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1. 发明授权

US06642323B1 Process to produce a homogeneous polyethylene material 失效
标题翻译：生产均质聚乙烯材料的方法
公开(公告)号：US06642323B1
公开(公告)日：2003-11-04
申请号：US09674912
申请日：2000-11-08
申请人： Ole Jan Myhre , Bjarne Jansen , Auli Nummila-Pakarinen , Jari Äärilä
发明人： Ole Jan Myhre , Bjarne Jansen , Auli Nummila-Pakarinen , Jari Äärilä
IPC分类号： C08F234
CPC分类号： C08F10/00 , C08F10/02 , C08F110/02 , C08L23/06 , C08L2205/02 , Y10S526/901 , Y10S526/905 , C08F4/651 , C08F4/6555 , C08F2/001 , C08L2666/04 , C08F2500/12 , C08F2500/18 , C08F2500/19 , C08F2500/02 , C08F2500/01
摘要： The present invention concerns a process for producing homogeneous polyethylene compositions and processes for making high density, medium density and low density films therefrom. The process comprises carrying out the polymerization in the presence of an ethylene-polymerizing catalyst system in a multistage reaction sequence of successive polymerization stages, at least one of which is a loop polymerization stage, and at least one of which is a gas phase polymerization stage. According to the invention, said loop polymerization stage is operated using a diluent selected from the group of linear and branched C4-C6 hydrocarbons and/or mixtures thereof. The reactor sequence is operated with different amounts of hydrogen and comonomers to produce a high molecular weight portion in one of the polymerization stages and a low molecular weight portion in another, so as to provide bimodal polyethylene composition with a low molecular weight part having an MFR2 of 250 g/10 min or more. The obtained material is homogenous and the fines level in the process is low.
摘要翻译：本发明涉及用于制备均匀的聚乙烯组合物的方法和从其制备高密度，中密度和低密度的薄膜的方法。该方法包括在乙烯聚合催化剂体系的存在下，在连续聚合阶段的多阶段反应顺序中进行聚合，其中至少一个是环聚合阶段，并且其中至少一个是气相聚合反应阶段。根据本发明，所述环路聚合阶段使用选自直链和支链C 4 -C 6烃和/或其混合物的稀释剂进行操作。反应器序列用不同量的氢和共聚单体操作以在聚合阶段之一和另一个聚合阶段中的低分子量部分产生高分子量部分，以便提供具有MFR 2的低分子量部分的双峰聚乙烯组合物为250g / 10min以上。获得的材料是均匀的，并且该方法中的细粉水平低。

2. 发明授权

US06552150B1 Polymer films and a process for the production thereof 有权
标题翻译：聚合物膜及其生产方法
公开(公告)号：US06552150B1
公开(公告)日：2003-04-22
申请号：US09601366
申请日：2000-09-14
申请人： Auli Nummila-Pakarinen , Ole Jan Myhre , Bjarne Jansen
发明人： Auli Nummila-Pakarinen , Ole Jan Myhre , Bjarne Jansen
IPC分类号： C08F1002
CPC分类号： C08F10/02 , C08L23/04 , C08L23/0815 , C08L2205/02 , C08F2/001 , C08L2666/04
摘要： The present invention concerns a polyethylene composition particularly suitable for film blowing. The invention also concerns a process for the production thereof. The composition comprises a low molecular weight portion having a density of more than 960 kg/m3 and a high molecular weight portion. The polyethylene composition has a density of about 925-940 kg/m3 and a melt flow rate in the range of MFR21, from 5 to 40 g/10 min. A polyethylene film blown from the polyethylene composition exhibits a tensile strength at yield in transverse direction at least 15 MPa, a 1% secant modulus in machine direction at least 300 MPa and in transverse direction at least 400 MPa, and a dart drop of at least 5 g/&mgr;m.
摘要翻译：本发明涉及特别适用于吹膜的聚乙烯组合物。本发明还涉及其生产方法。组合物包含密度高于960kg / m 3的高分子量部分的低分子量部分。聚乙烯组合物的密度为约925-940kg / m 3，熔体流动速率在MFR 21范围内，为5至40g / 10min。从聚乙烯组合物吹出的聚乙烯薄膜在横向收缩率表现出拉伸强度至少为15MPa，机器方向上的1％割草模数至少为300MPa，横向为至少400MPa，并且至少具有飞镖滴 5g / mum。

