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1. 发明授权

US06376417B1 Catalyst for the polymerization of propylene and its use 有权
标题翻译：用于丙烯聚合的催化剂及其用途
公开(公告)号：US06376417B1
公开(公告)日：2002-04-23
申请号：US09605828
申请日：2000-06-29
申请人： Aichun Yang , Zhulan Li , Yun Zhao , Wenbo Song , Juziu Yang , Bingquan Mao , Huiru Yang
发明人： Aichun Yang , Zhulan Li , Yun Zhao , Wenbo Song , Juziu Yang , Bingquan Mao , Huiru Yang
IPC分类号： B01J3100
CPC分类号： B01J31/0258 , B01J31/0201 , B01J31/0274 , B01J31/143 , B01J37/031 , C08F10/00 , C08F110/06 , C08F4/651 , C08F4/6543 , C08F2500/18 , C08F2500/24
摘要： A catalyst for the polymerization of propylene comprising components (A), (B) and (C) is provided. Component (A) is a solid product prepared by dissolving a halide of magnesium in a solvent system consisting of an organic epoxy compound, an organic phosphorus compound and an inert diluent to form a homogeneous solution; mixing the homogeneous solution with a halide of titanium to form a mixture; precipitating a solid from the mixture in the presence of an auxiliary precipitant; treating the solid with a polycarboxylic ester to load the ester on the solid; and treating the ester loaded solid with the halide of titanium and the inert diluent. Component (B) is an organic aluminium compound, and component (C) is an organic silicon compound. The particle size of the catalyst can be adjusted by increasing the amount of the inert diluent at a low ratio of the epoxy compound to the phosphorus compound.
摘要翻译：提供了包含组分（A），（B）和（C）的丙烯聚合催化剂。组分（A）是通过将镁的卤化物溶解在由有机环氧化合物，有机磷化合物和惰性稀释剂组成的溶剂体系中以形成均匀溶液而制备的固体产物; 将均匀溶液与钛的卤化物混合以形成混合物; 在辅助沉淀剂存在下，从混合物中沉淀出固体; 用聚羧酸酯处理固体以将酯负载在固体上; 并用钛和惰性稀释剂的卤化物处理酯负载的固体。组分（B）是有机铝化合物，组分（C）是有机硅化合物。可以通过以低比例的环氧化合物与磷化合物的比例增加惰性稀释剂的量来调节催化剂的粒径。

2. 发明授权

US06703339B2 Components and catalysts for the (co)polymerization of olefins 有权
标题翻译：用于（共）烯烃聚合的组分和催化剂
公开(公告)号：US06703339B2
公开(公告)日：2004-03-09
申请号：US09732523
申请日：2000-12-06
申请人： Zhulan Li , Juxiu Yang , Mingzhi Gao , Yun Zhao , Bingquan Mao , Aichun Yang , Chunmin Ding , Wenbo Song , Kunzheng Liu
发明人： Zhulan Li , Juxiu Yang , Mingzhi Gao , Yun Zhao , Bingquan Mao , Aichun Yang , Chunmin Ding , Wenbo Song , Kunzheng Liu
IPC分类号： B01J3100
CPC分类号： C08F10/00 , C08F4/654
摘要： A catalyst component for the (co)polymerization of olefins is provided. The catalyst comprises titanium, magnesium halogen and a mixed electron-donor and a catalyst for the (co)polymerization of olefins comprising:(A) the catalyst component; (B) an organic aluminum compound; and (C) an organic silicon compound. A polymer with high and adjustable stereospecificity and broad molecular weight distribution can be prepared by using the catalyst.
摘要翻译：提供了用于（共）聚合烯烃的催化剂组分。催化剂包括钛，镁卤素和混合电子给体和用于（共）聚合烯烃的催化剂，其包括：（A）催化剂组分; （B）有机铝化合物; 和（C）有机硅化合物。可以通过使用催化剂来制备具有高且可调立体定向性和宽分子量分布的聚合物。

3. 发明授权

US4784983A Catalyst system for use in olefinic polymerization 失效
标题翻译：用于烯烃聚合的催化剂体系
公开(公告)号：US4784983A
公开(公告)日：1988-11-15
申请号：US907664
申请日：1986-09-15
申请人： Bingquan Mao , Aichun Yang , Ying Zheng , Juxiou Yang , Zhulan Li
发明人： Bingquan Mao , Aichun Yang , Ying Zheng , Juxiou Yang , Zhulan Li
IPC分类号： C08F4/60 , C08F4/64 , C08F4/658 , C08F10/00
CPC分类号： C08F10/00
摘要： A catalyst system for use in olefinic polymerization and copolymerization is comprised of components (A), (B) and (C). The catalyst component (A) consisting essentially of titanium, magnesium, halogen, polycarboxylic acid esters and organic phosphorus compounds is a solid product, being prepared by mixing titanium tetrahalide and auxiliary precipitant with a homogeneous solution of magnesium halide in a solvent system consisting essentially of an organic epoxy compound and an organic phosphorus compound to form a solid product which is then treated with a polycarboxylic acid ester and titanium tetrahalide. Component (B) is an organic aluminum compound, and component (C) is an organic silicon compound. The catalyst system has a very high activity, and the resultant polymers have very high stereospecificity and good granular appearance.

