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1. 发明授权

US11236113B2 Hydrocarbon-soluble halogen and thiolate/magnesium exchange reagents 有权
公开(公告)号：US11236113B2
公开(公告)日：2022-02-01
申请号：US16651790
申请日：2018-09-20
申请人： ALBEMARLE GERMANY GMBH , Ludwig-Maximilians-Universität München
发明人： Paul Knochel , Dorothée Ziegler , Meike Simon
IPC分类号： C07B49/00 , C07F3/02 , C07C41/22 , C07C41/60 , C07D211/16 , C07C29/70 , C07C41/14 , C07F1/02
摘要： The invention relates to hydrocarbon-soluble halogen or thiolate/magnesium exchange reagents of the general formula R1MgR11-n(OR3)n.LiOR2.(1−n)LiOR3.aDonor in which: R1 is a C1-C8 alkyl and OR2 as well as OR3 are same or different and represent primary, secondary, or tertiary alkoxide residues having 3 to 18 carbon atoms, wherein R2 and/or R3 can for their part contain an alkoxy substituent OR4; a assumes a value of 0 to 2, n assumes a value between 0 and 1, and the donor is an organic molecule containing at least 2 nitrogen atoms.

2. 发明申请

US20160215000A1 Production And Use Of Zinc Amides 有权
标题翻译：生产和使用锌酰胺
公开(公告)号：US20160215000A1
公开(公告)日：2016-07-28
申请号：US15088285
申请日：2016-04-01
申请人： Ludwig-Maximilians-Universität München
发明人： Paul Knochel , Marc Mosrin
IPC分类号： C07F3/06 , C07D241/16 , C07D405/06 , C07D237/12 , C07D239/30
CPC分类号： C07F3/06 , C07D211/10 , C07D237/12 , C07D239/30 , C07D241/16 , C07D405/06 , C07F3/003
摘要： Compounds, methods of making the compounds and methods of using the compounds are generally described herein. The compounds are generally of formula R1R2N—ZnY LiY, wherein R1 and R2 are independently selected from H, aryl, heteroaryl containing one or more heteroatoms, alkyl, alkenyl, alkynyl, and silicon derivatives thereof; and each Y is independently selected from F, Cl, Br, I, CN, SCN, NCO, HalO3, HalO4, NO3, BF4, PF6, H, an alcoholate of formula OR5, a carboxylate of formula R5CO2; a thiolate of formula SR5, R5P(O)O2, SCOR5, SCSR5, OnSR5 and NOn, wherein n=2 or 3; wherein R5 is selected from substituted or unsubstituted aryls or heteroaryls containing 3 to 24 carbon atoms and one or more heteroatoms selected from B, O, N, S, Se, P, linear, branched or cyclic, substituted or unsubstituted alkyls, alkenyls, alkynyls or H; and wherein Hal is a halogen selected from Cl, Br and I.
摘要翻译：化合物，制备化合物的方法和使用化合物的方法一般在此描述。化合物通常为式R1R2N-ZnYLiY，其中R1和R2独立地选自H，芳基，含有一个或多个杂原子的杂芳基，其烷基，烯基，炔基和硅衍生物; 每个Y独立地选自F，Cl，Br，I，CN，SCN，NCO，HalO 3，HalO 4，NO 3，BF 4，PF 6，H，式OR 5的醇化物，式R 5 CO 2的羧酸酯; 式SR5，R5P（O）O2，SCOR5，SCSR5，OnSR5和NOn的硫醇盐，其中n = 2或3; 其中R 5选自具有3至24个碳原子的一个或多个选自B，O，N，S，Se，P，直链，支链或环状，取代或未取代的烷基，链烯基，炔基中的一个或多个杂原子的取代或未取代的芳基或杂芳基或H; 其中Hal是选自Cl，Br和I的卤素。

3. 发明授权

US09688701B2 Production and use of zinc amides 有权
公开(公告)号：US09688701B2
公开(公告)日：2017-06-27
申请号：US15088285
申请日：2016-04-01
申请人： Ludwig-Maximilians-Universität München
发明人： Paul Knochel , Marc Mosrin
IPC分类号： C07F3/06 , C07D211/10 , C07F3/00 , C07D237/12 , C07D239/30 , C07D241/16 , C07D405/06
CPC分类号： C07F3/06 , C07D211/10 , C07D237/12 , C07D239/30 , C07D241/16 , C07D405/06 , C07F3/003
摘要： Compounds, methods of making the compounds and methods of using the compounds are generally described herein. The compounds are generally of formula R1R2N—ZnY LiY, wherein R1 and R2 are independently selected from H, aryl, heteroaryl containing one or more heteroatoms, alkyl, alkenyl, alkynyl, and silicon derivatives thereof; and each Y is independently selected from F, Cl, Br, I, CN, SCN, NCO, HalO3, HalO4, NO3, BF4, PF6, H, an alcoholate of formula OR5, a carboxylate of formula R5CO2; a thiolate of formula SR5, R5P(O)O2, SCOR5, SCSR5, OnSR5 and NOn, wherein n=2 or 3; wherein R5 is selected from substituted or unsubstituted aryls or heteroaryls containing 3 to 24 carbon atoms and one or more heteroatoms selected from B, O, N, S, Se, P, linear, branched or cyclic, substituted or unsubstituted alkyls, alkenyls, alkynyls or H; and wherein Hal is a halogen selected from Cl, Br and I.

4. 发明申请

US20200239496A1 Hydrocarbon-Soluble Halogen and Thiolate/Magnesium Exchange Reagents 审中-公开
公开(公告)号：US20200239496A1
公开(公告)日：2020-07-30
申请号：US16651790
申请日：2018-09-20
申请人： ALBEMARLE GERMANY GMBH , Ludwig-Maximilans-Universität München
发明人： Paul Knochel , Dorothée Ziegler , Meike Simon
IPC分类号： C07F3/02 , C07C41/60 , C07D211/16 , C07C41/22
摘要： The invention relates to hydrocarbon-soluble halogen or thiolate/magnesium exchange reagents of the general formula R1MgR11−n(OR3)n·LiOR2·(1−n)LiOR3·aDonor in which: R1 is a C1-C8 alkyl and OR2 as well as OR3 are same or different and represent primary, secondary, or tertiary alkoxide residues having 3 to 18 carbon atoms, wherein R2 and/or R3 can for their part contain an alkoxy substituent OR4; a assumes a value of 0 to 2, n assumes a value between 0 and 1, and the donor is an organic molecule containing at least 2 nitrogen atoms.

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