3. 发明授权

US06562905B1 High density polyethylene compositions, a process for the production thereof and films prepared 有权
标题翻译：高密度聚乙烯组合物，其制备方法和制备的薄膜
公开(公告)号：US06562905B1
公开(公告)日：2003-05-13
申请号：US09647846
申请日：2000-11-09
申请人： Auli Nummila-Pakarinen , Ole Jan Myhre , Jarmo Lindroos , Solveig Johansson
发明人： Auli Nummila-Pakarinen , Ole Jan Myhre , Jarmo Lindroos , Solveig Johansson
IPC分类号： C08F1002
CPC分类号： C08F10/00 , C08L23/04 , C08L23/06 , C08L2205/02 , C08L2314/02 , Y10T428/13 , Y10T428/1334 , Y10T428/1345 , Y10T428/1352 , Y10T428/1397 , C08F4/6555 , C08L2666/04
摘要： The present invention concerns a bimodal film-making HDPE composition, a process for the preparation thereof, a film prepared thereof and a film-making process. The composition comprises at least one polyethylene component having a relatively low molecular weight and another polyethylene component having a relatively high molecular weight. The composition has a shear thinning index defined by the relationship: SHI5/300≦0.00014 &eegr;5kPa+78 wherein &eegr;5kPa is the complex viscosity at G*=5 Pa and SHI5/300 is the ratio of complex viscosity at G*=5 kPa to the complex viscosity at G*=300 kPa. By means of the invention it is possible to produce material for making HDPE blown films with good mechanical properties in a process where the whole range of PE products from LLD to HD can be produced.
摘要翻译：本发明涉及双峰成膜HDPE组合物，其制备方法，其制备的膜和成膜方法。组合物包含至少一种具有较低分子量的聚乙烯组分和另一种具有相对较高分子量的聚乙烯组分。该组合物具有由以下关系式定义的剪切稀化指数：其中η5kPa是G * = 5Pa时的复数粘度，SHI5 / 300是G * = 5kPa下的复数粘度与G * = 300kPa下的复数粘度的比率.By 在本发明的方法中，可以生产用于制造具有良好机械性能的HDPE吹塑薄膜的材料，其中可以生产从LLD到HD的全部范围的PE产品。

4. 发明授权

US06455642B1 Process for producing a homogeneous polyethylene material in the presence of a catalyst 有权
标题翻译：在催化剂存在下制备均匀的聚乙烯材料的方法
公开(公告)号：US06455642B1
公开(公告)日：2002-09-24
申请号：US09674854
申请日：2000-11-07
申请人： Ole Jan Myhre , Auli Nummila-Pakarinen , Jarmo Lindroos , Päivi Waldvogel , Thomas Garoff
发明人： Ole Jan Myhre , Auli Nummila-Pakarinen , Jarmo Lindroos , Päivi Waldvogel , Thomas Garoff
IPC分类号： C08F444
CPC分类号： C08F10/00 , C08F10/02 , C08F110/02 , C08L23/06 , C08L2205/02 , Y10S526/901 , Y10S526/905 , C08F4/651 , C08F4/6555 , C08F2/001 , C08L2666/04 , C08F2500/12 , C08F2500/18 , C08F2500/19 , C08F2500/02 , C08F2500/01
摘要： The present invention concerns a process for producing homogeneous polyethylene materials and processes for making high density, medium density and low density films therefrom. The process involves producing a polyethylene composition in a multistage reaction sequence of successive polymerization stages in the presence of an ethylene-polymerizing catalyst system. According to the invention, the process is carried out using an unsupported catalyst having magnesium and titanium as active constituents, in at least one loop polymerization stage and at least one gas phase polymerization stage and, operated with different amounts of hydrogen and comonomers to produce a high molecular weight portion in one of the polymerization stages and a low molecular weight portion in another so as to provide a polyethylene composition with the low molecular weight part having a MFR2 of 250 g/10 min or more. With this process it is possible to obtain homogeneous bimodal polyethylene material.
摘要翻译：本发明涉及用于制造均匀的聚乙烯材料的方法和由其制备高密度，中密度和低密度的薄膜的方法。该方法包括在乙烯聚合催化剂体系的存在下，在连续聚合阶段的多阶段反应顺序中制备聚乙烯组合物。根据本发明，该方法使用具有镁和钛作为活性成分的无载体催化剂，在至少一个环聚合阶段和至少一个气相聚合阶段中进行，并且用不同量的氢和共聚单体操作以产生在一个聚合阶段中的高分子量部分和另一个聚合阶段中的低分子量部分，从而提供具有250g / 10分钟以上的MFR 2的低分子量部分的聚乙烯组合物。通过该方法，可以获得均匀的双峰聚乙烯材料。

