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1. 发明申请

US20100139823A1 PYROPHORIC METAL-CARBON FOAM COMPOSITES AND METHODS OF MAKING THE SAME 有权
标题翻译： PORROPHORIC金属碳泡沫复合材料及其制备方法
公开(公告)号：US20100139823A1
公开(公告)日：2010-06-10
申请号：US12329437
申请日：2008-12-05
申请人： Alexander E. Gash , Joe H. Satcher, JR. , Randall L. Simpson , Theodore F. Baumann , Marcus A. Worsley
发明人： Alexander E. Gash , Joe H. Satcher, JR. , Randall L. Simpson , Theodore F. Baumann , Marcus A. Worsley
IPC分类号： C06B45/04
CPC分类号： C06C15/00 , C06B45/00
摘要： A method for creating a pyrophoric material according to one embodiment includes thermally activating a carbon foam for creating micropores therein; contacting the activated carbon foam with a liquid solution comprising a metal salt for depositing metal ions in the carbon foam; and reducing the metal ions in the foam to metal particles. A pyrophoric material in yet another embodiment includes a pyrophoric metal-carbon foam composite comprising a carbon foam having micropores and mesopores and a surface area of greater than or equal to about 2000 m2/g, and metal particles in the pores of the carbon foam. Additional methods and materials are also disclosed.
摘要翻译：根据一个实施例的用于产生自燃材料的方法包括热活化碳泡沫以在其中产生微孔; 使活性炭泡沫与包含用于在碳泡沫中沉积金属离子的金属盐的液体溶液接触; 并将泡沫中的金属离子还原成金属颗粒。在另一个实施方案中的自燃材料包括自发金属 - 碳泡沫复合材料，其包含具有微孔和介孔的碳泡沫，并且表面积大于或等于约2000m 2 / g，以及碳泡沫的孔中的金属颗粒。还公开了附加的方法和材料。

2. 发明授权

US08172964B2 Pyrophoric metal-carbon foam composites and methods of making the same 有权
标题翻译：发火金属碳泡沫复合材料及其制备方法
公开(公告)号：US08172964B2
公开(公告)日：2012-05-08
申请号：US12329437
申请日：2008-12-05
申请人： Alexander E. Gash , Joe H. Satcher, Jr. , Randall L. Simpson , Theodore F. Baumann , Marcus A. Worsley
发明人： Alexander E. Gash , Joe H. Satcher, Jr. , Randall L. Simpson , Theodore F. Baumann , Marcus A. Worsley
IPC分类号： C06B45/00 , C06B45/04 , C06B27/00 , D03D23/00 , D03D43/00
CPC分类号： C06C15/00 , C06B45/00
摘要： A method for creating a pyrophoric material according to one embodiment includes thermally activating a carbon foam for creating micropores therein; contacting the activated carbon foam with a liquid solution comprising a metal salt for depositing metal ions in the carbon foam; and reducing the metal ions in the foam to metal particles. A pyrophoric material in yet another embodiment includes a pyrophoric metal-carbon foam composite comprising a carbon foam having micropores and mesopores and a surface area of greater than or equal to about 2000 m2/g, and metal particles in the pores of the carbon foam. Additional methods and materials are also disclosed.
摘要翻译：根据一个实施例的用于产生自燃材料的方法包括热活化碳泡沫以在其中产生微孔; 使活性炭泡沫与包含用于在碳泡沫中沉积金属离子的金属盐的液体溶液接触; 并将泡沫中的金属离子还原成金属颗粒。在另一个实施方案中的自燃材料包括自发金属 - 碳泡沫复合材料，其包含具有微孔和介孔的碳泡沫，并且表面积大于或等于约2000m 2 / g，以及碳泡沫的孔中的金属颗粒。还公开了附加的方法和材料。

