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1. 发明授权

US10222356B2 Sequential oxidation-reduction reactor for post column reaction GC/FID system 有权
公开(公告)号：US10222356B2
公开(公告)日：2019-03-05
申请号：US15002070
申请日：2016-01-20
申请人： Activated Research Company, LLC
发明人： Andrew Jones
IPC分类号： G01N30/46 , G01N30/68 , G01N30/84 , B33Y80/00 , B29L31/00
摘要： Provided is a system comprising a conduit from a gas chromatograph column to a single reactor comprising a Fe, Co, Pt, Ni, Rh, Pd and/or Ru catalyst(s), with hydrogen and oxygen feed conduits for providing hydrogen and oxygen to the reactor, and a conduit from the reactor to an FID detector. This allows one to practice a method for the detection and quantification of organic molecules from a gas chromatograph which comprises passing the effluent from a gas chromatograph column to a reactor comprising a Fe, Co, Pt, Ni, Rh, Pd and/or Ru catalyst; adding hydrogen and air/oxygen to the reactor; reacting the effluent from the gas chromatograph column in the reactor to sequentially oxidize then reduce all organic containing molecules to CH4 by heating to an elevated temperature, and passing the reactor effluent to an FID.

2. 发明授权

US11428675B2 Liquid chromatography analyte reaction and analysis system 有权
公开(公告)号：US11428675B2
公开(公告)日：2022-08-30
申请号：US16524269
申请日：2019-07-29
申请人： Activated Research Company, LLC
发明人： Andrew Jones , Tommy Saunders , Mike Hofflander
IPC分类号： G01N30/64 , G01N30/38 , G01N30/34 , G01N30/02 , G01N30/84
摘要： In the present system and method, a conduit from a LC device continuously transports solvent, buffers, and analytes to the inlet of a solvent removal and analyte conversion device which evaporates the solvents, leaving non-volatile analytes for detection. The device comprises a rotating disk. The liquid chromatograph device can be any device using liquid chromatography to separate molecules. The solvents in the LC effluent can include, but are not limited to, water, methanol, acetonitrile, tetrahydrofuran, and acetone. After removal of the volatile components, the non-volatile analytes are converted with a concentrated energy source so that they may be detectable.

3. 发明授权

US10041913B2 One reactor post column reaction GC/FID system using Ru catalyst 有权
公开(公告)号：US10041913B2
公开(公告)日：2018-08-07
申请号：US14984801
申请日：2015-12-30
申请人： Activated Research Company, LLC
发明人： Andrew Jones
IPC分类号： G01N30/68 , G01N30/88 , B01J23/46 , G01N30/02
摘要： Provided is a system comprising a conduit from a gas chromatograph column to a reactor comprising a Ru catalyst, with a hydrogen feed conduit for providing hydrogen to the conduit from the gas chromatograph column, and a conduit from the reactor to an FID detector. This allows one to practice a method for the detection and quantification of organic molecules from a gas chromatograph which comprises passing the effluent from a gas chromatograph column to a reactor comprising a Ru catalyst; adding hydrogen to the effluent prior to the effluent reaching the catalyst; reacting the effluent from the gas chromatograph column in the reactor to reduce all organic containing molecules to CH4 by heating to an elevated temperature, and passing the effluent from the reactor to an FID.

4. 发明授权

US11835497B2 Liquid chromatography analyte reaction and analysis system 有权
公开(公告)号：US11835497B2
公开(公告)日：2023-12-05
申请号：US17869244
申请日：2022-07-20
申请人： Activated Research Company, LLC
发明人： Andrew Jones , Tommy Saunders , Mike Hofflander
IPC分类号： G01N30/64 , G01N30/38 , G01N30/34 , G01N30/02 , G01N30/84
CPC分类号： G01N30/64 , G01N30/38 , G01N2030/027 , G01N2030/347 , G01N2030/8417 , G01N2030/8447 , G01N2030/8494
摘要： In the present system and method, a conduit from a LC device continuously transports solvent, buffers, and analytes to the inlet of a solvent removal and analyte conversion device which evaporates the solvents, leaving non-volatile analytes for detection. The device comprises a rotating disk. The liquid chromatograph device can be any device using liquid chromatography to separate molecules. The solvents in the LC effluent can include, but are not limited to, water, methanol, acetonitrile, tetrahydrofuran, and acetone. After removal of the volatile components, the non-volatile analytes are converted with a concentrated energy source so that they may be detectable.

