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1. 发明授权

US09068077B2 Light-conversion flexible polymer material and use thereof 有权
标题翻译：光转换柔性聚合物材料及其用途
公开(公告)号：US09068077B2
公开(公告)日：2015-06-30
申请号：US13496548
申请日：2010-09-15
申请人： Zhiguo Xiao , Ying Chang , Yulong Sui , Yuening Wu , Maolong Li
发明人： Zhiguo Xiao , Ying Chang , Yulong Sui , Yuening Wu , Maolong Li
IPC分类号： C08L83/00 , C08K3/24 , C08K3/34 , C08K3/30 , H01L33/00 , F21V9/10 , C08L83/04 , C09K11/02 , C08G77/04 , H01L33/50
CPC分类号： C08L83/04 , C08G77/04 , C08K3/24 , C09K11/02 , H01L33/501 , H01L33/505 , C08L83/00
摘要： A light-conversion flexible polymer material consists of an organic silicone rubber (bi-component addition thermal vulcanizing liquid silicone rubber, 20.0-75.0%), a diluting agent (silicone oil, 10.0-20.0%), a luminescent material (one or more of aluminate, silicate, siliconitride and oxysulfide luminescent materials, 15.0-65.0%) and auxiliary. The polymer material can be bent randomly as required. The polymer material is made by mixing raw materials uniformly in a blending container, inpouring the obtained mixture into a mold and thermal-curing. The polymer material is used on the surface of a blue-light LED and the luminescent material in the light-conversion flexible polymer material can be excitated by light emitted from the blue light LED to give out light, which is combined with residual blue light into white light. The polymer material can be widely used in light-source devices such as lamp, nixie tube and backlight.
摘要翻译：光转换柔性聚合物材料由有机硅橡胶（双组分加成热硫化液硅橡胶，20.0-75.0％），稀释剂（硅油，10.0-20.0％），发光材料（一种或多种）的铝酸盐，硅酸盐，硅氮化物和氧硫化物发光材料，15.0-65.0％）和辅助剂。聚合物材料可以根据需要随机弯曲。聚合物材料通过将原料均匀地混合在共混容器中，将所得混合物浸入模具中并热固化而制成。聚合物材料用于蓝光LED的表面，并且光转换柔性聚合物材料中的发光材料可以被从蓝色LED发出的光激发，以发出与剩余蓝色光合并的光白光。聚合物材料可广泛用于灯具，数码管和背光源等光源装置中。

2. 发明申请

US20120097896A1 BLUE-GREEN SILICATE LUMINESCENT MATERIAL 审中-公开
标题翻译：蓝绿色硅酸盐光泽材料
公开(公告)号：US20120097896A1
公开(公告)日：2012-04-26
申请号：US13319272
申请日：2010-05-05
申请人： Zhiguo Xiao , Xifeng Wang , Wei Xia , Shiyun Sang , Jianxiong Liu , Hongwei Zhang
发明人： Zhiguo Xiao , Xifeng Wang , Wei Xia , Shiyun Sang , Jianxiong Liu , Hongwei Zhang
IPC分类号： C09K11/79 , C09K11/85
CPC分类号： C09K11/7792 , Y02B20/181
摘要： The present invention provides blue-green silicate luminescent materials, which are rare earth activated alkaline-earth metals silicates having a formula of Ba1-bMbSi2O(5-a/2)Da:Eux, Lny, wherein M is one or two elements selected from the group consisting of Mg, Ca and Sr; D is one or two ions selected from the group consisting of Cl− and F−; Ln is an ion selected from Ce, Er, Pr or Mn; a, b, x, and y are molar coefficients and within following ranges: 0≦a
摘要翻译：本发明提供蓝色 - 绿色硅酸盐发光材料，它们是具有式Ba1-bMbSi2O（5-a / 2）Da:Eux，Lny的稀土活化的碱土金属硅酸盐，其中M是选自以下的一种或两种元素：由Mg，Ca和Sr组成的组; D是选自Cl-和F-的一种或两种离子; Ln是选自Ce，Er，Pr或Mn的离子; a，b，x和y是摩尔系数，并在以下范围内：0＆nlE; a <2,0＆nlE; b <0.5,0