5. 发明申请

US20160009959A9 Adhesive Propylene Polymer Composition Suitable for Extrusion Coating of Paper Substrates 有权
公开(公告)号：US20160009959A9
公开(公告)日：2016-01-14
申请号：US14534721
申请日：2014-11-06
申请人： Erkki Laiho , Auli Nummila-Pakarinen , Elke Pachner , Hanna Rajala , Markku Sainio , Juha Yli-Peltola
发明人： Erkki Laiho , Auli Nummila-Pakarinen , Elke Pachner , Hanna Rajala , Markku Sainio , Juha Yli-Peltola
IPC分类号： C09J123/12
CPC分类号： C09J123/12 , A61B50/30 , A61B50/33 , A61B2050/3008 , B32B25/06 , B32B27/10 , B32B27/14 , B32B27/18 , B32B27/20 , B32B27/306 , B32B27/32 , B32B27/327 , B32B2255/12 , B32B2270/00 , B32B2307/30 , B32B2307/306 , B32B2307/412 , B32B2307/50 , B32B2323/10 , B32B2439/70 , B32B2439/80 , B32B2553/00 , C08L23/0853 , C08L51/06 , C08L2666/24 , C09J5/00 , C09J123/10 , C09J123/30 , C09J2423/10 , Y10T428/31808 , Y10T428/31895 , Y10T428/31899 , Y10T428/31902 , Y10T428/31906
摘要： Two-component adhesion composition suitable for extrusion coating paper substrates comprising: a) from 70 to 98 wt % of high melt strength polypropylene (A) with a branching index g′ of 0.9 or less; and b) from 2 to 30 wt % of a component (B) selected from the group of: (i) polypropylene homopolymer with high melt flow rate; or (ii) ethylene-vinyl acetate-based hot melt adhesive, and its use.

6. 发明申请

US20150065640A1 Adhesive Propylene Polymer Composition Suitable for Extrusion Coating of Paper Substrates 有权
标题翻译：适用于纸基材挤出涂层的胶粘剂丙烯聚合物组合物
公开(公告)号：US20150065640A1
公开(公告)日：2015-03-05
申请号：US14534721
申请日：2014-11-06
申请人： Erkki Laiho , Auli Nummila-Pakarinen , Elke Pachner , Hanna Rajala , Markku Sainio , Juha Yli-Peltola
发明人： Erkki Laiho , Auli Nummila-Pakarinen , Elke Pachner , Hanna Rajala , Markku Sainio , Juha Yli-Peltola
IPC分类号： C09J123/12
CPC分类号： C09J123/12 , A61B50/30 , A61B50/33 , A61B2050/3008 , B32B25/06 , B32B27/10 , B32B27/14 , B32B27/18 , B32B27/20 , B32B27/306 , B32B27/32 , B32B27/327 , B32B2255/12 , B32B2270/00 , B32B2307/30 , B32B2307/306 , B32B2307/412 , B32B2307/50 , B32B2323/10 , B32B2439/70 , B32B2439/80 , B32B2553/00 , C08L23/0853 , C08L51/06 , C08L2666/24 , C09J5/00 , C09J123/10 , C09J123/30 , C09J2423/10 , Y10T428/31808 , Y10T428/31895 , Y10T428/31899 , Y10T428/31902 , Y10T428/31906
摘要： Two-component adhesion composition suitable for extrusion coating paper substrates comprising: a) from 70 to 98 wt % of high melt strength polypropylene (A) with a branching index g′ of 0.9 or less; and b) from 2 to 30 wt % of a component (B) selected from the group of: (i) polypropylene homopolymer with high melt flow rate; or (ii) ethylene-vinyl acetate-based hot melt adhesive, and its use.
摘要翻译：适合用于挤出涂布纸基材的双组分粘合组合物，包括：a）70至98重量％的支链指数g'为0.9或更小的高熔体强度聚丙烯（A）; 和b）2至30重量％的选自以下的组分（B）：（i）具有高熔体流动速率的聚丙烯均聚物; 或（ii）乙烯 - 乙酸乙烯酯类热熔胶，及其用途。

