密化多孔结构的方法。以特征方式，使用甲苯作为碳前体来实施所述致密化方法。所述甲苯通常与至少一种载气混合使用。

3. 发明授权

US08084079B2 Method for chemical infiltration in the gas phase for the densification of porous substrates with pyrolytic carbon 有权
标题翻译：在气相中化学渗透的方法用于用热解碳致密化多孔基材
公开(公告)号：US08084079B2
公开(公告)日：2011-12-27
申请号：US11795938
申请日：2006-01-23
申请人： Jacques Thebault , Sébastien Bertrand , Christian Robin-Brosse , Bruno Bernard , Jean-Luc Domblides
发明人： Jacques Thebault , Sébastien Bertrand , Christian Robin-Brosse , Bruno Bernard , Jean-Luc Domblides
IPC分类号： C23C16/26 , C23C16/52
CPC分类号： C23C16/45593 , C23C16/045 , C23C16/26 , Y10S427/10
摘要： A method of densifying a porous substrate with pyrolytic carbon includes loading the substrate into an oven, admitting a reaction gas mixture to the oven, extracting an effluent gas from the oven, and recycling components of the effluent gas into the reaction gas mixture. The reaction gas mixture contains a pyrolytic carbon precursor gas together with a vector gas. The effluent gas contains residual components of the reaction gas mixture together with reaction products, including hydrogen. The recycling is performed after eliminating heavy hydrocarbons contained in the effluent gas.
摘要翻译：用热解碳致密化多孔基材的方法包括将基底加载到烘箱中，将反应气体混合物加入到烘箱中，从烘箱中提取出来的废气，并将废气中的成分再循环到反应气体混合物中。反应气体混合物与载气一起含有热解碳前体气体。废气中含有反应气体混合物的残留组分和反应产物，包括氢气。在排除废气中含有的重质烃后进行回收。

4. 发明申请

US20080160192A1 Method For Chemical Infiltration in the Gas Phase For the Densification of Porous Substrates With Pyrolytic Carbon 有权
标题翻译：气相中化学渗透方法用于热解碳多孔基材的致密化
公开(公告)号：US20080160192A1
公开(公告)日：2008-07-03
申请号：US11795938
申请日：2006-01-23
申请人： Jacques Thebault , Sebastien Bertrand , Christian Robin-Brosse , Bruno Bernard , Jean-Luc Domblides
发明人： Jacques Thebault , Sebastien Bertrand , Christian Robin-Brosse , Bruno Bernard , Jean-Luc Domblides
IPC分类号： C23C16/04 , C23C16/26
CPC分类号： C23C16/45593 , C23C16/045 , C23C16/26 , Y10S427/10
摘要： One or more porous substrates for densification (10) are loaded into an oven (12) into which there is admitted a reaction gas containing a pyrolytic carbon precursor gas comprising at least one gaseous hydrocarbons CxHy in which x and y are integers and x is such that 1
摘要翻译：将一个或多个用于致密化的多孔基材（10）装载到烘箱（12）中，其中允许含有包含至少一种气态碳氢化合物的热解碳前体气体的反应气体其中x和y是整数，x是1

5. 发明授权

US06942893B2 Densifying hollow porous substrates by chemical vapor infiltration 有权
标题翻译：通过化学气相渗透对中空多孔基材进行致密化
公开(公告)号：US06942893B2
公开(公告)日：2005-09-13
申请号：US10024272
申请日：2001-12-18
申请人： Bernard Delperier , Jean-Luc Domblides , Jean-Philippe Richard , Pierre Delaurens
发明人： Bernard Delperier , Jean-Luc Domblides , Jean-Philippe Richard , Pierre Delaurens
IPC分类号： C04B41/85 , C04B35/83 , C23C16/04 , C23C16/26 , C23C16/455 , C23C16/458
CPC分类号： C04B35/83 , C23C16/045 , C23C16/26 , Y10S427/10
摘要： A porous substrate having a concave inside face and an outside face is disposed in an enclosure, and reactive gas is introduced into the enclosure to densify the substrate. At least a portion of the gas is divided into two non-zero fractions. The first fraction of the gas is fed to the inside face of the substrate. The second fraction of the gas is fed to only the outside face of the substrate. Alternatively, the first fraction of the gas is fed via a tooling extending into an inside volume defined by the concave inside face of the substrate.
摘要翻译：具有凹入的内表面和外表面的多孔基材设置在外壳中，并且将反应性气体引入外壳中以使基底致密。气体的至少一部分被分成两个非零分数。气体的第一部分被供给到衬底的内表面。气体的第二部分仅被供给到基板的外表面。或者，气体的第一部分经由延伸到由衬底的凹入内表面限定的内部体积的工具进给。