4. 发明授权

US4861847A Catalyst system for use in olefinic polymerization 失效
标题翻译：用于烯烃聚合的催化剂体系
公开(公告)号：US4861847A
公开(公告)日：1989-08-29
申请号：US211459
申请日：1988-06-24
申请人： Bingquan Mao , Aichun Yang , Ying Zheng , Juxiou Yang , Zhulan Li
发明人： Bingquan Mao , Aichun Yang , Ying Zheng , Juxiou Yang , Zhulan Li
IPC分类号： C08F4/60 , C08F4/64 , C08F4/658 , C08F10/00
CPC分类号： C08F10/00
摘要： A catalyst system for use in olefinic polymerization and copolymerization is comprised of components (A), (B) and (C). The catalyst component (A) consisting essentially of titanium, magnesium, halogen, polycarboxylic acid esters and organic phosphorus compounds is a solid product, being prepared by mixing titanium tetrahalide and auxiilary precipitant with a homogeneous solution of magnesium halide in a solvent system consisting essentially of an organic epoxy compound and an organic phosphorus compound to form a solid product which is then treated with a polycarboxylic acid ester and titanium tetrahalide. Component (B) is an organic aluminum compound, and component (C) is an organic silicon compound. The catalyst system has very high activity, and the resultant polymers have very high stereospecificity and good granular appearance.
摘要翻译：用于烯烃聚合和共聚的催化剂体系由组分（A），（B）和（C）组成。基本上由钛，镁，卤素，多元羧酸酯和有机磷化合物组成的催化剂组分（A）是固体产物，其通过将四卤化钛和自缩速沉淀剂与卤化镁的均匀溶液在基本上由有机环氧化合物和有机磷化合物形成固体产物，然后用多元羧酸酯和四卤化钛处理。组分（B）是有机铝化合物，组分（C）是有机硅化合物。该催化剂体系具有非常高的活性，所得聚合物具有非常高的立体定向性和良好的粒状外观。

5. 发明授权

US06683017B2 Catalyst system for the (co) polymerization of olefins 有权
标题翻译：用于（共）烯烃聚合的催化剂体系
公开(公告)号：US06683017B2
公开(公告)日：2004-01-27
申请号：US09732045
申请日：2000-12-06
申请人： Mingzhi Gao , Jian Zhou , Yun Zhao , Zhulan Li , Yantoo Yang , Juxiu Yang , Weihua Feng
发明人： Mingzhi Gao , Jian Zhou , Yun Zhao , Zhulan Li , Yantoo Yang , Juxiu Yang , Weihua Feng
IPC分类号： B01J3100
CPC分类号： C08F10/00 , C08F4/654 , C08F4/651
摘要： A catalyst system for the (co)polymerization of propylene contains (A) a solid catalyst component comprising titanium, magnesium, halogen and a 1,3-diether; (B) an organic aluminum compound; and optionally (C) an organic silicon compound. In comparison with the prior art, stereospecificity of the polymer prepared by using the catalyst system of this invention evenl containing no external electron-donor is greater than 99%. Also, the activity of the catalyst system and hydrogen gas adjustability on the molecular weight of the polymer do not significantly decrease.
摘要翻译：用于丙烯（共）聚合的催化剂体系包含（A）包含钛，镁，卤素和1,3-二醚的固体催化剂组分; （B）有机铝化合物; 和（C）有机硅化合物。与现有技术相比，通过使用本发明的催化剂体系制备的聚合物的立体定向性不含外电子给体的偶联剂大于99％。此外，催化剂体系的活性和氢气可调整性对聚合物的分子量没有显着降低。

