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1. 发明授权

US09249091B2 Post-treated sulfurized salt of an alkyl-substituted hydroxyaromatic composition 有权
标题翻译：经后处理的烷基取代的羟基芳族组合物的硫化盐
公开(公告)号：US09249091B2
公开(公告)日：2016-02-02
申请号：US13727892
申请日：2012-12-27
申请人： Andrew R. Gibbs , Curtis Campbell
发明人： Andrew R. Gibbs , Curtis Campbell
IPC分类号： C07C307/00 , C10M159/16 , C07G99/00
CPC分类号： C07C307/00 , C07G17/00 , C10M159/16 , C10M2217/043 , C10N2230/64 , C10N2240/04 , C10N2240/08 , C10N2240/10 , C10N2240/102 , C10N2240/30 , C10N2250/10 , C10N2260/10 , C10N2210/02
摘要： Disclosed herein is a post-treated salt of a sulfurized alkyl-substituted hydroxyaromatic composition which is a reaction product of (a) a salt of a sulfurized alkyl-substituted hydroxyaromatic composition, wherein the alkyl-substituted hydroxyaromatic compound is derived from alkylation of a hydroxyaromatic compound with one or more olefins comprising C9 to C18 oligomers of monomers selected from propylene, butylene or mixtures thereof, (b) a source of an aldehyde and (c) a primary and/or secondary monoamine compound having at least one active hydrogen. The post-treated salt of a sulfurized alkylhydroxyaromatic composition disclosed herein has a reduced content of unsulfurized alkyl-substituted hydroxyaromatic compound and its unsulfurized metal salt as compared to the content, by combined mass, of the unsulfurized alkyl-substituted hydroxyaromatic compound and its unsulfurized metal salt present in the non-post-treated salt of a sulfurized alkyl-substituted hydroxyaromatic composition.
摘要翻译：本文公开了硫化烷基取代的羟基芳族组合物的后处理盐，其是（a）硫化烷基取代的羟基芳族组合物的盐的反应产物，其中烷基取代的羟基芳族化合物衍生自羟基芳族化合物的烷基化包含选自丙烯，丁烯或其混合物的单体的C 9至C 18低聚物的一种或多种烯烃的化合物，（b）醛源和（c）具有至少一个活性氢的伯和/或仲单胺化合物。本文公开的硫化烷基羟基芳族化合物的后处理盐与未硫化的烷基取代的羟基芳族化合物及其未硫化金属的组合质量相比，未硫化的烷基取代的羟基芳族化合物及其未硫化金属盐的含量降低存在于硫化烷基取代的羟基芳族组合物的非后处理盐中的盐。

2. 发明申请

US20130165359A1 POST-TREATED SULFURIZED SALT OF AN ALKYL-SUBSTITUTED HYDROXYAROMATIC COMPOSITION 有权
标题翻译：烷基取代羟基化合物的后处理硫化盐
公开(公告)号：US20130165359A1
公开(公告)日：2013-06-27
申请号：US13727892
申请日：2012-12-27
申请人： Andrew R. Gibbs , Curtis Campbell
发明人： Andrew R. Gibbs , Curtis Campbell
IPC分类号： C07C307/00
CPC分类号： C07C307/00 , C07G17/00 , C10M159/16 , C10M2217/043 , C10N2230/64 , C10N2240/04 , C10N2240/08 , C10N2240/10 , C10N2240/102 , C10N2240/30 , C10N2250/10 , C10N2260/10 , C10N2210/02
摘要： Disclosed herein is a post-treated salt of a sulfurized alkyl-substituted hydroxyaromatic composition which is a reaction product of (a) a salt of a sulfurized alkyl-substituted hydroxyaromatic composition, wherein the alkyl-substituted hydroxyaromatic compound is derived from alkylation of a hydroxyaromatic compound with one or more olefins comprising C9 to C18 oligomers of monomers selected from propylene, butylene or mixtures thereof, (b) a source of an aldehyde and (c) a primary and/or secondary monoamine compound having at least one active hydrogen. The post-treated salt of a sulfurized alkylhydroxyaromatic composition disclosed herein has a reduced content of unsulfurized alkyl-substituted hydroxyaromatic compound and its unsulfurized metal salt as compared to the content, by combined mass, of the unsulfurized alkyl-substituted hydroxyaromatic compound and its unsulfurized metal salt present in the non-post-treated salt of a sulfurized alkyl-substituted hydroxyaromatic composition.
摘要翻译：本文公开了硫化烷基取代的羟基芳族组合物的后处理盐，其是（a）硫化烷基取代的羟基芳族组合物的盐的反应产物，其中烷基取代的羟基芳族化合物衍生自羟基芳族化合物的烷基化包含选自丙烯，丁烯或其混合物的单体的C 9至C 18低聚物的一种或多种烯烃的化合物，（b）醛源和（c）具有至少一个活性氢的伯和/或仲单胺化合物。本文公开的硫化烷基羟基芳族化合物的后处理盐与未硫化的烷基取代的羟基芳族化合物及其未硫化金属的组合质量相比，未硫化的烷基取代的羟基芳族化合物及其未硫化金属盐的含量降低存在于硫化烷基取代的羟基芳族组合物的非后处理盐中的盐。

