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1. 发明授权

US3553246A Process for producing unsaturated aliphatic nitriles 失效
标题翻译：生产不饱和脂肪硝酸盐的方法
公开(公告)号：US3553246A
公开(公告)日：1971-01-05
申请号：US3553246D
申请日：1969-03-21
申请人： ASAHI CHEMICAL IND
发明人： KOMINAMI NAOYA , NAKAJIMA HITOSHI , KIMURA TAKEO , SAKURAI TAKIO
IPC分类号： B01J23/46 , B01J23/56 , B01J23/89 , C07C121/04
CPC分类号： B01J23/46 , B01J23/464 , B01J23/56 , B01J23/89 , C07C253/10 , Y02P20/52 , C07C255/08 , C07C255/07
摘要： A PROCESS FOR PRODUCING LOWER OLEFINIC NITRILES BY CATALYTICALLY REACTING IN THE GAS PHASE AT 100-500* C., A GAS COMPRISING ETHYLENE, PROPYLENE, NORMAL BUTYLENE OR ISOBUTYLENE, HYDROGEN CYANIDE AND OXYGEN OR A MOLECULAR OXYGEN-CONTAINING GAS IN THE PRESENCE OF A HYDROGEN HALIDE AND A CATALYST WHICH COMPRISES PALLADIUM AND RHODIUM AND THE OXIDES, HYDROXIDES, INORGANIC ACID SALTS OR ORGANIC ACID SALTS THEREOF.

2. 发明授权

US3465028A Process for preparing unsaturated aliphatic nitriles 失效
标题翻译：制备不饱和脂肪酸的方法
公开(公告)号：US3465028A
公开(公告)日：1969-09-02
申请号：US3465028D
申请日：1967-04-03
申请人： ASAHI CHEMICAL IND
发明人： KOMINAMI NAOYA , NAKAJIMA HITOSHI , WATANABE ITARU , KIMURA TAKEO , SAKURAI TOKIO
IPC分类号： C07C121/04 , C07C121/16
CPC分类号： C07C253/10 , C07C255/08

3. 发明授权

US3524874A Process for the production of phenylacrylonitriles 失效
标题翻译：生产苯丙氨酸锂的方法
公开(公告)号：US3524874A
公开(公告)日：1970-08-18
申请号：US3524874D
申请日：1967-12-20
申请人： ASAHI CHEMICAL IND
发明人： KOMINAMI NAOYA , NAKAJIMA HITOSHI , KIMURA TAKEO , SAKURAI TOKIO
IPC分类号： C07C255/34 , B01J11/12 , C07C121/70 , C07C121/72
CPC分类号： C07C253/10 , B01J31/2239 , B01J2231/322 , B01J2231/766 , B01J2531/822 , B01J2531/824 , Y02P20/584 , C07C255/34 , C07C255/35

4. 发明授权

US3524873A Process for producing alpha-alkylacrylonitrile 失效
标题翻译：生产α-羟基丙烯酸甲酯的方法
公开(公告)号：US3524873A
公开(公告)日：1970-08-18
申请号：US3524873D
申请日：1967-12-20
申请人： ASAHI CHEMICAL IND
发明人： KOMINAMI NAOYA , NAKAJIMA HITOSHI , CHONO MASAZUMI
IPC分类号： C07C121/32
CPC分类号： C07C255/00