3. 发明授权

US08664143B2 High surface area, electrically conductive nanocarbon-supported metal oxide 有权
标题翻译：高表面积，导电性纳米碳载体金属氧化物
公开(公告)号：US08664143B2
公开(公告)日：2014-03-04
申请号：US13281185
申请日：2011-10-25
申请人： Marcus A. Worsley , Thomas Yong-Jin Han , Joshua D. Kuntz , Octavio Cervantes , Alexander E. Gash , Theodore F. Baumann , Joe H. Satcher, Jr.
发明人： Marcus A. Worsley , Thomas Yong-Jin Han , Joshua D. Kuntz , Octavio Cervantes , Alexander E. Gash , Theodore F. Baumann , Joe H. Satcher, Jr.
IPC分类号： B01J13/00 , B01J21/18 , B01J23/00 , B01J23/02 , B01J23/06 , B01J23/40 , B01J23/74 , B01F3/08 , C08J3/02 , C08L91/08 , C08L95/00 , C09D195/00 , C09K3/00 , B01D21/01
CPC分类号： H01B1/08 , B01J21/06 , B01J21/063 , B01J21/185 , B01J35/004 , B01J37/084 , B82Y30/00 , C04B35/532 , C04B35/624 , C04B35/62655 , C04B35/83 , C04B2235/3232 , C04B2235/3418 , C04B2235/3826 , C04B2235/3856 , C04B2235/3886 , C04B2235/3895 , C04B2235/441 , C04B2235/46 , C04B2235/5288 , C04B2235/606 , C04B2235/616 , C04B2235/652 , C04B2235/77 , C04B2235/80 , H01B1/06 , H01G11/36 , H01G11/46 , H01G11/86 , H01M4/48 , H01M4/50 , H01M4/52 , H01M4/625 , Y02E60/13
摘要： A metal oxide-carbon composite includes a carbon aerogel with an oxide overcoat. The metal oxide-carbon composite is made by providing a carbon aerogel, immersing the carbon aerogel in a metal oxide sol under a vacuum, raising the carbon aerogel with the metal oxide sol to atmospheric pressure, curing the carbon aerogel with the metal oxide sol at room temperature, and drying the carbon aerogel with the metal oxide sol to produce the metal oxide-carbon composite. The step of providing a carbon aerogel can provide an activated carbon aerogel or provide a carbon aerogel with carbon nanotubes that make the carbon aerogel mechanically robust.
摘要翻译：金属氧化物 - 碳复合材料包括具有氧化物外涂层的碳气凝胶。金属氧化物 - 碳复合材料通过提供碳气凝胶制成，将碳气凝胶在真空下浸入金属氧化物溶胶中，将金属氧化物溶胶的碳气凝胶升高至大气压，用金属氧化物溶胶固化碳气凝胶室温下，用金属氧化物溶胶干燥碳气凝胶，制成金属氧化物 - 碳复合材料。提供碳气凝胶的步骤可以提供活性炭气凝胶或提供碳气凝胶与碳纳米管，使碳气凝胶机械坚固。

