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    • 1. 发明授权
    • Spectrometer with validation cell
    • 光谱仪带有验证单元
    • US08358417B2
    • 2013-01-22
    • US13026921
    • 2011-02-14
    • Alfred FeitischLutz KellerXiang LiuMathias SchrempelKeith Benjamin Helbley
    • Alfred FeitischLutz KellerXiang LiuMathias SchrempelKeith Benjamin Helbley
    • G01J3/28G01N21/00
    • G01J3/28G01J3/42G01N21/031G01N21/274G01N21/31G01N21/3504G01N21/3518G01N21/39G01N2021/399
    • A valid state of an analytical system that includes a light source and a detector can be verified by determining that deviation of first light intensity data quantifying a first intensity of light received at the detector from the light source after the light has passed at least once through each of a reference gas in a validation cell and a zero gas from a stored data set does not exceed a pre-defined threshold deviation. The stored data set can represent at least one previous measurement collected during a previous instrument validation process performed on the analytical system. The reference gas can include a known amount of an analyte. A concentration of the analyte in a sample gas can be determined by correcting second light intensity data quantifying a second intensity of the light received at the detector after the light passes at least once through each of the reference gas in the validation cell and a sample gas containing an unknown concentration of the analyte compound. Related systems, methods, and articles of manufacture are also described.
    • 包括光源和检测器的分析系统的有效状态可以通过确定在光已经通过至少一次通过之后量化在检测器处接收的第一光强度的光的第一光强度数据与来自光源的偏差 验证单元中的参考气体和来自存储的数据组的零气体中的每一个不超过预定义的阈值偏差。 存储的数据集可以表示在分析系统上执行的先前的仪器验证过程期间收集的至少一个以前的测量。 参考气体可以包括已知量的分析物。 样品气体中分析物的浓度可以通过校正第二光强度数据来确定,该第二光强度数据在光通过至少一次通过验证单元中的每个参考气体之后,量化在检测器处接收的光的第二强度,并且样品气体 含有未知浓度的分析物。 还描述了相关系统,方法和制品。
    • 4. 发明申请
    • SPECTROMETER WITH VALIDATION CELL
    • 带有验证单元的光谱仪
    • US20110299076A1
    • 2011-12-08
    • US13026921
    • 2011-02-14
    • ALFRED FEITISCHLutz KellerXiang LiuMathias Schrempel
    • ALFRED FEITISCHLutz KellerXiang LiuMathias Schrempel
    • G01J3/28
    • G01J3/28G01J3/42G01N21/031G01N21/274G01N21/31G01N21/3504G01N21/3518G01N21/39G01N2021/399
    • A valid state of an analytical system that includes a light source and a detector can be verified by determining that deviation of first light intensity data quantifying a first intensity of light received at the detector from the light source after the light has passed at least once through each of a reference gas in a validation cell and a zero gas from a stored data set does not exceed a pre-defined threshold deviation. The stored data set can represent at least one previous measurement collected during a previous instrument validation process performed on the analytical system. The reference gas can include a known amount of an analyte. A concentration of the analyte in a sample gas can be determined by correcting second light intensity data quantifying a second intensity of the light received at the detector after the light passes at least once through each of the reference gas in the validation cell and a sample gas containing an unknown concentration of the analyte compound. Related systems, methods, and articles of manufacture are also described.
    • 包括光源和检测器的分析系统的有效状态可以通过确定在光已经通过至少一次通过之后量化在检测器处接收的第一光强度的光的第一光强度数据与来自光源的偏差 验证单元中的参考气体和来自存储的数据组的零气体中的每一个不超过预定义的阈值偏差。 存储的数据集可以表示在分析系统上执行的先前的仪器验证过程期间收集的至少一个以前的测量。 参考气体可以包括已知量的分析物。 样品气体中分析物的浓度可以通过校正第二光强度数据来确定,该第二光强数据在光通过至少一次通过验证单元中的每个参考气体之后,量化在检测器处接收的光的第二强度,并且样品气体 含有未知浓度的分析物。 还描述了相关系统,方法和制品。
    • 6. 发明申请
    • OPTICAL REFLECTORS FOR SPECTROMETER GAS CELLS
    • 用于光谱仪气体细胞的光反射器
    • US20140160474A1
    • 2014-06-12
    • US13712923
    • 2012-12-12
    • Lutz KellerAlfred FeitischPeter ScottMathias SchrempelNathan St. John
    • Lutz KellerAlfred FeitischPeter ScottMathias SchrempelNathan St. John
    • G01N21/03
    • G01N21/0303G01J3/42G01N21/031G01N21/09G01N21/3504
    • A spectrometer cell can include a spacer, at least one end cap, and at least one mirror with a reflective surface. The end cap can be positioned proximate to a first contact end of the spacer such that the end cap and spacer at least partially enclose an internal volume of the spectrometer cell. The mirror can be secured in place by a mechanical attachment that includes attachment materials that are chemically inert to at least one reactive gas compound. The mechanical attachment can hold an optical axis of the reflective surface in a fixed orientation relative to other components of the spectrometer cell and or a spectrometer device that comprises the spectrometer cell. The mirror can optionally be constructed of a material such as stainless steel, ceramic, or the like. Related methods, articles of manufacture, systems, and the like are described.
    • 光谱仪单元可以包括间隔物,至少一个端盖和至少一个具有反射表面的反射镜。 端盖可以定位成靠近隔离物的第一接触端,使得端盖和间隔件至少部分地包围光谱仪单元的内部体积。 镜子可以通过机械附件固定在适当的位置,该机械附件包括对至少一种反应性气体化合物具有化学惰性的附着材料。 机械附件可以将反射表面的光轴相对于分光计单元的其他部件和包括光谱仪单元的光谱仪装置固定在一定方向。 镜子可以任意地由诸如不锈钢,陶瓷等的材料构成。 描述了相关方法,制品,系统等。