3. 发明申请

US20050059560A1 Process for the preparation of stabilized polyalkenyl sulfonic acids 审中-公开
标题翻译：制备稳定的聚链烯基磺酸的方法
公开(公告)号：US20050059560A1
公开(公告)日：2005-03-17
申请号：US10660948
申请日：2003-09-12
申请人： Jesse Meyer , Richard Nelson , William King , James Harrison , Curtis Campbell , Eugene Spala
发明人： Jesse Meyer , Richard Nelson , William King , James Harrison , Curtis Campbell , Eugene Spala
IPC分类号： C07C303/42 , C07C303/02 , C07C303/32 , C07C309/20 , C08F8/44 , C10M135/10 , C10M151/04 , C10M159/24 , C10M177/00 , C10N10/04 , C10N70/00 , C07C39/20
CPC分类号： C10M151/04 , C08F8/44 , C10M135/10 , C10M159/24 , C10M2219/044 , C10M2219/046 , C10M2221/04 , C10N2210/02 , C10N2230/04 , C10N2240/042 , C10N2240/08 , C10N2240/10
摘要： An improved process for making stabilized polyalkenyl sulfonic acids, whereby the product resulting from the reaction between a polyalkene and sulfur trioxide is stabilized by neutralizing with a neutralizing agent prior to storage or further processing. Neutralization at this point in the process results in polyalkenyl sulfonic acid that is stable and has a decreased amount of sultones.
摘要翻译：制备稳定的聚链烯基磺酸的改进方法，其中由聚烯烃和三氧化硫之间的反应产生的产物通过在储存或进一步加工之前用中和剂中和来稳定。该过程中的中和过程导致稳定且具有降低量的磺内酯的聚链烯基磺酸。

4. 发明申请

US20070049508A1 Linear alkylphenol derived detergent substantially free of endocrine disruptive chemicals 有权
标题翻译：直链烷基酚衍生的洗涤剂基本上不含内分泌破坏性化学物质
公开(公告)号：US20070049508A1
公开(公告)日：2007-03-01
申请号：US11218390
申请日：2005-09-01
申请人： Peter Stonebraker , Curtis Campbell , Linda Roberts
发明人： Peter Stonebraker , Curtis Campbell , Linda Roberts
IPC分类号： C10M129/10
CPC分类号： C10M159/22 , C10M135/02 , C10M2207/023 , C10M2207/027 , C10M2207/028 , C10M2207/144 , C10M2207/146 , C10M2219/087 , C10M2219/089 , C10N2210/01 , C10N2210/02 , C10N2220/027 , C10N2230/64
摘要： Disclosed is a lubricating oil composition displaying reduced endocrine disruption response, comprising a major amount of an oil of lubricating viscosity; and a detergent comprising an unsulfurized alkali or alkaline earth metal salt of a reaction product of (1) an olefin having at least 10 carbon atoms, wherein greater than 80 mole % of the olefin is a linear C20-C30 n-alpha olefin, wherein less than 10 mole % of the olefin is a linear olefin of less than 20 carbon atoms, and wherein less than 5 mole % of the olefin is branched chain olefin of 18 carbons or less, and (2) a hydroxyaromatic compound.
摘要翻译：公开了显示减少的内分泌干扰反应的润滑油组合物，其包含主要量的润滑粘度的油; 和包含（1）具有至少10个碳原子的烯烃的反应产物的未硫化碱金属或碱土金属盐的洗涤剂，其中大于80摩尔％的烯烃为直链C 20 -C 30 O-α-烯烃，其中小于10摩尔％的烯烃是小于20个碳原子的直链烯烃，并且其中小于5摩尔％的烯烃是支链烯烃 18个碳以下，和（2）羟基芳族化合物。

