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1. 发明申请

US20040072935A1 Fluoropolymers resistant to stress cracking 失效
标题翻译：耐应力开裂的含氟聚合物
公开(公告)号：US20040072935A1
公开(公告)日：2004-04-15
申请号：US10680537
申请日：2003-10-07
申请人： 3M Innovative Properties Company
发明人： Thomas J. Blong , Lisa P. Chen , Ralph Kaulbach , Friedrich Kloos , Georg Burkard
IPC分类号： C08F216/12
CPC分类号： C08F214/262
摘要： The invention provides a fluorothermoplastic composition comprising interpolymerized units derived from about 94 to about 97.5 mole percent (mol %) tetrafluoroethylene (TFE), about 2 to about 3 mol % perfluoro (propyl vinyl ether) (PPVE), and about 0.5 to about 3 mol % hexafluoropropylene (HFP). The invention also provides a fluorothermoplastic composition comprising interpolymerized units derived from about 94 to about 97 mol % TFE, about 0.75 to about 3 mol % PPVE, and about 1.5 to about 3.5 mol % HFP. These fluorothermoplastic compositions have a flex life that fits the equation: log(flex life cycles)null0.71null4.0*(MFI(null0.294)), a method of making fluorothermoplastic compositions, a method of improving stress crack resistance, and fluorothermoplastic articles.
摘要翻译：本发明提供一种含氟热塑性组合物，其包含衍生自约94至约97.5摩尔％（摩尔％）四氟乙烯（TFE），约2至约3摩尔％全氟（丙基乙烯基醚）（PPVE）和约0.5至约3 mol％六氟丙烯（HFP）。本发明还提供一种含氟热塑性组合物，其包含衍生自约94至约97摩尔％TFE，约0.75至约3摩尔％PPVE和约1.5至约3.5摩尔％HFP的互聚单元。这些氟热塑性组合物具有适合以下等式的柔性寿命：log（挠曲寿命周期）> = 0.71 + 4.0 *（MFI <（ - 0.294）>），制备含氟热塑性组合物的方法，改善抗应力开裂性的方法，和氟热塑性制品。

2. 发明申请

US20020013419A1 High purity fluoropolymers 失效
标题翻译：高纯度氟聚合物
公开(公告)号：US20020013419A1
公开(公告)日：2002-01-31
申请号：US09864649
申请日：2001-05-23
申请人： 3M Innovative Properties Company
发明人： Thomas J. Blong , Denis Duchesne , Gernot Loehr , Albert Killich , Tilman Zipplies , Ralph Kaulbach , Herbert Strasser
IPC分类号： C08F014/18
CPC分类号： C08F6/06 , C08F6/22 , C08L27/12
摘要： The invention relates to high purity fluoropolymers and processes for making such materials. These polymers are particularly suited for applications in the semiconductor industry. The process comprises removal of unstable polymer end groups by fluorination and removal of heavy metal impurities by extraction with an aqueous acid medium.
摘要翻译：本发明涉及高纯度氟聚合物及其制备方法。这些聚合物特别适用于半导体工业中的应用。该方法包括通过用含水酸性介质萃取氟化和除去重金属杂质来除去不稳定的聚合物端基。

3. 发明申请

US20040132927A1 High purity fluoropolymers 失效
公开(公告)号：US20040132927A1
公开(公告)日：2004-07-08
申请号：US10743208
申请日：2003-12-22
申请人： 3M Innovative Properties Company
发明人： Thomas J. Blong , Denis Duchesne , Gernot Loehr , Albert Killich , Tilman Zipplies , Ralph Kaulbach , Herbert Strasser
IPC分类号： C08L061/06
CPC分类号： C08F6/06 , C08F6/22 , C08L27/12
摘要： The invention relates to high purity fluoropolymers and processes for making such materials. These polymers are particularly suited for applications in the semiconductor industry. The process comprises removal of unstable polymer end groups by fluorination and removal of heavy metal impurities by extraction with an aqueous acid medium.

4. 发明申请

US20030130459A1 TETRAFLUOROETHYLENE/HEXAFLUOROPROPYLENE COPOLYMERS WITH HIGHER DRAWABILITY 失效
标题翻译：具有更高拉伸性的四氢氟乙烯/十六烷基二苯醚共聚物
公开(公告)号：US20030130459A1
公开(公告)日：2003-07-10
申请号：US10356227
申请日：2003-01-31
申请人： 3M Innovative Properties Company
发明人： Ralph Kaulbach , Albert Killich , Friedrich Kloos , Gernot Loehr , Ludwig Mayer , Erik Peters , Thomas J. Blong , Denis Duchesne
IPC分类号： C08F114/18 , C08F214/18
CPC分类号： C08F214/26 , B29C47/0004 , B29C47/0016 , B29C47/0021 , B29C47/0023 , B29K2027/18 , B29L2031/3462 , C08F8/22
摘要： A tetrafluoroethylene/hexafluoropropylene copolymer with high drawability is provided. Also provided is a process employing the polymer and an article coated with the polymer.
摘要翻译：提供了具有高拉伸性的四氟乙烯/六氟丙烯共聚物。还提供了使用聚合物和涂覆有聚合物的制品的方法。

5. 发明申请

US20040192868A1 Melt-processible thermoplastic fluoropolymers having improved processing characteristics and method of producing same 有权
标题翻译：具有改进的加工特性的可熔融加工的热塑性含氟聚合物及其制备方法
公开(公告)号：US20040192868A1
公开(公告)日：2004-09-30
申请号：US10774154
申请日：2004-02-06
申请人： 3M Innovative Properties Company
发明人： Harald Kaspar , Klaus Hintzer , Tilman Zipplies , Ralph Kaulbach
IPC分类号： C08F012/20
CPC分类号： H01B3/445 , C08F214/18 , C09D127/12
摘要： The present invention provides a fluoropolymer that is melt-processible and thermoplastic and that has a melting point between 100null C. and 320null C. The fluoropolymer is derived from (a) one or more gaseous fluorinated monomers, (b) one or more modifiers selected from (i) olefins having a bromine or iodine atom bonded to a carbon of the double bond of the olefin, (ii) olefins corresponding to formula (I): Xa2CnullCXanullRfnullBr nullnull(I) wherein each Xa independently represents hydrogen, fluorine, bromine, chlorine or iodine, Rf is a perfluoroalkylene group, typically having 1 to 8 carbon atoms, a perfluorooxyalkylene group or a perfluoropolyether group and (iii) mixtures thereof; and (c) optionally one or more comonomers selected from non-gaseous fluorinated monomers and non-fluorinated monomers. The resulting fluoropolymer has long chain branches. The invention further provides a method for making these polymers.
摘要翻译：本发明提供了可熔融加工和热塑性且熔点在100℃和320℃之间的含氟聚合物。该含氟聚合物衍生自（a）一种或多种气态氟化单体，（b）一种或多种选自（i）具有与烯烃双键结合的溴或碘原子的烯烃的改性剂，（ii）对应于式（I）的烯烃：X <= 2C = CX a -Rf-Br （I）其中每个X 5'独立地表示氢，氟，溴，氯或碘，Rf是通常具有1至8个碳原子的全氟亚烷基，全氟氧化烯基或全氟聚醚基和（iii）其混合物; 和（c）任选的一种或多种选自非气态氟化单体和非氟化单体的共聚单体。得到的含氟聚合物具有长链分支。本发明还提供了制备这些聚合物的方法。

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