3. 发明申请

US20120058322A1 WATERPROOF SELF-LUMINESCENT SPRAY-PAINTED FILM 审中-公开
标题翻译：防水自发光喷涂膜
公开(公告)号：US20120058322A1
公开(公告)日：2012-03-08
申请号：US13266679
申请日：2010-04-28
申请人： Zhiguo Xiao , Maolong Li , Yingying Li , Kuiwu Shao , Hongwei Zhang
发明人： Zhiguo Xiao , Maolong Li , Yingying Li , Kuiwu Shao , Hongwei Zhang
IPC分类号： B32B7/02 , B05D3/02 , B05D1/28 , B05D1/42 , B05D1/18 , B05D5/00 , B05D1/02
CPC分类号： B41M5/508 , B41M5/52 , B41M5/5218 , B41M5/5227 , B41M5/5245 , B41M5/5254 , Y10T428/24975
摘要： The invention provides a waterproof self-luminescent spray-painted film with a thickness of 0.150-1.560 mm. The film has, from top to bottom, ink reception layer (1), connection layer (2) and light-storing photo-luminescent film (3); wherein the ink reception layer (1) is prepared by mixing inorganic filler, adhesive, color fixing agent, coupling agent, surfactant, cross-linking agent, fluorescent whitening agent and water at a ratio. The film has good waterproof property, rapid ink-drying, clear image after being ink-jet printed, and high color density. The film is self-luminescent after absorbing external visible light, and is visible and has the illumination function of low lighting intensity in darkness after a pattern or character is printed on the surface of the film. The film can be widely used in various occasions, such as home decoration, hotels, corridors, office buildings, cinemas, warehouses, ship cabins, underpasses and the places in need of large scale printing and high-precision patterns.
摘要翻译：本发明提供了一种厚度为0.150-1.560mm的防水自发光喷涂膜。该墨水从上到下具有墨水接收层（1），连接层（2）和储光光致发光膜（3）。其中所述油墨接收层（1）通过以一定比例混合无机填料，粘合剂，着色剂，偶联剂，表面活性剂，交联剂，荧光增白剂和水来制备。该胶片具有良好的防水性能，快速的油墨干燥，喷墨打印后的图像清晰，色彩浓度高。在吸收外部可见光之后，该膜是自发光的，并且在图案或字符被印刷在膜的表面上之后，在黑暗中具有低照明强度的照明功能。该电影可广泛应用于家居装饰，酒店，走廊，办公楼，电影院，仓库，船舱，地下通道等需要大型印刷和高精度图案的场合。

4. 发明申请

US20100052513A1 SILICATE BASE LUMINESCENT MATERIALS HAVING MULTIPLE EMISSION PEAKS, PROCESSES FOR PREPARING THE SAME AND LIGHT EMITTING DEVICES USING THE SAME 有权
标题翻译：具有多个发射峰的硅酸盐基发光材料，其制备方法和使用该发光峰的发光装置
公开(公告)号：US20100052513A1
公开(公告)日：2010-03-04
申请号：US12377491
申请日：2007-08-15
申请人： Wei Xia , Yi Xin , Daqiang Hu , Zhiguo Xiao
发明人： Wei Xia , Yi Xin , Daqiang Hu , Zhiguo Xiao
IPC分类号： H01L33/00 , C09K11/61 , C09K11/79
CPC分类号： C09K11/7734 , C09K11/7792 , H01L33/483 , H01L33/502 , H01L33/507 , H01L2224/32245 , H01L2224/32257 , H01L2224/48091 , H01L2224/48247 , H01L2224/48257 , H01L2224/49107 , H01L2224/73265 , H01L2224/8592 , H01L2924/181 , Y02B20/181 , H01L2924/00014 , H01L2924/00 , H01L2924/00012
摘要： A silicate luminescent material excitable by an excitation light source having emissions in UV to blue light region, a process for producing the same, and a white light emitting device. The luminescent material has an emission spectrum with at least two peaks in a range of from 370 to 760 nm, and has a general chemical composition formula of aAO.bA′O.cSiO2:xEu.yLn.zM.δN, wherein A is selected from the group consisting of Sr, Ca, Ba, and combinations thereof; A′ is selected from the group consisting of Mg, Zn, and combinations thereof; Ln is selected from the group consisting of Nd, Dy, Ho, Tm, La, Ce, Er, Pr, Bi, Sm, Sn, Y, Lu, Ga, Sb, Tb, Mn, Pb and combinations thereof; M is one or a combination of halogen ions; N is selected from the group consisting of Li+, Na+, K+, Ag+, and combinations thereof; and a, b, c, x, y, z, and δ are molar coefficients.
摘要翻译：由具有紫外至蓝光区域的发射的激发光源可激发的硅酸盐发光材料，其制造方法和白色发光装置。发光材料具有在370至760nm范围内具有至少两个峰的发射光谱，并具有一般的化学组成分子式为：aA.bA'O.cSiO2：xEu.yLn.zM.δN，其中选择A 由Sr，Ca，Ba及其组合组成的组; A'选自Mg，Zn及其组合; Ln选自Nd，Dy，Ho，Tm，La，Ce，Er，Pr，Bi，Sm，Sn，Y，Lu，Ga，Sb，Tb，Mn，Pb及其组合; M是卤素离子之一或组合; N选自Li +，Na +，K +，Ag +及其组合; 和a，b，c，x，y，z和δ是摩尔系数。