4. 发明申请

US20120122652A1 HIGH SURFACE AREA, ELECTRICALLY CONDUCTIVE NANOCARBON-SUPPORTED METAL OXIDE 有权
标题翻译：高表面积，电导电性纳米支撑金属氧化物
公开(公告)号：US20120122652A1
公开(公告)日：2012-05-17
申请号：US13281185
申请日：2011-10-25
申请人： Marcus A. WORSLEY , Thomas Yong-Jin Han , Joshua D. Kuntz , Octavio Cervantes , Alexander E. Gash , Theodore F. Baumann , Joe H. Satcher, JR.
发明人： Marcus A. WORSLEY , Thomas Yong-Jin Han , Joshua D. Kuntz , Octavio Cervantes , Alexander E. Gash , Theodore F. Baumann , Joe H. Satcher, JR.
IPC分类号： B01J21/18 , B82Y30/00 , B82Y40/00
CPC分类号： H01B1/08 , B01J21/06 , B01J21/063 , B01J21/185 , B01J35/004 , B01J37/084 , B82Y30/00 , C04B35/532 , C04B35/624 , C04B35/62655 , C04B35/83 , C04B2235/3232 , C04B2235/3418 , C04B2235/3826 , C04B2235/3856 , C04B2235/3886 , C04B2235/3895 , C04B2235/441 , C04B2235/46 , C04B2235/5288 , C04B2235/606 , C04B2235/616 , C04B2235/652 , C04B2235/77 , C04B2235/80 , H01B1/06 , H01G11/36 , H01G11/46 , H01G11/86 , H01M4/48 , H01M4/50 , H01M4/52 , H01M4/625 , Y02E60/13
摘要： A metal oxide-carbon composite includes a carbon aerogel with an oxide overcoat. The metal oxide-carbon composite is made by providing a carbon aerogel, immersing the carbon aerogel in a metal oxide sol under a vacuum, raising the carbon aerogel with the metal oxide sol to atmospheric pressure, curing the carbon aerogel with the metal oxide sol at room temperature, and drying the carbon aerogel with the metal oxide sol to produce the metal oxide-carbon composite. The step of providing a carbon aerogel can provide an activated carbon aerogel or provide a carbon aerogel with carbon nanotubes that make the carbon aerogel mechanically robust.
摘要翻译：金属氧化物 - 碳复合材料包括具有氧化物外涂层的碳气凝胶。金属氧化物 - 碳复合材料通过提供碳气凝胶制成，将碳气凝胶在真空下浸入金属氧化物溶胶中，将金属氧化物溶胶的碳气凝胶升高至大气压，用金属氧化物溶胶固化碳气凝胶室温下，用金属氧化物溶胶干燥碳气凝胶，制成金属氧化物 - 碳复合材料。提供碳气凝胶的步骤可以提供活性炭气凝胶或提供碳气凝胶与碳纳米管，使碳气凝胶机械坚固。

5. 发明申请

US20100190639A1 HIGH SURFACE AREA, ELECTRICALLY CONDUCTIVE NANOCARBON-SUPPORTED METAL OXIDE 审中-公开
标题翻译：高表面积，电导电性纳米支撑金属氧化物
公开(公告)号：US20100190639A1
公开(公告)日：2010-07-29
申请号：US12694425
申请日：2010-01-27
申请人： Marcus A. Worsley , Thomas Yong-Jin Han , Joshua D. Kuntz , Octavio Cervantes , Alexander E. Gash , Theodore F. Baumann , Joe H. Satcher, JR.
发明人： Marcus A. Worsley , Thomas Yong-Jin Han , Joshua D. Kuntz , Octavio Cervantes , Alexander E. Gash , Theodore F. Baumann , Joe H. Satcher, JR.
IPC分类号： B01J21/18 , B01J23/74 , B01J23/72 , B01J23/06
CPC分类号： H01B1/08 , B01J21/06 , B01J21/063 , B01J21/185 , B01J35/004 , B01J37/084 , B82Y30/00 , C04B35/532 , C04B35/624 , C04B35/62655 , C04B35/83 , C04B2235/3232 , C04B2235/3418 , C04B2235/3826 , C04B2235/3856 , C04B2235/3886 , C04B2235/3895 , C04B2235/441 , C04B2235/46 , C04B2235/5288 , C04B2235/606 , C04B2235/616 , C04B2235/652 , C04B2235/77 , C04B2235/80 , H01B1/06 , H01G11/36 , H01G11/46 , H01G11/86 , H01M4/48 , H01M4/50 , H01M4/52 , H01M4/625 , Y02E60/13
摘要： A metal oxide-carbon composite includes a carbon aerogel with an oxide overcoat. The metal oxide-carbon composite is made by providing a carbon aerogel, immersing the carbon aerogel in a metal oxide sol under a vacuum, raising the carbon aerogel with the metal oxide sol to atmospheric pressure, curing the carbon aerogel with the metal oxide sol at room temperature, and drying the carbon aerogel with the metal oxide sol to produce the metal oxide-carbon composite. The step of providing a carbon aerogel can provide an activated carbon aerogel or provide a carbon aerogel with carbon nanotubes that make the carbon aerogel mechanically robust.
摘要翻译：金属氧化物 - 碳复合材料包括具有氧化物外涂层的碳气凝胶。金属氧化物 - 碳复合材料通过提供碳气凝胶制成，将碳气凝胶在真空下浸入金属氧化物溶胶中，将金属氧化物溶胶的碳气凝胶升高至大气压，用金属氧化物溶胶固化碳气凝胶室温下，用金属氧化物溶胶干燥碳气凝胶，制成金属氧化物 - 碳复合材料。提供碳气凝胶的步骤可以提供活性炭气凝胶或提供碳气凝胶与碳纳米管，使碳气凝胶机械坚固。