6. 发明申请

US20140193530A1 PHARMACEUTICAL COMPOSITION CONTAINING HONEYSUCKLE EXTRACT AND ANTIBIOTICS, PHARMACEUTICAL KIT, AND USE OF HONEYSUCKLE EXTRACT FOR PREPARATION OF DRUG 有权
标题翻译：含有蜂胶提取物和抗生素的药物组合物，药物包，以及用于制备药物的蜂胶提取物的用途
公开(公告)号：US20140193530A1
公开(公告)日：2014-07-10
申请号：US14238448
申请日：2011-08-12
申请人： Tiejun Zhang , Jiangong Shi , Hong Meng , Fengnian Han , Xuwei Ma , Zhulan Li
发明人： Tiejun Zhang , Jiangong Shi , Hong Meng , Fengnian Han , Xuwei Ma , Zhulan Li
IPC分类号： A61K31/7048 , A61K31/428 , A61K36/355
CPC分类号： A61K31/7048 , A61K31/428 , A61K31/7042 , A61K36/355 , C07H17/04 , Y02A50/473
摘要： Provided is a pharmaceutical composition useful for prevention and/or treatment of diseases caused by bacteria, wherein the pharmaceutical composition comprising a honeysuckle extract containing iridoid compounds and an antibiotic. Also provided is a pharmaceutical kit comprising the honeysuckle extract containing the iridoid compounds and the antibiotics which are separately placed. The honeysuckle extract is used in combination with the antibiotics, the responsiveness of multi-drug resistant bacteria to antibiotics is improved, a clinical application prospect is presented, especially the current status of the refractory bacterial infection diseases caused by the pathogenic bacteria resistant to the antibiotics can be improved. Also provided is a use of the pharmaceutical composition and pharmaceutical kit in the preparation of drugs for prevention and/or treatment a diseases caused by bacteria. In addition, also provided is a use of the honeysuckle extract in the preparation of drugs for reversing bacterial resistance.
摘要翻译：提供了可用于预防和/或治疗由细菌引起的疾病的药物组合物，其中所述药物组合物包含含有环烯醚萜烯化合物和抗生素的金银花提取物。还提供了包含含有环烯醚萜烯化合物的金银花提取物和分开放置的抗生素的药物试剂盒。金银花提取物与抗生素结合使用，多药耐药细菌对抗生素的反应性得到改善，提出了临床应用前景，特别是耐药菌耐药菌耐药细菌感染疾病的现状可以改进。还提供了药物组合物和药物试剂盒在制备用于预防和/或治疗由细菌引起的疾病的药物中的用途。此外，还提供了金银花提取物在制备用于逆转细菌耐药性的药物中的用途。

7. 发明授权

US09849145B2 Pharmaceutical composition containing honeysuckle extract and antibiotics, pharmaceutical kit, and use of honeysuckle extract for preparation of drug 有权
公开(公告)号：US09849145B2
公开(公告)日：2017-12-26
申请号：US14238448
申请日：2011-08-12
申请人： Tiejun Zhang , Jiangong Shi , Hong Meng , Fengnian Han , Xuwei Ma , Zhulan Li
发明人： Tiejun Zhang , Jiangong Shi , Hong Meng , Fengnian Han , Xuwei Ma , Zhulan Li
IPC分类号： A61K36/355 , A61K36/36 , A61K31/7048 , C07H17/04 , A61K31/428 , A61K31/7042
CPC分类号： A61K31/7048 , A61K31/428 , A61K31/7042 , A61K36/355 , C07H17/04 , Y02A50/473
摘要： Provided is a pharmaceutical composition useful for prevention and/or treatment of diseases caused by bacteria, wherein the pharmaceutical composition comprising a honeysuckle extract containing iridoid compounds and an antibiotic. Also provided is a pharmaceutical kit comprising the honeysuckle extract containing the iridoid compounds and the antibiotics which are separately placed. The honeysuckle extract is used in combination with the antibiotics, the responsiveness of multi-drug resistant bacteria to antibiotics is improved, a clinical application prospect is presented, especially the current status of the refractory bacterial infection diseases caused by the pathogenic bacteria resistant to the antibiotics can be improved. Also provided is a use of the pharmaceutical composition and pharmaceutical kit in the preparation of drugs for prevention and/or treatment a diseases caused by bacteria. In addition, also provided is a use of the honeysuckle extract in the preparation of drugs for reversing bacterial resistance.