6. 发明授权

US6001419A Chemical vapor infiltration method with variable infiltration parameters 失效
标题翻译：化学气相渗透法具有可变渗透参数
公开(公告)号：US6001419A
公开(公告)日：1999-12-14
申请号：US930743
申请日：1997-10-06
申请人： Jean-Luc Leluan , Jean-Luc Domblides , Bernard Delperier , Jacques Thebault , Jean-Marie Toussaint
发明人： Jean-Luc Leluan , Jean-Luc Domblides , Bernard Delperier , Jacques Thebault , Jean-Marie Toussaint
IPC分类号： C04B35/80 , C04B35/83 , C23C16/52 , F16D69/02 , C23C16/00
CPC分类号： F16D69/023 , C04B35/806 , C04B35/83
摘要： Between the start and the end of the chemical vapor infiltration process, filtration conditions are modified by causing at least one of the following infiltration parameters to vary: retention time of the gas, pressure, temperature, concentration of precursor in the gas, and concentration of dopant, if any, in the gas; thereby adapting infiltration conditions to changes in the porometry of the substrate in order to control the microstructure of the material deposited within the substrate, in particular in order to conserve a microstructure that is constant.
摘要翻译： PCT No.PCT / FR96 / 00530 Sec。 371日期：1997年10月6日 102（e）日期1997年10月6日PCT 1996年4月9日PCT PCT。公开号WO96 / 31447 日期1996年10月10日在化学气相渗透过程的开始和结束之间，通过使至少一个以下渗透参数变化来改变渗透条件：气体的保留时间，压力，温度，前体浓度气体和气体中掺杂剂的浓度（如果有的话）; 从而使渗透条件适应于衬底的孔隙率的变化，以便控制沉积在衬底内的材料的微结构，特别是为了保持恒定的微结构。

7. 发明授权

US5789026A Chemical vapor infiltration process of a pyrocarbon matrix within a porous substrate with creation of a temperature gradient in the substrate 失效
标题翻译：在多孔基材内的热解碳基质的化学气相渗透过程，在基质中产生温度梯度
公开(公告)号：US5789026A
公开(公告)日：1998-08-04
申请号：US632487
申请日：1996-04-25
申请人： Bernard Delperier , Jean-Luc Domblides
发明人： Bernard Delperier , Jean-Luc Domblides
IPC分类号： C04B35/80 , C04B35/83 , C04B35/84 , C23C16/26
CPC分类号： C04B35/806 , C04B35/83
摘要： The substrate (10) is placed in an enclosure (12) and is heated so as to establish a temperature gradient within the substrate such that the substrate has a temperature in its portions remote from its exposed surfaces that is greater than its temperature at said surfaces. A gas constituting a precursor of carbon and comprising at least one saturated or unsaturated hydrocarbon is admitted into the enclosure, with the formation of pyrolytic carbon be favored in the higher temperature portions of the substrate. The gas comprises a mixture containing at least one saturated or unsaturated hydrocarbon and hydrogen, and the substrate is heated in such a manner as to establish a temperature gradient within the substrate on either side of a temperature of 1500 K, with hydrogen having an inhibiting role at temperatures below 1500 K.
摘要翻译： PCT No.PCT / FR94 / 01074 Sec。 371日期：1996年4月25日 102（e）日期1996年4月25日PCT提交1994年9月14日PCT公布。公开号WO95 / 11867 日期1995年5月4日将衬底（10）放置在外壳（12）中并被加热以便在衬底内建立温度梯度，使得衬底的远离其暴露表面的部分的温度大于其所述表面的温度。构成碳前体并含有至少一种饱和或不饱和烃的气体进入外壳，热解碳的形成在基材的较高温度部分受到青睐。气体包括含有至少一种饱和或不饱和烃和氢的混合物，并且以这样一种方式加热底物，以便在1500K温度的两侧在衬底内建立温度梯度，其中氢具有抑制作用温度低于1500K。

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