5. 发明申请

US20140142347A1 PROCESS FOR PREPARING A SALT OF A SULFURIZED ALKYL-SUBSTITUTED HYDROXYAROMATIC COMPOSITION 有权
标题翻译：制备磺化烷基取代羟基芳族化合物的盐的方法
公开(公告)号：US20140142347A1
公开(公告)日：2014-05-22
申请号：US13682172
申请日：2012-11-20
申请人： Cedrick Mahieux , Richard Dutta , Curtis Campbell
发明人： Cedrick Mahieux , Richard Dutta , Curtis Campbell
IPC分类号： C07C37/86
CPC分类号： C10M159/20 , C10M2219/089 , C10N2230/04 , C10N2230/64 , C10N2270/00
摘要： Disclosed herein is a process for preparing a salt of a sulfurized alkyl-substituted hydroxyaromatic composition having a reduced content of unsulfurized alkyl-substituted hydroxyaromatic compound and its unsulfurized metal salt. The process involves the steps of: (a) providing a composition comprising (i) a salt of a sulfurized alkyl-substituted hydroxyaromatic compound; (ii) an unsulfurized alkyl-substituted hydroxyaromatic compound and (iii) an unsulfurized metal salt of the alkyl-substituted hydroxyaromatic compound; wherein the alkyl-substituted hydroxyaromatic compound is derived from alkylation of a hydroxyaromatic compound with one or more olefins comprising C9 to C18 oligomers of monomers selected from propylene, butylene or mixtures thereof; (b) protonating the unsulfurized metal salt of the alkyl-substituted hydroxyaromatic compound with an effective amount of an acidic compound capable of protonating the unsulfurized metal salt of the alkyl-substituted hydroxyaromatic compound; and (c) removing the unsulfurized alkyl-substituted hydroxyaromatic compound and the protonated unsulfurized metal salt of the alkyl-substituted hydroxyaromatic compound from the composition.
摘要翻译：本文公开了一种制备具有降低的未硫化烷基取代的羟基芳族化合物和其未硫化金属盐含量降低的硫化烷基取代的羟基芳族组合物的盐的方法。该方法包括以下步骤：（a）提供包含（i）硫化烷基取代的羟基芳族化合物的盐的组合物; （ii）未硫化烷基取代的羟基芳族化合物和（iii）烷基取代的羟基芳族化合物的未硫化金属盐; 其中烷基取代的羟基芳族化合物衍生自羟基芳族化合物与一种或多种烯烃的烷基化，所述烯烃包含选自丙烯，丁烯或其混合物的单体的C 9至C 18低聚物; （b）用有效量的能够使烷基取代的羟基芳族化合物的未硫化金属盐进行质子化的酸性化合物使烷基取代的羟基芳族化合物的未硫化金属盐质子化; 和（c）从组合物中除去未硫化烷基取代的羟基芳族化合物和烷基取代的羟基芳族化合物的质子化未硫化金属盐。

6. 发明申请

US20070027057A1 Low sulfur metal detergent-dispersants 有权
标题翻译：低硫金属洗涤剂分散剂
公开(公告)号：US20070027057A1
公开(公告)日：2007-02-01
申请号：US11192757
申请日：2005-07-29
申请人： Jean-Louis Le Coent , Jeffrey Toman , Curtis Campbell
发明人： Jean-Louis Le Coent , Jeffrey Toman , Curtis Campbell
IPC分类号： C11D3/20 , C07C65/00
CPC分类号： C10M159/22 , C10M2207/262 , C10M2219/089 , C10N2210/01 , C10N2210/02 , C10N2230/12 , C10N2230/52 , C10N2270/00
摘要： A process for preparing alkylhydroxybenzoate detergent-dispersant additives having low sulfur content and high TBN is described. The alkali metal alkylhydroxylbenzoate, alkaline earth metal alkylhydroxybenzoate and overbased alkaline earth metal alkylhydroxybenzoate reaction products described have a sulfur content in the range of from about 0.1 to 1.2 wt % are effective anti-corrosive detergent-dispersant additives in lubricating oil compositions.
摘要翻译：描述了制备具有低硫含量和高TBN的烷基羟基苯甲酸盐洗涤剂 - 分散剂添加剂的方法。碱式金属烷基羟基苯甲酸酯，碱土金属烷基羟基苯甲酸酯和高碱性碱土金属烷基羟基苯甲酸酯反应产物的硫含量在约0.1至1.2重量％范围内是润滑油组合物中有效的防腐蚀洗涤剂 - 分散剂添加剂。

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