5. 发明申请

US20080031797A1 SILICATE PHOSPHOR AND ITS MANUFACTURE METHOD AS WELL AS LIGHT-EMITTING DEVICE USING THE SAME 有权
标题翻译：硅酸盐及其制造方法作为使用其的发光装置
公开(公告)号：US20080031797A1
公开(公告)日：2008-02-07
申请号：US11754432
申请日：2007-05-29
申请人： Wei Xia , Jing Xu , Guangxu Lin , Xifeng Wang , Zhiguo Xiao
发明人： Wei Xia , Jing Xu , Guangxu Lin , Xifeng Wang , Zhiguo Xiao
IPC分类号： C01F17/00
CPC分类号： C09K11/774 , C09K11/7734 , C09K11/7792 , C09K11/7796 , C09K11/7797 , Y02B20/181
摘要： The invention relates to an ultraviolet to green light region silicate phosphor capable of being excited by radiation light source and its manufacturing method, particularly to white and multicolor systems light-emitting device. The material has luminous color in the range from blue to red color system. The essential composition of the phosphor is aMO.bM′O.SiO2.cR:xEu.yLn.zLv.δLm, wherein M is an element or a combination of elements selected from the group consisting of Sr, Ca, Ba and Zn; M′ is an element or a combination of elements selected from the group consisting of Mg, Cd and Be; R is one or two of B2O3 and P2O5; Ln is an element or a combination of elements selected from the group consisting of Nd, Dy, Ho, Tm, La, Ce, Er, Pr, Bi, Sm, Sn, Y, Lu, Ga, Sb, Tb, Mn and Pb; Lv is an element or a combination of elements selected from the group consisting of Cl, F, Br, I and S; Lm is an element or a combination of elements selected from the group consisting of Li, Na and K
摘要翻译：本发明涉及能够被辐射光源激发的紫外至绿光区域硅酸盐荧光体及其制造方法，特别涉及白色和多色系统的发光装置。该材料具有从蓝色到红色系统范围内的发光颜色。荧光体的基本组成是M 1，M 2 SiO 2，cR：xEu.yLn.zLv.deltaLm，其中M是元素或选自Sr ，Ca，Ba和Zn; M'是选自Mg，Cd和Be的元素或元素的组合; R是B 2 O 3和P 2 O 5 5中的一个或两个; Ln是选自Nd，Dy，Ho，Tm，La，Ce，Er，Pr，Bi，Sm，Sn，Y，Lu，Ga，Sb，Tb，Mn和Pb中的元素或元素的组合 ; Lv是选自Cl，F，Br，I和S的元素或元素的组合; Lm是选自Li，Na和K的元素或元素的组合

