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1. 发明申请

US20150005538A1 PROCESS FOR PRODUCING 2, 3, 3, 3-TETRAFLUOROPROPENE AND 1, 1-DIFLUOROETHYLENE 有权
标题翻译：生产2,3,3,3-四氯丙烯和1,1-二氟乙烯的方法
公开(公告)号：US20150005538A1
公开(公告)日：2015-01-01
申请号：US14486143
申请日：2014-09-15
申请人： ASAHI GLASS COMPANY, LIMITED
发明人： Shoji FURUTA , Yu TAKEUCHI
IPC分类号： C07C17/269 , C07C17/25
CPC分类号： C07C17/269 , C07C17/25 , C07C21/18
摘要： To provide an economically advantageous process for producing HFO-1234yf useful as a new refrigerant in sufficiently high yield by one reaction involving thermal decomposition. A process for producing HFO-1234yf and VdF from raw material containing R22, R40 and TFE, by a synthetic reaction involving thermal decomposition, which comprises (a) a step of supplying the R22, the R40 and the TFE to a reactor, as preliminarily mixed or separately, (b) a step of supplying a heat medium to the reactor, and (c) a step of bringing the heat medium in contact with the R22, the R40 and the TFE in the reactor to form the HFO-1234yf and the VdF.
摘要翻译：通过涉及热分解的一个反应，提供一种经济上有利的生产HFO-1234yf作为新制冷剂的方法，该方法可以以足够高的产率生产。通过涉及热分解的合成反应从含有R22，R40和TFE的原料生产HFO-1234yf和VdF的方法，其包括（a）将R22，R40和TFE供应到反应器中的步骤，混合或分开，（b）向反应器供应热介质的步骤，和（c）使热介质与反应器中的R22，R40和TFE接触以形成HFO-1234yf的步骤，以及 VdF。

2. 发明申请

US20160002518A1 COMPOSITION CONTAINING TRIFLUOROETHYLENE 审中-公开
标题翻译：含有三氟乙烯的组合物
公开(公告)号：US20160002518A1
公开(公告)日：2016-01-07
申请号：US14851473
申请日：2015-09-11
申请人： Asahi Glass Company, Limited
发明人： Tomoaki TANIGUCHI , Hidekazu OKAMOTO , Shoji FURUTA , Yu TAKEUCHI
IPC分类号： C09K5/04 , B01F17/00 , C09K3/30 , C09K3/00
CPC分类号： C09K5/044 , B01F17/0085 , C07C17/278 , C07C17/383 , C09K3/00 , C09K3/30 , C09K5/045 , C09K2205/112 , C09K2205/12 , C09K2205/126 , C09K2205/22 , C07C21/18
摘要： To provide a composition containing HFO-1123 having a low GWP, useful as a heat transfer composition, an aerosol sprayer, a foaming agent, a blowing agent, a solvent or the like.A composition containing HFO-1123, and at least one first compound selected from the group consisting of HFO-1132, HFO-1132a, CFO-1113, HCFO-1122, HCFO-1122a, HFC-143 and methane.
摘要翻译：提供含有低GWP的HFO-1123，可用作传热组合物，气溶胶喷雾器，发泡剂，发泡剂，溶剂等的组合物。含有HFO-1123和至少一种选自HFO-1132，HFO-1132a，CFO-1113，HCFO-1122，HCFO-1122a，HFC-143和甲烷的第一化合物的组合物。

3. 发明申请

US20150291490A1 METHOD FOR PURIFYING TETRAFLUOROPROPENE 有权
标题翻译：净化四氯丙烯的方法
公开(公告)号：US20150291490A1
公开(公告)日：2015-10-15
申请号：US14749877
申请日：2015-06-25
申请人： ASAHI GLASS COMPANY, LIMITED
发明人： Shoji FURUTA , Tetsuo OTSUKA
IPC分类号： C07C17/386
CPC分类号： C07C17/386 , C07C17/18 , C07C17/395 , C07C21/18 , C07C19/03
摘要： To provide a method for efficiently separating 2,3,3,3-tetrafluoropropene (HFO-1234yf) and chloromethane (R40) from a composition containing HFO-1234yf and R40.A method for separating HFO-1234yf containing substantially no R40, which comprises bringing an azeotropic composition or azeotrope-like composition of HFO-1234yf and R40 into contact with a specific extraction solvent.
摘要翻译：提供从含有HFO-1234yf和R40的组合物有效分离2,3,3,3-四氟丙烯（HFO-1234yf）和氯甲烷（R40）的方法。一种分离基本上不含R40的HFO-1234yf的方法，其包括使HFO-1234yf和R40的共沸组合物或类共沸组合物与特定的提取溶剂接触。