5. 发明授权

US3869500A Process for the production of unsaturated aliphatic nitriles 失效
标题翻译：生产不饱和脂肪硝酸盐的方法
公开(公告)号：US3869500A
公开(公告)日：1975-03-04
申请号：US38500373
申请日：1973-08-21
申请人： ASAHI CHEMICAL IND
发明人： KOMINAMI NAOYA , NAKAJIMA HITOSHI , MIYATA SEIJI , KIMURA TAKEO , CHONO MASAZUMI , SAKURAI TOKIO
IPC分类号： B01J23/40 , B01J23/44 , B01J23/56 , B01J23/58 , B01J23/63 , B01J37/20 , C07C121/04 , C07C121/02
CPC分类号： B01J23/63 , B01J23/40 , B01J23/44 , B01J23/56 , B01J23/58 , B01J37/20 , C07C253/10 , Y02P20/52 , C07C255/08 , C07C255/07 , C07C255/10
摘要： Process for the production of unsaturated aliphatic nitriles selected from acrylonitrile, methacrylonitrile, crotononitrile, alpha-ethylacrylonitrile, beta-ethylacrylonitrile, alpha, betadimethylacrylonitrile, beta, beta-dimethylacrylonitrile, chloroacrylonitrile and fumaronitrile, which comprises contacting a gas mixture consisting essentially of an olefinic compound selected from ethylene, propylene, normal butylene, isobutylene and vinyl chloride, hydrogen cyanide and oxygen or a molecular oxygen-containing gas at a temperature of 100* to 500*C with a catalyst selected from palladium metal, chloride, bromide, iodide, cyanide, thiocyanide, oxide, hydroxide, sulfide, sulfate, nitrate, phosphate, hypochlorite, chlorite, chlorate, bromate, iodate, formate, acetate, mono-chloroacetate and oxalate which has been treated with a reducing sulfur compound at a temperature of from -10* to 1,200*C. The treatment with a reducing sulfur compound remarkably improves the catalytic life. Hydrogen sulfide and sulfur dioxide are especially preferred as reducing sulfur compound.
摘要翻译：用于生产选自丙烯腈，甲基丙烯腈，巴豆腈，α-乙基丙烯腈，β-乙基丙烯腈，α，β-二甲基丙烯腈，β，β-二甲基丙烯腈，氯丙烯腈和富马腈的不饱和脂族腈的方法，其包括将基本上由选自乙烯，丙烯，正丁烯，异丁烯和氯乙烯的烯烃化合物，氰化氢和氧气或分子氧气体在100至500℃的温度下与选自钯金属，氯化物，溴化物，碘化物，氰化物，硫氰酸盐，氧化物，氢氧化物，硫酸盐，硝酸盐，磷酸盐，次氯酸盐，亚氯酸盐，氯酸盐，溴酸盐，碘酸盐，甲酸盐，乙酸盐，单氯乙酸盐和草酸盐，其在还原硫化合物的温度 -10℃〜1200℃。用还原硫化合物处理显着提高了催化剂的含量 fe。特别优选硫化氢和二氧化硫作为还原硫化合物。

6. 发明授权

US3584029A Process for the production of lower saturated aliphatic nitriles 失效
标题翻译：生产低饱和脂肪硝酸盐的方法
公开(公告)号：US3584029A
公开(公告)日：1971-06-08
申请号：US3584029D
申请日：1968-04-09
申请人： ASAHI CHEMICAL IND
发明人： KOMINAMI NAOYA , NAKAJIMA HITOSHI , TAMURA NOBUHIRO
IPC分类号： B01J27/185 , C07C121/04
CPC分类号： B01J27/1853 , C07C253/10 , C07C255/03
摘要： THE PRODUCTION OF LOWER SATURATED ALIPHATIC NITRILES (I.E. PROPIONITRILE, ISOBUTYRONITRILE AND NORMAL BUTYRONITRILE) BY SUBJECTING A GAS MIXTURE CONTAINING A LOWER ALIPHATIC OLEFIN (I.E. ETHYLENE OR PROPYLENE) AND HYDROGEN CYANIDE TO CATALYTIC ADDITION REACTION AT A TEMPERATURE OF FROM 100 TO 600*C. IN THE PRESENCE OF, AS CATALYST, AT LEAST ONE COMPOUND SELECTED FROM NICKEL METAL, NICKEL CHLORIDE, NICKEL BROMIDE, NICKEL IODIDE, NICKEL OXALATE, NICKEL ACETATE, NICKEL CYANATE, NICKEL THIOCYANATE, NICKEL SULFATE AND NICKEL NITRATE AND AT LEAST ONE COMPOUND SELECTED FROM PHOSPHORIC ACID, PYROPHOSPHORIC ACID AND PHORPHORUS PENTOXIDE.

7. 发明授权

US3433820A Preparation of aromatic nitriles from substituted benzenes,hcn and oxygen in the presence of copper cyanide 失效
标题翻译：在氰化物存在下，从取代的苯乙烯，HCN和氧气中制备芳族硝酸盐
公开(公告)号：US3433820A
公开(公告)日：1969-03-18
申请号：US3433820D
申请日：1965-10-15
申请人： ASAHI CHEMICAL IND
发明人： KOMINAMI NAOYA , NAKAJIMA HITOSHI , TAMURA NOBUHIRO
IPC分类号： C07C255/49 , C07C121/04 , C07C121/02
CPC分类号： C07C255/49