7. 发明申请

US20070161739A1 Use 审中-公开
标题翻译：使用
公开(公告)号：US20070161739A1
公开(公告)日：2007-07-12
申请号：US11587470
申请日：2005-04-25
申请人： Irene Helland , Jorunn Nilsen , Ole Myhre , Auli Nummila-Pakarinen , Arja Lehtinen
发明人： Irene Helland , Jorunn Nilsen , Ole Myhre , Auli Nummila-Pakarinen , Arja Lehtinen
IPC分类号： C08K3/34
CPC分类号： C08K3/346 , C08L23/08
摘要： Use of talc as a nucleating agent for linear low density polyethylene formed from ethylene and at least one C4-10 alpha-olefin comonomer, said polyethylene having a density below 940 g/cm3.
摘要翻译：使用滑石作为由乙烯和至少一种C 4-10α-烯烃共聚单体形成的线性低密度聚乙烯的成核剂，所述聚乙烯的密度低于940g / cm 3， / SUP>。

8. 发明申请

US20150064487A1 Adhesive Propylene Polymer Composition Suitable for Extrusion Coating of Paper Substrates 有权
标题翻译：适用于纸基材挤出涂层的胶粘剂丙烯聚合物组合物
公开(公告)号：US20150064487A1
公开(公告)日：2015-03-05
申请号：US14534701
申请日：2014-11-06
申请人： Erkki Laiho , Auli Nummila-Pakarinen , Elke Pachner , Hanna Rajala , Markku Sainio , Juha Yli-Peltola
发明人： Erkki Laiho , Auli Nummila-Pakarinen , Elke Pachner , Hanna Rajala , Markku Sainio , Juha Yli-Peltola
IPC分类号： C09J123/30 , C09J5/00 , B32B27/10
CPC分类号： C09J123/12 , A61B50/30 , A61B50/33 , A61B2050/3008 , B32B25/06 , B32B27/10 , B32B27/14 , B32B27/18 , B32B27/20 , B32B27/306 , B32B27/32 , B32B27/327 , B32B2255/12 , B32B2270/00 , B32B2307/30 , B32B2307/306 , B32B2307/412 , B32B2307/50 , B32B2323/10 , B32B2439/70 , B32B2439/80 , B32B2553/00 , C08L23/0853 , C08L51/06 , C08L2666/24 , C09J5/00 , C09J123/10 , C09J123/30 , C09J2423/10 , Y10T428/31808 , Y10T428/31895 , Y10T428/31899 , Y10T428/31902 , Y10T428/31906
摘要： Two-component adhesion composition suitable for extrusion coating paper substrates which comprises: a) from 70 to 98 wt % of high melt strength polypropylene (A) with a branching index g′ of 0.9 or less; and b) from 2 to 30 wt % of a component (B) selected from the group consisting of: (i) maleic anhydride-modified polypropylene (MAPP); (ii) maleic anhydride-modified polypropylene wax; (iii) polypropylene homopolymer with high melt flow rate; or (iv) ethylene-vinyl acetate-based hot melt adhesive, and its use.
摘要翻译：适用于挤出涂布纸基材的双组分粘合组合物，其包括：a）70至98重量％的支链指数g'为0.9或更小的高熔体强度聚丙烯（A）; 和b）2至30重量％的选自以下的组分（B）：（i）马来酸酐改性聚丙烯（MAPP）; （ii）马来酸酐改性聚丙烯蜡; （iii）熔体流动速率高的聚丙烯均聚物; 或（iv）基于乙烯 - 乙酸乙烯酯的热熔粘合剂及其用途。