4. 发明申请

US20150005537A1 PROCESS FOR PRODUCING 2, 3, 3, 3-TETRAFLUOROPROPENE 有权
标题翻译：生产2,3,3,3-四氯丙烯的方法
公开(公告)号：US20150005537A1
公开(公告)日：2015-01-01
申请号：US14486125
申请日：2014-09-15
申请人： ASAHI GLASS COMPANY, LIMITED
发明人： Shoji FURUTA , Yu Takeuchi
IPC分类号： C07C17/269
CPC分类号： C07C17/269 , C07C21/18
摘要： To provide an economically advantageous process for producing industrially useful HFO-1234yf efficiently and in a sufficiently controlled state by one reaction involving thermal decomposition, by using readily available raw material. A process for producing 2,3,3,3-tetrafluoropropene from a raw material composition containing chlorodifluoromethane and chloromethane, by a synthetic reaction involving thermal decomposition, which comprises (a) a step of supplying the chlorodifluoromethane and the chloromethane to a reactor, as preliminarily mixed or separately, in such amounts that the chloromethane would be in a ratio of from 0.01 to 3 mol to 1 mol of the chlorodifluoromethane, (b) a step of supplying a heat medium to the reactor, and (c) a step of bringing the heat medium in contact with the chlorodifluoromethane and the chloromethane in the reactor to form the 2,3,3,3-tetrafluoropropene.
摘要翻译：通过使用容易获得的原料，通过一种涉及热分解的反应，有效地并在足够受控的状态下提供经济上有利的工业生产工业上有用的HFO-1234yf方法。通过涉及热分解的合成反应，由包含氯二氟甲烷和氯甲烷的原料组合物制备2,3,3,3-四氟丙烯的方法，其包括（a）将氯二氟甲烷和氯甲烷供应到反应器中的步骤如预先混合或分开，使得氯甲烷的比例为0.01至3摩尔至1摩尔氯代二氟甲烷，（b）将热介质供应至反应器的步骤，和（c）使热介质与反应器中的氯二氟甲烷和氯甲烷接触以形成2,3,3,3-四氟丙烯。

5. 发明申请

US20140171697A1 FLUOROALKYL IODIDE AND ITS PRODUCTION PROCESS 有权
标题翻译：氟代碘及其生产工艺
公开(公告)号：US20140171697A1
公开(公告)日：2014-06-19
申请号：US14103072
申请日：2013-12-11
申请人： Asahi Glass Company, Limited
发明人： Shoji FURUTA , Yusuke SUGAHARA , Keiko NAKASE , Keisuke MORI
IPC分类号： C07C19/16
CPC分类号： C07C19/16 , C07C17/278
摘要： A process for producing a fluoroalkyl iodide as a telomer Rf(CF2CF2)nI (wherein Rf is a C1-10 fluoroalkyl group, and n is an integer of from 1 to 6) by telomerization from a fluoroalkyl iodide represented by the formula RfI (wherein Rf is as defined above) as a telogen and tetrafluoroethylene (CF2CF2) as a taxogen, which comprises a liquid phase telomerization step of supplying a homogeneous liquid mixture of the telogen and the taxogen from the lower portion of a tubular reactor, moving the mixture from the lower portion towards the upper portion of the reactor in the presence of a radical initiator over a retention time of at least 5 minutes while the reaction system is kept in a liquid phase state under conditions where no gas-liquid separation will take place, so that the taxogen supplied to the reactor is substantially consumed by the reaction in the reactor, and drawing the reaction product from the upper portion of the reactor.
摘要翻译：通过由式RfI表示的氟代烷基碘（其中Rf为（CF 2 CF 2）n I（其中R f为C 1-10氟烷基，n为1至6的整数）通过调聚而制备氟代烷基碘的方法 Rf为如上所定义），作为脱色酶的四环素（CF2CF2），其包括液相调聚步骤，从管状反应器的下部供应前体和衍生物的均匀液体混合物，将混合物从在自由基引发剂的存在下，在保持时间至少5分钟的同时反应体系在不发生气液分离的条件下保持在液相状态下的反应器上部的下部，因此提供给反应器的税主体基本上被反应器中的反应消耗，并从反应器的上部抽出反应产物。

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