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1. 发明申请

US20210245112A1 MIXED MATRIX MEMBRANES, AND RELATED GAS SEPARATION MEMBRANE APPARATUSES, GASEOUS FLUID TREATMENT SYSTEMS, AND METHODS 有权
公开(公告)号：US20210245112A1
公开(公告)日：2021-08-12
申请号：US17174796
申请日：2021-02-12
申请人： Battelle Energy Alliance, LLC , UChicago Argonne, LLC , Adamas Nanotechnologies, Inc.
发明人： Frederick F. Stewart , Christopher J. Orme , John R. Klaehn , Birendra Adhikari , Olga Aleksandrovna Shenderova , Nicholas Austin Nunn , Marco D. Torelli , Gary Elder McGuire , Tae H. Lee , Uthamalingam Balachandran
IPC分类号： B01D69/14 , B01D53/22 , B01D67/00 , B01D71/02 , B01D71/68 , B01D71/38 , B01D71/82
摘要： A mixed matrix membrane comprises a support structure. The support structure comprises a glassy polymer matrix, and nanodiamond particles dispersed within the glassy polymer matrix. A gas separation membrane apparatus, a gaseous fluid treatment system, and a method of forming a mixed matrix membrane are also described.

2. 发明申请

US20130345350A1 POLYMER COMPOSITIONS, POLYMER FILMS, AND METHODS FOR FORMING SAME 有权
标题翻译：聚合物组合物，聚合物膜及其形成方法
公开(公告)号：US20130345350A1
公开(公告)日：2013-12-26
申请号：US14014664
申请日：2013-08-30
申请人： Battelle Energy Alliance, LLC
发明人： John R. Klaehn , Eric S. Peterson , Christopher J. Orme
IPC分类号： C08L79/04
CPC分类号： C08L79/04 , C08L61/28 , Y10T428/31862
摘要： Stable, high performance polymer compositions including polybenzimidazole (PBI) and a melamine-formaldehyde polymer, such as methylated, poly(melamine-co-formaldehyde), for forming structures such as films, fibers and bulky structures. The polymer compositions may be formed by combining polybenzimidazole with the melamine-formaldehyde polymer to form a precursor. The polybenzimidazole may be reacted and/or intertwined with the melamine-formaldehyde polymer to form the polymer composition. For example, a stable, free-standing film having a thickness of, for example, between about 5 μm and about 30 μm may be formed from the polymer composition. Such films may be used as gas separation membranes and may be submerged into water for extended periods without crazing and cracking. The polymer composition may also be used as a coating on substrates, such as metal and ceramics, or may be used for spinning fibers. Precursors for forming such polymer compositions are also disclosed.
摘要翻译：稳定的高性能聚合物组合物，包括聚苯并咪唑（PBI）和三聚氰胺 - 甲醛聚合物，例如甲基化，聚（三聚氰胺 - 共 - 甲醛），用于形成诸如膜，纤维和大体积结构的结构。聚合物组合物可以通过将聚苯并咪唑与三聚氰胺 - 甲醛聚合物组合以形成前体而形成。聚苯并咪唑可以与三聚氰胺 - 甲醛聚合物反应和/或缠结形成聚合物组合物。例如，可以由聚合物组合物形成具有例如约5μm至约30μm厚度的稳定的自立膜。这样的膜可以用作气体分离膜，并且可以长时间浸入水中而不会龟裂和破裂。聚合物组合物也可以用作基底上的涂层，例如金属和陶瓷，或者可以用于纺丝纤维。还公开了用于形成这种聚合物组合物的前体。

3. 发明公开

US20240055680A1 METHODS OF RECOVERING LITHIUM FROM A LITHIUM-CONTAINING MATERIAL, AND RELATED SYSTEMS 审中-公开
公开(公告)号：US20240055680A1
公开(公告)日：2024-02-15
申请号：US18257786
申请日：2021-12-15
申请人： Battelle Energy Alliance, LLC
发明人： Luis A. Diaz Aldana , Tedd E. Lister , Aaron D. Wilson , John R. Klaehn , Meng Shi
IPC分类号： H01M10/54 , C25B1/14 , C22B7/00 , C25B9/19 , C25B15/08 , C22B26/12 , C22B3/00
CPC分类号： H01M10/54 , C25B1/14 , C22B7/007 , C25B9/19 , C25B15/083 , C22B26/12 , C22B23/0415 , H01M10/0525
摘要： A method of recovering lithium from a lithium-containing material comprises introducing a lithium-containing material to an electrochemical cell, transporting lithium ions from the lithium-containing material through a cation exchange membrane to a catholyte within a cathode chamber of the electrochemical cell, reacting the lithium ions with bicarbonate ions in the cathode chamber to form lithium carbonate, and removing the lithium carbonate from the catholyte. Related methods of recovering lithium from lithium-containing, materials, and related systems are disclosed.

