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    • 5. 发明授权
    • Method for making colloidal nanocrystals
    • 制备胶态纳米晶体的方法
    • US07846216B2
    • 2010-12-07
    • US12002190
    • 2007-12-14
    • Ya-Dong LiFeng BaiDing-Sheng WangZi-Yang HuoWei ChenLi-Ping Liu
    • Ya-Dong LiFeng BaiDing-Sheng WangZi-Yang HuoWei ChenLi-Ping Liu
    • C01B15/013
    • C01B9/08B82Y30/00C01B19/007C01F17/0062C01G11/02C01G23/08C01G37/14C01G49/08C01P2004/04C01P2004/52C01P2004/62C01P2004/64C01P2006/90
    • A method for making colloidal nanocrystals includes the following steps: dissolving a nanocrystal powder in an organic solvent, and achieving a solution A of a concentration of 1-30 mg/ml; dissolving a surfactant in water, and achieving a solution B of a concentration of 0.002-0.05 mmol/ml; mixing the solution A and the solution B in a volume ratio of 1: (5-30), and achieving a mixture; stirring and emulsifying the mixture, until an emulsion C is achieved; removing the organic solvent from the emulsion C, and achieving a deposit; then washing the deposit with deionized water, and achieving colloidal nanocrystals. The present method for making colloidal nanocrystals is economical and timesaving, and has a low toxicity associated therewith. Thus, the method is suitable for industrial mass production. The colloidal nanocrystals made by the present method have a readily controllable size, a narrow size distribution, and good configuration.
    • 制备胶态纳米晶体的方法包括以下步骤:将纳米晶体粉末溶解在有机溶剂中,并获得浓度为1-30mg / ml的溶液A; 将表面活性剂溶解在水中,得到浓度为0.002〜0.05mmol / ml的溶液B; 以1:(5-30)的体积比混合溶液A和溶液B,得到混合物; 搅拌并乳化混合物,直到达到乳液C. 从乳液C中除去有机溶剂,并实现沉积; 然后用去离子水洗涤沉积物,并获得胶体纳米晶体。 本发明制备胶态纳米晶体的方法是经济的并且节省时间,并且与其相关的毒性低。 因此,该方法适用于工业量产。 通过本方法制备的胶体纳米晶体具有容易控制的尺寸,窄尺寸分布和良好的构型。