6. 发明申请

US20070296326A1 LIGHT-STORAGE SELF-LUMINESCENT GLASS AND THE PROCESS FOR PRODUCING THE SAME 审中-公开
标题翻译：光储存自发光玻璃及其生产方法
公开(公告)号：US20070296326A1
公开(公告)日：2007-12-27
申请号：US11851031
申请日：2007-09-06
申请人： Zhiguo Xiao , Jialing Dai , Xixian Luo , Jianxiong Liu , Wei Xia , Lifang Liu
发明人： Zhiguo Xiao , Jialing Dai , Xixian Luo , Jianxiong Liu , Wei Xia , Lifang Liu
IPC分类号： H01J63/04 , C03B9/00
CPC分类号： C09K11/7792 , C03C4/12 , C03C14/004 , C03C2214/04 , C03C2214/16
摘要： A light-storage self-luminescent glass is disclosed, comprising from 0.01 to 40% of a light-storage self-luminescent material activated by multiple ions and from 99.99 to 60% of a matrix glass; wherein the light-storage self-luminescent material has a particle size from 10 μm to 20 mm, and the matrix glass can be a low melting point glass or a common silicate glass. A process for producing the glass is also disclosed, comprising doping a light-storage self-luminescent material during the forming process of a common silicate glass, or thoroughly mixing low melting point glass powder with a light-storage self-luminescent material, and then heat treating the system at 700-1100° C. to obtain the light-storage self-luminescent glass. The process is simple and the cost is low.
摘要翻译：公开了一种储光自发光玻璃，其包含0.01〜40％的多重离子活化的储光自发光材料和99.99〜60％的基质玻璃; 其中，所述储光自发光材料的粒径为10μm〜20mm，所述基体玻璃可以为低熔点玻璃或普通硅酸盐玻璃。还公开了一种制造玻璃的方法，包括在普通硅酸盐玻璃的成型过程中掺杂储光自发光材料，或将低熔点玻璃粉末与储光自发光材料充分混合，然后在700-1100℃下对系统进行热处理以获得储光自发光玻璃。流程简单，成本低廉。

7. 发明申请

US20130089729A1 PEELABLE LIGHT CONVERSION LUMINESCENT FILM 审中-公开
标题翻译：可变光转换发光膜
公开(公告)号：US20130089729A1
公开(公告)日：2013-04-11
申请号：US13699136
申请日：2010-05-20
申请人： Zhiguo Xiao , Maolong Li , Ying Chang , Yulong Sui , Xingjian Dai , Yuening Wu , Hongwei Zhang
发明人： Zhiguo Xiao , Maolong Li , Ying Chang , Yulong Sui , Xingjian Dai , Yuening Wu , Hongwei Zhang
IPC分类号： B32B27/08 , B32B33/00
CPC分类号： B32B27/08 , B32B33/00 , C08J7/042 , C08J2367/00 , C08J2427/12 , C08J2483/04 , C09D5/20 , C09D183/04 , H01L33/501 , H01L2933/0041 , Y10T428/264
摘要： A peelable light conversion luminescent film consisting of a substrate and a light conversion coating layer thereon is provided. The light conversion coating layer consists of a fluorescent material, a two-component silicone resin, a diluent and an adjuvant. The substrate is a fluorine-containing polyester film which can be easily peeled off from the light conversion coating layer when using the light conversion film. The fluorine-containing polyester film can function as a substrate and as a protective film. The fluorine-containing polyester film can be easily peeled off to avoid the deformation of light conversion coating layer. After the peeling off from the fluorine-containing polyester film, the light refraction is reduced and the luminescent efficiency is increased. The fluorescent material is pretreated with ethanol-alkoxy oligomeric polysiloxane mixture solution, its compatibility with silicone resin is enhanced, the surface condition of the coated film is improved, and the uniformity of the film is increased.
摘要翻译：提供由基板和其上的光转换涂层组成的可剥离的光转换发光膜。光转换涂层由荧光材料，双组分有机硅树脂，稀释剂和佐剂组成。基板是使用光转换膜时可以容易地从光转换涂层剥离的含氟聚酯膜。含氟聚酯膜可以用作基材和保护膜。含氟聚酯膜可以容易地剥离，以避免光转化涂层的变形。从含氟聚酯膜剥离后，光折射降低，发光效率提高。荧光材料用乙醇 - 烷氧基低聚聚硅氧烷混合溶液预处理，增强了与硅树脂的相容性，改善了涂膜的表面状态，提高了膜的均匀性。