4. 发明申请

US20210060492A1 THERMALLY REFLECTIVE MEMBRANE APPARATUSES, AND RELATED FLUID TREATMENT SYSTEMS AND METHODS 有权
公开(公告)号：US20210060492A1
公开(公告)日：2021-03-04
申请号：US17009421
申请日：2020-09-01
申请人： Battelle Energy Alliance, LLC
发明人： John R. Klaehn , Christopher J. Orme , Aaron D. Wilson , Birendra Adhikari , Frederick F. Stewart , Seth W. Snyder
IPC分类号： B01D61/36 , B01D69/02 , B01D69/12
摘要： A thermally reflective membrane apparatus comprises a housing structure, and a thermally reflective membrane contained within the housing structure. The thermally reflective membrane comprises a semipermeable structure, and a porous, thermally reflective structure physically contacting the semipermeable structure. The porous, thermally reflective structure comprises discrete thermally reflective particles, and a binder material coupling the discrete thermally reflective particles to one another and the semipermeable structure. A fluid treatment system and method of treating a fluid are also described.

5. 发明申请

US20210060488A1 METHODS, SYSTEMS, AND APPARATUSES FOR TREATING FLUIDS USING THERMAL GRADIENT OSMOSIS 有权
公开(公告)号：US20210060488A1
公开(公告)日：2021-03-04
申请号：US17009360
申请日：2020-09-01
申请人： Battelle Energy Alliance, LLC
发明人： Aaron D. Wilson , Christopher J. Orme , John R. Klaehn , Birendra Adhikari , Frederick F. Stewart , Seth W. Snyder
IPC分类号： B01D61/00 , B01D69/10 , B01D69/02 , B01D53/22 , C02F1/44
摘要： A method of treating a fluid comprises introducing a feed fluid stream comprising multiple materials to first side of a semi-permeable membrane. A draw fluid stream having a higher temperature than the feed fluid stream is introduced to second, opposing side of the semi-permeable membrane to form a thermal gradient across the semi-permeable membrane. One or more of the multiple materials of the feed fluid stream is drawn through the semi-permeable membrane and into the draw fluid stream via thermal gradient osmosis. A fluid treatment system and a thermal gradient osmosis apparatus are also described.

6. 发明授权

US09080052B2 Precursor polymer compositions comprising polybenzimidazole 有权
标题翻译：包含聚苯并咪唑的前体聚合物组合物
公开(公告)号：US09080052B2
公开(公告)日：2015-07-14
申请号：US14014664
申请日：2013-08-30
申请人： Battelle Energy Alliance, LLC
发明人： John R. Klaehn , Eric S. Peterson , Christopher J. Orme
IPC分类号： C08L79/04 , C08L61/28 , C08G14/10 , C08G73/18 , C08F283/00
CPC分类号： C08L79/04 , C08L61/28 , Y10T428/31862
摘要： Stable, high performance polymer compositions including polybenzimidazole (PBI) and a melamine-formaldehyde polymer, such as methylated, poly(melamine-co-formaldehyde), for forming structures such as films, fibers and bulky structures. The polymer compositions may be formed by combining polybenzimidazole with the melamine-formaldehyde polymer to form a precursor. The polybenzimidazole may be reacted and/or intertwined with the melamine-formaldehyde polymer to form the polymer composition. For example, a stable, free-standing film having a thickness of, for example, between about 5 μm and about 30 μm may be formed from the polymer composition. Such films may be used as gas separation membranes and may be submerged into water for extended periods without crazing and cracking. The polymer composition may also be used as a coating on substrates, such as metal and ceramics, or may be used for spinning fibers. Precursors for forming such polymer compositions are also disclosed.
摘要翻译：稳定的高性能聚合物组合物，包括聚苯并咪唑（PBI）和三聚氰胺 - 甲醛聚合物，例如甲基化，聚（三聚氰胺 - 共 - 甲醛），用于形成诸如膜，纤维和大体积结构的结构。聚合物组合物可以通过将聚苯并咪唑与三聚氰胺 - 甲醛聚合物组合以形成前体而形成。聚苯并咪唑可以与三聚氰胺 - 甲醛聚合物反应和/或缠结形成聚合物组合物。例如，可以由聚合物组合物形成具有例如约5μm至约30μm的厚度的稳定的自立膜。这样的膜可以用作气体分离膜，并且可以长时间浸入水中而不会龟裂和破裂。聚合物组合物也可以用作基底上的涂层，例如金属和陶瓷，或者可以用于纺丝纤维。还公开了用于形成这种聚合物组合物的前体。