8. 发明授权

US3865864A Process for producing cyanoalkadienes 失效
标题翻译：生产甘氨酸的方法
公开(公告)号：US3865864A
公开(公告)日：1975-02-11
申请号：US15245071
申请日：1971-06-11
申请人： ASAHI CHEMICAL IND
发明人： NAKAJIMA HITOSHI , NISHIMARU HIROJI
IPC分类号： C07B61/00 , B01J23/00 , B01J27/00 , B01J31/00 , C07C67/00 , C07C253/00 , C07C253/10 , C07C255/07 , C07C121/04
CPC分类号： C07C253/10 , C07C255/07
摘要： A process is provided for producing cyanoalkadienes by causing a diolefinic hydrocarbon to react with hydrogen cyanide and oxygen in the presence of palladium catalyst. The products are useful intermediates in the preparation of synthetic rubber, ABS plastic and other commercially important plastics.
摘要翻译：提供了通过在钯催化剂存在下使二烯烃与氰化氢和氧反应来制备氰基链二烯的方法。该产品是制备合成橡胶，ABS塑料等商业重要塑料的有用中间体。

9. 发明授权

US3574701A Process for producing ethylenically unsaturated aliphatic nitriles 失效
标题翻译：生产乙烯不饱和脂肪酸硝基酯的方法
公开(公告)号：US3574701A
公开(公告)日：1971-04-13
申请号：US3574701D
申请日：1969-05-06
申请人： ASAHI CHEMICAL IND
发明人： KOMINAMI NAOYA , TAMURA NOBUHIRO , NAKAJIMA HITOSHI
IPC分类号： B01J23/72 , B04B1/14 , B04B1/18 , C07C121/04
CPC分类号： C07C253/10 , B04B1/18 , B04B11/06 , Y02P20/52 , C07C255/08 , C07C255/07
摘要： PROCESS FOR PRODUCING ETHYLENICALLY UNSATURATED ALIPHATIC NITRILES OF ACRYLONITRILE, METHACRYLONITRILE, CROTONITRILE, 1-CYANO-BUTENE-1, 2-CYANO-BUTENE-1, 2-CYANO-BUTENE-2 AND 1-CYANO-2-METHYL-PROPENE-1, BY REACTING AN OLEFINIC HYDROCARBON CONTAINING 2 TO 4 CARBON ATOMS I.E. ETHYLENE, PROPYLENE, NORMAL BUTYLENE AND ISOBUTYLENE WITH HYDROGEN CYANIDE AND OXYGEN OR A MOLECULAR OXYGEN CONTAINING GAS IN THE GASEOUS PHASE IN THE PRESENCE OF A CATALYST SELECTED FROM THE GROUP CONSISTING OF THE OXIDES OF RHODIUM SELECTED FROM THE GROUP CONSISTING OF RHO, RH2O3, RHO3 AND RHO2; THE HYDROXIDES OF PALLADIUM AND RHODIUM SELECTED FROM THE GROUP CONSISTING OF PD(OH)2, PD(OH)4, RH(OH)3 AND RH(OH)4; THE CHLORIDES OF PALLADIUM AND RHODIUM SELECTED FROM THE GROUP CONSISTING OF PDCL, PDCL2, PDCL3, PDCL4, RHCL2 AND RHCL3; THE BROMIDES OF PALLADIUM AND RHODIUM SELECTED FROM THE GROUP CONSISTING OF PDBR2 AND RHBR3; THE NITRATES OF PALLADIUM AND RHODIUM SELECTED FROM THE GROUP CONSISTING OF PD(NO3)2 AND RH(NO3)3; PD(CH)2 AND PD(OCOCH3)2 AT A TEMPERATURE OF 200*C.
摘要翻译：用于间歇排放污泥的离心分离器。分离鼓的一个端部构件是垂直移动的阀活塞封闭件，以便打开和关闭设置在滚筒外周处的污泥排放喷嘴。阀活塞关闭形成滚筒中污泥室的一端。在污泥室的径向向内，盖子安装在分离器鼓中，覆盖阀活塞封闭件的一部分，盖和阀活塞封闭件处于滑动密封接触处，在阀活塞封闭件的鼓侧上提供腔室，用于接收并保持流体以迫使阀活塞关闭到打开位置。在阀活塞关闭的另一侧，设置有用于接收用于关闭阀的流体的腔室。

10. 发明授权

US3520915A Process for the dehydrogenation of lower saturated aliphatic nitriles 失效
标题翻译：降低饱和脂肪酸硝基脱氢酶的方法
公开(公告)号：US3520915A
公开(公告)日：1970-07-21
申请号：US3520915D
申请日：1966-10-20
申请人： ASAHI CHEMICAL IND
发明人： KOMINAMI NAOYA , KAWARAZAKI KUSUO , CHONO MASAZUMI , NAKAJIMA HITOSHI
IPC分类号： B01J23/14 , B01J23/92 , C07C121/32
CPC分类号： C07C253/30 , B01J23/14 , B01J23/92 , Y02P20/52 , Y02P20/584 , C07C255/08

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