9. 发明授权

US08278393B2 Polyethylene blend component and blends containing the same 有权
标题翻译：聚乙烯共混物组分和含有它们的共混物
公开(公告)号：US08278393B2
公开(公告)日：2012-10-02
申请号：US12083640
申请日：2006-09-14
申请人： Auli Nummila-Pakarinen , Oivind Moen , Pertti Mikkola , Janne Jamsen
发明人： Auli Nummila-Pakarinen , Oivind Moen , Pertti Mikkola , Janne Jamsen
IPC分类号： C08L23/04 , C08L23/06 , C08F10/02
CPC分类号： C08F10/02 , C08F110/02 , C08F210/16 , C08L23/04 , C08L23/06 , C08L23/10 , C08L23/20 , C08L2666/06 , C08F2500/12 , C08F2500/17 , C08F2500/19 , C08F210/08
摘要： According to one aspect, the present invention relates to a low-density polyethylene having a melt index MFR2 of 2.5 to 10.0 g/10 min, a density of 910 to 935 kg/m3, and a dynamic viscosity η0.05 at a shear rate of 0.05 rad/s and a dynamic viscosity η300 at a shear rate of 300 rad/s which satisfy the following relationship: η300≦108 Pa*s+0.0253*η0.05. According to a second aspect, the present invention relates to a low-density polyethylene having a melt index MFR2 of 2.5 to 10.0 g/10 min, a density of 910 to 935 kg/m3, and a phase shift δ0.5 at a frequency of 0.5 rad/s and a phase shift δ300 at a frequency of 300 rad/s, which satisfy the following relationship: tan δ300≧0.45+0.164*tan δ0.5.
摘要翻译：一方面，本发明涉及熔体指数MFR 2为2.5〜10.0g / 10min，密度为910〜935kg / m 3的动态粘度和剪切速率为0.05的低密度聚乙烯在300rad / s的剪切速率下为0.05rad / s，动态粘度为300，满足以下关系：＆eegr; 300＆nlE; 108Pa * s + 0.0253 *＆eegr; 0.05。根据第二方面，本发明涉及熔体指数MFR 2为2.5〜10.0g / 10min，密度为910〜935kg / m 3，频率相位δ0.5的低密度聚乙烯为0.5rad / s，相位偏移δ300为300rad / s，满足以下关系：tanδ300≥0.45+ 0.164 *tanδ0.5。

10. 发明申请

US20110111243A1 Adhesive Propylene Polymer Composition Suitable for Extrusion Coating of Paper Substrates 审中-公开
公开(公告)号：US20110111243A1
公开(公告)日：2011-05-12
申请号：US12990026
申请日：2009-08-25
申请人： Erkki Laiho , Auli Nummila-Pakarinen , Elke Pachner , Hanna Rajala , Markku Sainio , Juha Yli-Peltola
发明人： Erkki Laiho , Auli Nummila-Pakarinen , Elke Pachner , Hanna Rajala , Markku Sainio , Juha Yli-Peltola
IPC分类号： B32B27/10 , C08K5/1539 , C09J137/00
CPC分类号： C09J123/12 , A61B50/30 , A61B50/33 , A61B2050/3008 , B32B25/06 , B32B27/10 , B32B27/14 , B32B27/18 , B32B27/20 , B32B27/306 , B32B27/32 , B32B27/327 , B32B2255/12 , B32B2270/00 , B32B2307/30 , B32B2307/306 , B32B2307/412 , B32B2307/50 , B32B2323/10 , B32B2439/70 , B32B2439/80 , B32B2553/00 , C08L23/0853 , C08L51/06 , C08L2666/24 , C09J5/00 , C09J123/10 , C09J123/30 , C09J2423/10 , Y10T428/31808 , Y10T428/31895 , Y10T428/31899 , Y10T428/31902 , Y10T428/31906
摘要： Two-component adhesion composition suitable for extrusion coating paper substrates which comprises a) from 70 to 98 wt % of high melt strength polypropylene (A) with a branching index g′ of 0.9 or less and b) from 2 to 30 wt % of a component (B) selected from the group of (i) maleic anhydride-modified polypropylene (MAPP) (ii) maleic anhydride-modified polypropylene wax (iii) polypropylene homopolymer with high melt flow rate or (iv) ethylene-vinyl acetate-based hot melt adhesive and its use.

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