6. 发明授权

US07291653B2 Preparation of hydrophobic organic aeorgels 失效
标题翻译：疏水性有机物的制备
公开(公告)号：US07291653B2
公开(公告)日：2007-11-06
申请号：US10927679
申请日：2004-08-26
申请人： Theodore F. Baumann , Joe H. Satcher, Jr. , Alexander E. Gash
发明人： Theodore F. Baumann , Joe H. Satcher, Jr. , Alexander E. Gash
IPC分类号： C08J9/28
CPC分类号： C08J9/28 , C08J2201/05 , C08J2203/08 , C08J2361/02 , Y02P20/544
摘要： Synthetic methods for the preparation of hydrophobic organics aerogels. One method involves the sol-gel polymerization of 1,3-dimethoxybenzene or 1,3,5-trimethoxybenzene with formaldehyde in non-aqueous solvents. Using a procedure analogous to the preparation of resorcinol-formaldehyde (RF) aerogels, this approach generates wet gels that can be dried using either supercritical solvent extraction to generate the new organic aerogels or air dried to produce an xerogel. Other methods involve the sol-gel polymerization of 1,3,5 trihydroxy benzene (phloroglucinol) or 1,3 dihydroxy benzene (resorcinol) and various aldehydes in non-aqueous solvents. These methods use a procedure analogous to the one-step base and two-step base/acid catalyzed polycondensation of phloroglucinol and formaldehyde, but the base catalyst used is triethylamine. These methods can be applied to a variety of other sol-gel precursors and solvent systems. These hydrophobic organics aerogels have numerous application potentials in the field of material absorbers and water-proof insulation.
摘要翻译：制备疏水性有机物气凝胶的合成方法。一种方法涉及1,3-二甲氧基苯或1,3,5-三甲氧基苯与甲醛在非水溶剂中的溶胶 - 凝胶聚合。使用类似于间苯二酚 - 甲醛（RF）气凝胶的制备方法，该方法产生湿凝胶，其可以使用超临界溶剂萃取干燥以产生新的有机气凝胶或空气干燥以产生干凝胶。其他方法涉及在非水溶剂中1,3,5-三羟基苯（间苯三酚）或1,3-二羟基苯（间苯二酚）和各种醛的溶胶 - 凝胶聚合。这些方法使用类似于间苯三酚和甲醛的一步碱和两步碱/酸催化缩聚的方法，但所用的碱催化剂是三乙胺。这些方法可以应用于各种其他溶胶 - 凝胶前体和溶剂体系。这些疏水性有机气凝胶在材料吸收体和防水绝缘领域具有许多应用潜力。