7. 发明授权

US12128358B2 Methods of treating fluids using thermal gradient osmosis 有权
公开(公告)号：US12128358B2
公开(公告)日：2024-10-29
申请号：US17009360
申请日：2020-09-01
申请人： Battelle Energy Alliance, LLC
发明人： Aaron D. Wilson , Christopher J. Orme , John R. Klaehn , Birendra Adhikari , Frederick F. Stewart , Seth W. Snyder
IPC分类号： B01D53/22 , B01D61/00 , B01D69/02 , B01D69/10 , B01D69/12 , C02F1/44
CPC分类号： B01D61/005 , B01D53/228 , B01D61/002 , B01D69/02 , B01D69/107 , B01D69/1216 , C02F1/445 , B01D2311/103 , B01D2313/221 , B01D2313/903 , B01D2325/36 , B01D2325/38
摘要： A method of treating a fluid comprises introducing a feed fluid stream comprising multiple materials to first side of a semi-permeable membrane. A draw fluid stream having a higher temperature than the feed fluid stream is introduced to second, opposing side of the semi-permeable membrane to form a thermal gradient across the semi-permeable membrane. One or more of the multiple materials of the feed fluid stream is drawn through the semi-permeable membrane and into the draw fluid stream via thermal gradient osmosis. A fluid treatment system and a thermal gradient osmosis apparatus are also described.

8. 发明申请

US20220223932A1 METHODS OF RECOVERING ACTIVE MATERIALS FROM RECHARGEABLE BATTERIES, AND RELATED APPARATUSES 有权
公开(公告)号：US20220223932A1
公开(公告)日：2022-07-14
申请号：US17595967
申请日：2020-05-28
申请人： Battelle Energy Alliance, LLC
发明人： Joshua S. McNally , Luis A. Diaz Aldana , John R. Klaehn , Tedd E. Lister , David W, Reed
IPC分类号： H01M10/54 , H01M4/525 , H01M4/505 , H01M10/0525 , H01M10/44 , C22B7/00 , C22B3/00 , C22B26/12 , C22B26/22
摘要： A method of recovering active materials from a rechargeable battery comprises placing an active material of a rechargeable battery in a cathode chamber comprising a cathode of an electrochemical cell comprising the cathode chamber, an anode chamber comprising an anode, and a membrane separating the cathode chamber from the anode chamber, contacting the active material in the cathode chamber with an electrolyte comprising an acid, ferric ions, and ferrous ions, and dissolving at least one of lithium and cobalt from the active material into the electrolyte. Related apparatuses for recovering metals from active materials of rechargeable batteries are also disclosed.

9. 发明公开

US20240392409A1 METHODS OF SEPARATING METALS FROM A LITHIUM-ION BATTERY LEACHATE 审中-公开
公开(公告)号：US20240392409A1
公开(公告)日：2024-11-28
申请号：US18689835
申请日：2022-09-08
申请人： Battelle Energy Alliance, LLC
发明人： John R. Klaehn , Luis A. Diaz Aldana , Tedd E. Lister , Joshua S. McNally , Meng Shi , Daniel E. Molina Montes De Oca
IPC分类号： C22B3/00 , C22B7/00 , C22B26/12 , H01M10/0525 , H01M10/54
CPC分类号： C22B23/0484 , C22B7/007 , C22B23/0461 , C22B26/12 , H01M10/0525 , H01M10/54
摘要： A method of separating metals from a lithium-ion battery leachate includes obtaining a solution with iron, aluminum, nickel, and cobalt. Ammonium phosphate is added to the solution to adjust a pH of the solution to greater than or equal to about 3.00. After adjusting the pH of the solution, at least one phosphate—including iron phosphate and aluminum phosphate—is precipitated from the solution. Then, without adding a base to the solution, a crystallized nickel-cobalt Tutton's salt is precipitated from the solution.

10. 发明授权

US11925902B2 Thermally reflective membrane apparatuses, and related fluid treatment systems and methods 有权
公开(公告)号：US11925902B2
公开(公告)日：2024-03-12
申请号：US17009421
申请日：2020-09-01
申请人： Battelle Energy Alliance, LLC
发明人： John R. Klaehn , Christopher J. Orme , Aaron D. Wilson , Birendra Adhikari , Frederick F. Stewart , Seth W. Snyder
IPC分类号： B01D61/36 , B01D69/02 , B01D69/12
CPC分类号： B01D61/364 , B01D69/02 , B01D69/12 , B01D2313/22 , B01D2313/221 , B01D2313/36 , B01D2323/46 , B01D2325/22 , B01D2325/38
摘要： A thermally reflective membrane apparatus comprises a housing structure, and a thermally reflective membrane contained within the housing structure. The thermally reflective membrane comprises a semipermeable structure, and a porous, thermally reflective structure physically contacting the semipermeable structure. The porous, thermally reflective structure comprises discrete thermally reflective particles, and a binder material coupling the discrete thermally reflective particles to one another and the semipermeable structure. A fluid treatment system and method of treating a fluid are also described.

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