5. 发明授权

US10416129B2 Catalytic reactor coupled with flame ionization detector for liquid chromatography 有权
公开(公告)号：US10416129B2
公开(公告)日：2019-09-17
申请号：US15356110
申请日：2016-11-18
申请人： Activated Research Company, LLC
发明人： Andrew Jones , Charles Spanjers
IPC分类号： G01N30/68 , G01N30/84 , G01N30/32 , B01J23/56 , B01J23/00 , G01N30/06
摘要： Provided is a system comprising a device that performs one or more reactions to liquid or supercritical fluid chromatograph effluents and produces molecules that are subsequently detected by a suitable detector. This allows for one to practice a method for the detection and quantification of organic molecules from a liquid chromatograph for the purpose of increasing detection limits and allowing for the universal detection of organic molecules. The linear dynamic range and molecular response are greater than those previously available.

6. 发明申请

US20160187307A1 ONE REACTOR POST COLUMN REACTION GC/FID SYSTEM USING Ru CATALYST 审中-公开
标题翻译：一个反应器柱反应GC / FID系统使用钌催化剂
公开(公告)号：US20160187307A1
公开(公告)日：2016-06-30
申请号：US14984801
申请日：2015-12-30
申请人： Activated Research Company, LLC
发明人： Andrew Jones
IPC分类号： G01N30/68
CPC分类号： G01N30/68 , B01J23/462 , B01J2531/821 , G01N30/88 , G01N2030/025 , G01N2030/884
摘要： Provided is a system comprising a conduit from a gas chromatograph column to a reactor comprising a Ru catalyst, with a hydrogen feed conduit for providing hydrogen to the conduit from the gas chromatograph column, and a conduit from the reactor to an FID detector. This allows one to practice a method for the detection and quantification of organic molecules from a gas chromatograph which comprises passing the effluent from a gas chromatograph column to a reactor comprising a Ru catalyst; adding hydrogen to the effluent prior to the effluent reaching the catalyst; reacting the effluent from the gas chromatograph column in the reactor to reduce all organic containing molecules to CH4 by heating to an elevated temperature, and passing the effluent from the reactor to an FID.
摘要翻译：提供了一种系统，其包括从气相色谱柱到包含Ru催化剂的反应器的管道，具有用于从气相色谱仪柱向管道提供氢气的氢气供给管道以及从反应器到FID检测器的导管。这允许从气相色谱仪中实施用于检测和定量有机分子的方法，该方法包括将来自气相色谱仪柱的流出物传送到包含Ru催化剂的反应器中; 在流出物到达催化剂之前向流出物中加入氢气; 使来自气相色谱柱的流出物在反应器中反应，通过加热至高温将所有含有机物的分子还原成CH 4，并将流出物从反应器送至FID。

7. 发明授权

US10859543B2 Sequential oxidation-reduction reactor for post column reaction GC/FID system 有权
公开(公告)号：US10859543B2
公开(公告)日：2020-12-08
申请号：US16261772
申请日：2019-01-30
申请人： Activated Research Company, LLC
发明人： Andrew Jones
IPC分类号： G01N30/68 , G01N30/84 , B22F3/10 , B33Y80/00 , B29L31/00 , B22F3/105
摘要： Provided is a system comprising a conduit from a gas chromatograph column to a single reactor comprising a Fe, Co, Pt, Ni, Rh, Pd and/or Ru catalyst(s), with hydrogen and oxygen feed conduits for providing hydrogen and oxygen to the reactor, and a conduit from the reactor to an FID detector. This allows one to practice a method for the detection and quantification of organic molecules from a gas chromatograph which comprises passing the effluent from a gas chromatograph column to a reactor comprising a Fe, Co, Pt, Ni, Rh, Pd and/or Ru catalyst; adding hydrogen and air/oxygen to the reactor; reacting the effluent from the gas chromatograph column in the reactor to sequentially oxidize then reduce all organic containing molecules to CH4 by heating to an elevated temperature, and passing the reactor effluent to an FID.

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