7. 发明授权

US06806299B2 Preparation of hydrophobic organic aeorgels 失效
标题翻译：疏水性有机物的制备
公开(公告)号：US06806299B2
公开(公告)日：2004-10-19
申请号：US10132893
申请日：2002-04-24
申请人： Theodore F. Baumann , Joe H. Satcher, Jr. , Alexander E. Gash
发明人： Theodore F. Baumann , Joe H. Satcher, Jr. , Alexander E. Gash
IPC分类号： C08J928
CPC分类号： C08J9/28 , C08J2201/05 , C08J2203/08 , C08J2361/02 , Y02P20/544
摘要： Synthetic methods for the preparation of hydrophobic organics aerogels. One method involves the sol-gel polymerization of 1,3-dimethoxybenzene or 1,3,5-trimethoxybenzene with formaldehyde in non-aqueous solvents. Using a procedure analogous to the preparation of resorcinol-formaldehyde (RF) aerogels, this approach generates wet gels that can be dried using either supercritical solvent extraction to generate the new organic aerogels or air dried to produce an xerogel. Other methods involve the sol-gel polymerization of 1,3,5 trihydroxy benzene (phloroglucinol) or 1,3 dihydroxy benzene (resorcinol) and various aldehydes in non-aqueous solvents. These methods use a procedure analogous to the one-step base and two-step base/acid catalyzed polycondensation of phloroglucinol and formaldehyde, but the base catalyst used is triethylamine. These methods can be applied to a variety of other sol-gel precursors and solvent systems. These hydrophobic organics aerogels have numerous application potentials in the field of material absorbers and water-proof insulation.
摘要翻译：制备疏水性有机物气凝胶的合成方法。一种方法涉及1,3-二甲氧基苯或1,3,5-三甲氧基苯与甲醛在非水溶剂中的溶胶 - 凝胶聚合。使用类似于间苯二酚 - 甲醛（RF）气凝胶的制备方法，该方法产生湿凝胶，其可以使用超临界溶剂萃取干燥以产生新的有机气凝胶或空气干燥以产生干凝胶。其他方法涉及在非水溶剂中1,3,5-三羟基苯（间苯三酚）或1,3-二羟基苯（间苯二酚）和各种醛的溶胶 - 凝胶聚合。这些方法使用类似于间苯三酚和甲醛的一步碱和两步碱/酸催化缩聚的方法，但所用的碱催化剂是三乙胺。这些方法可以应用于各种其他溶胶 - 凝胶前体和溶剂体系。这些疏水性有机气凝胶在材料吸收体和防水绝缘领域具有许多应用潜力。

8. 发明申请

US20110203714A1 NANO-LAMINATE-BASED IGNITORS 有权
标题翻译：基于纳米层压的IGNITORS
公开(公告)号：US20110203714A1
公开(公告)日：2011-08-25
申请号：US13100154
申请日：2011-05-03
申请人： Troy W. Barbee, JR. , Randall L. Simpson , Alexander E. Gash , Joe H. Satcher, JR.
发明人： Troy W. Barbee, JR. , Randall L. Simpson , Alexander E. Gash , Joe H. Satcher, JR.
IPC分类号： B32B37/14 , B05D7/00 , B05D5/00 , B05D1/02 , B05D1/18 , B05D3/12 , C23C16/44 , B82Y30/00 , B82Y99/00
CPC分类号： C06C9/00 , C06B33/00 , C06B45/14 , Y10T156/10
摘要： Sol-gel chemistry is used to prepare igniters comprising energetic multilayer structures coated with energetic materials. These igniters can be tailored to be stable to environmental aging, i.e., where the igniters are exposed to extremes of both hot and cold temperatures (−30 C to 150 C) and both low (0%) and high relative humidity (100%).
摘要翻译：溶胶 - 凝胶化学用于制备包含高能材料的能量多层结构的点火器。这些点火器可以被定制为对环境老化是稳定的，即点火器暴露于热和冷温度（-30℃至150℃）以及低（0％）和高相对湿度（100％）的极限的地方。。