8. 发明授权

US07388061B2 Solid catalyst component for polymerization of olefins, catalyst comprising the same and use thereof 有权
公开(公告)号：US07388061B2
公开(公告)日：2008-06-17
申请号：US10503515
申请日：2003-01-30
申请人： Mingzhi Gao , Haitao Liu , Zhulan Li , Jun Wang , Juxiu Yang , Tianyi Li , Xiaodong Wang , Changxiu Li , Chunming Ding
发明人： Mingzhi Gao , Haitao Liu , Zhulan Li , Jun Wang , Juxiu Yang , Tianyi Li , Xiaodong Wang , Changxiu Li , Chunming Ding
IPC分类号： C08F4/42
CPC分类号： C08F10/00 , C08F110/06 , C08F4/651 , C08F4/6494 , C08F4/6492 , C08F4/6465 , C08F2500/18 , C08F2500/12 , C08F2500/15 , C08F2500/04
摘要： The present invention provides a solid catalyst component for the polymerization of olefins, comprising magnesium, titanium, a halogen and an electron donor, wherein said electron donor comprises at least one selected from the group consisting of ester of polyol of the formula (I): R1CO—O—CR3R4—A—CR5R6—O—CO—R2 (I) wherein, R1 and R2 groups, which may be identical or different, can be substituted or unsubstituted hydrocarbyl having 1 to 20 carbon atoms, R3-R6 groups, which may be identical or different, can be selected from the group consisting of hydrogen, halogen or substituted or unsubstituted hydrocarbyl having 1 to 20 carbon atoms, R1-R6 groups optionally contain one or more hetero-atoms replacing carbon, hydrogen atom or the both, said hetero-atom is selected from the group consisting of nitrogen, oxygen, sulfur, silicon, phosphorus and halogen atom, two or more of R3-R6 groups can be linked to form saturated or unsaturated monocyclic or polycyclic ring A is a single bond or bivalent linking group with chain length between two free radicals being 1-10 atoms, wherein said bivalent linking group is selected from the group consisting of aliphatic, alicyclic and aromatic bivalent radicals, and can carry C1-C20 linear or branched substituents one or more of carbon atom and/or hydrogen atom on above-mentioned bivalent linking group and substituents can be replaced by a hetero-atom selected from the group consisting of nitrogen, oxygen, sulfur, silicon, phosphorus, and halogen atom, and two or more said substituents on the linking group as well as above-mentioned R3-R6 groups can be linked to form saturated or unsaturated monocyclic or polycyclic ring.

9. 发明申请

US20050239636A1 Solid catalyst component for polymerization of olefins, catalyst comprising the same and use thereof 有权
公开(公告)号：US20050239636A1
公开(公告)日：2005-10-27
申请号：US10503515
申请日：2003-01-30
申请人： Mingzhi Gao , Haitao Liu , Zhulan Li , Jun Wang , Juxiu Yang , Tianyi Li , Xiaodong Wang , Changxiu Li , Chunming Ding
发明人： Mingzhi Gao , Haitao Liu , Zhulan Li , Jun Wang , Juxiu Yang , Tianyi Li , Xiaodong Wang , Changxiu Li , Chunming Ding
IPC分类号： C08F4/649 , C08F4/654 , C08F10/00 , C08F110/06 , B01J31/00 , C08F4/44
CPC分类号： C08F10/00 , C08F110/06 , C08F4/651 , C08F4/6494 , C08F4/6492 , C08F4/6465 , C08F2500/18 , C08F2500/12 , C08F2500/15 , C08F2500/04
摘要： The present invention provides a solid catalyst component for the polymerization of olefins, comprising magnesium, titanium, a halogen and an electron donor, wherein said electron donor comprises at least one selected from the group consisting of polyol ester compounds of the formula (I): R1CO—O—CR3R4-A-CR5R6—O—CO—R2 (I) wherein, R1 and R2 groups, which may be identical or different, can be substituted or unsubstituted hydrocarbyl having 1 to 20 carbon atoms, R3-R6 groups, which may be identical or different, can be selected from the group consisting of hydrogen, halogen or substituted or unsubstituted hydrocarbyl having 1 to 20 carbon atoms, R1-R6 groups optionally contain one or more hetero-atoms replacing carbon, hydrogen atom or the both, said hetero-atom is selected from the group consisting of nitrogen, oxygen, sulfur, silicon, phosphorus and halogen atom, two or more of R3-R6 groups can be linked to form saturated or unsaturated monocyclic or polycyclic ring; A is a single bond or bivalent linking group with chain length between two free radicals being 1-10 atoms, wherein said bivalent linking group is selected from the group consisting of aliphatic, alicyclic and aromatic bivalent radicals, and can carry C1-C20 linear or branched substituents; one or more of carbon atom and/or hydrogen atom on above-mentioned bivalent linking group and substituents can be replaced by a hetero-atom selected from the group consisting of nitrogen, oxygen, sulfur, silicon, phosphorus, and halogen atom, and two or more said substituents on the linking group as well as above-mentioned R3-R6 groups can be linked to form saturated or unsaturated monocyclic or polycyclic ring.

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