9. 发明申请

US20100267541A1 Nano-ceramics and method thereof 审中-公开
标题翻译：纳米陶瓷及其方法
公开(公告)号：US20100267541A1
公开(公告)日：2010-10-21
申请号：US11477331
申请日：2006-06-28
申请人： Joe H. Satcher, JR. , Alexander E. Gash , Randall L. Simpson , Richard L. Landingham , Robert A. Reibold
发明人： Joe H. Satcher, JR. , Alexander E. Gash , Randall L. Simpson , Richard L. Landingham , Robert A. Reibold
IPC分类号： C04B35/563 , C04B35/624
CPC分类号： B01J13/0091 , B82Y30/00 , C01B13/32 , C01F7/34 , C01P2002/72 , C01P2004/03 , C01P2004/64 , C04B35/111 , C04B35/117 , C04B35/624 , C04B35/6264 , C04B35/62695 , C04B35/63488 , C04B35/645 , C04B2111/00793 , C04B2235/3217 , C04B2235/3409 , C04B2235/3804 , C04B2235/3821 , C04B2235/3843 , C04B2235/449 , C04B2235/5427 , C04B2235/604 , C04B2235/608 , C04B2235/656 , C04B2235/658 , C04B2235/77 , C04B2235/781 , C04B2235/80 , C04B2235/95 , C04B2235/96
摘要： A method for producing ceramic materials utilizing the sol-gel process enables the preparation of intimate homogeneous dispersions of materials while offering the ability to control the size of one component within another. The method also enables the preparation of materials that densify at reduced temperatures. Applications of the compositions include filters, solid-oxide fuel cells, membranes, ceramic cutting tools and wear and auto parts. In one example, 10 g of AlCl6.6H2O is added to a 150 ml beaker and dissolved in 10 g EtOH and 1 g H2O. While stirring, 0.456 g of B4C powder is added. Then 9.6 g of propylene oxide is added. The gel sets up in about 10 minutes and is dried overnight. It is then washed with 1% NH4OH and air dried to yield 3.969 g of Al2O3/B4C xerogel.
摘要翻译：使用溶胶 - 凝胶法生产陶瓷材料的方法使得能够制备材料的均匀均匀分散体，同时提供控制另一种组分的尺寸的能力。该方法还能够制备在降低的温度下致密化的材料。组合物的应用包括过滤器，固体氧化物燃料电池，膜，陶瓷切削工具和磨损和汽车部件。在一个实例中，将10g AlCl 6·6H 2 O加入到150ml烧杯中并溶解在10g EtOH和1g H 2 O中。搅拌的同时，加入0.456g的B4C粉末。然后加入9.6g环氧丙烷。凝胶在约10分钟内成型并干燥过夜。然后用1％NH 4 OH洗涤，空气干燥，得到3.969g的Al2O3 / B4C干凝胶。

10. 发明授权

US08328967B2 Nano-laminate-based ignitors 有权
标题翻译：基于纳米层压板的点火器
公开(公告)号：US08328967B2
公开(公告)日：2012-12-11
申请号：US13100154
申请日：2011-05-03
申请人： Troy W. Barbee, Jr. , Randall L. Simpson , Alexander E. Gash , Joe H. Satcher, Jr.
发明人： Troy W. Barbee, Jr. , Randall L. Simpson , Alexander E. Gash , Joe H. Satcher, Jr.
IPC分类号： C06B23/00 , D03D23/00
CPC分类号： C06C9/00 , C06B33/00 , C06B45/14 , Y10T156/10
摘要： Sol-gel chemistry is used to prepare igniters comprising energetic multilayer structures coated with energetic materials. These igniters can be tailored to be stable to environmental aging, i.e., where the igniters are exposed to extremes of both hot and cold temperatures (−30 C to 150 C) and both low (0%) and high relative humidity (100%).
摘要翻译：溶胶 - 凝胶化学用于制备包含高能材料的能量多层结构的点火器。这些点火器可以被定制为对环境老化是稳定的，即点火器暴露于热和冷温度（-30℃至150℃）以及低（0％）和高相对湿度（100％）的极限的地方。。

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