8. 发明授权

US07998364B2 Silicate phosphor and its manufacture method as well as light-emitting device using the same 有权
标题翻译：硅酸盐荧光粉及其制造方法以及使用其的发光装置
公开(公告)号：US07998364B2
公开(公告)日：2011-08-16
申请号：US11754432
申请日：2007-05-29
申请人： Wei Xia , Jing Xu , Guangxu Lin , Xifeng Wang , Zhiguo Xiao
发明人： Wei Xia , Jing Xu , Guangxu Lin , Xifeng Wang , Zhiguo Xiao
IPC分类号： C09K11/59 , C09K11/63 , C09K11/73 , C09K11/55 , C09K11/54
CPC分类号： C09K11/774 , C09K11/7734 , C09K11/7792 , C09K11/7796 , C09K11/7797 , Y02B20/181
摘要： The invention relates to an ultraviolet to green light region silicate phosphor capable of being excited by radiation light source and its manufacturing method, particularly to white and multicolor systems light-emitting device. The material has luminous color in the range from blue to red color system. The essential composition of the phosphor is aMO.bM′O.SiO2.cR:xEu.yLn.zLv.δLm, wherein M is an element or a combination of elements selected from the group consisting of Sr, Ca, Ba and Zn; M′ is an element or a combination of elements selected from the group consisting of Mg, Cd and Be; R is one or two of B2O3 and P2O5; Ln is an element or a combination of elements selected from the group consisting of Nd, Dy, Ho, Tm, La, Ce, Er, Pr, Bi, Sm, Sn, Y, Lu, Ga, Sb, Tb, Mn and Pb; Lv is an element or a combination of elements selected from the group consisting of Cl, F, Br, I and S; Lm is an element or a combination of elements selected from the group consisting of Li, Na and K.
摘要翻译：本发明涉及能够被辐射光源激发的紫外至绿光区域硅酸盐荧光体及其制造方法，特别涉及白色和多色系统的发光装置。该材料具有从蓝色到红色系统范围内的发光颜色。荧光体的基本组成是M，SbMO，SiO 2，cR：xEu.yLn.zLv.δLm，其中M是选自Sr，Ca，Ba和Zn的元素或元素的组合; M'是选自Mg，Cd和Be的元素或元素的组合; R是B2O3和P2O5中的一种或两种; Ln是选自Nd，Dy，Ho，Tm，La，Ce，Er，Pr，Bi，Sm，Sn，Y，Lu，Ga，Sb，Tb，Mn和Pb中的元素或元素的组合 ; Lv是选自Cl，F，Br，I和S的元素或元素的组合; Lm是选自Li，Na和K的元素或元素的组合。

9. 发明申请

US20070069181A1 Long afterglow luminescent material and its manufacturing method 有权
标题翻译：长余辉发光材料及其制造方法
公开(公告)号：US20070069181A1
公开(公告)日：2007-03-29
申请号：US11518603
申请日：2006-09-08
申请人： Xixian Luo , Wei Xia , Zhiguo Xiao , Jingjie Yu , Jinxia Duan , Qi Chai
发明人： Xixian Luo , Wei Xia , Zhiguo Xiao , Jingjie Yu , Jinxia Duan , Qi Chai
IPC分类号： C09K11/08 , C09K11/77
CPC分类号： C09K11/886 , C09K11/7738 , C09K11/774 , C09K11/7795 , C09K11/7796 , C09K11/7797
摘要： A long afterglow luminescent material of the formula aMO.bM′ (SβSe1-β).cAl2O3.d B2O3.eP2O5: XEu.yLn, wherein M is/are selected from Sr, Ca, Ba, and Mg, and any combinations thereof; M′ is/are selected from Sr, Ca, and Ba, and any combinations thereof; Ln is/are selected from Nd, Dy, Ho, Tm, La, Ce, Er, Pr, Bi, and Sm, and any combinations thereof; a, b, c, d, e, x and y are mole ratios, wherein 0.5
摘要翻译：式aMO.bM'的长余辉发光材料（S，β1-β）。cAl 2 O 3 其中M是（Ⅳ），其中M是（Ⅳ），其中M是 /选自Sr，Ca，Ba和Mg及其任何组合; M'选自Sr，Ca和Ba及其任何组合; Ln选自Nd，Dy，Ho，Tm，La，Ce，Er，Pr，Bi和Sm及其任何组合; a，b，c，d，e，x和y是摩尔比，其中0.5

10. 发明申请

US20050179008A1 Light-storage self-luminescent glass and the process for producing the same 审中-公开
标题翻译：光存储自发光玻璃及其制造方法
公开(公告)号：US20050179008A1
公开(公告)日：2005-08-18
申请号：US10782621
申请日：2004-02-18
申请人： Zhiguo Xiao , Jialing Dai , Xixian Luo , Jianxiong Liu , Wei Xia , Lifang Liu
发明人： Zhiguo Xiao , Jialing Dai , Xixian Luo , Jianxiong Liu , Wei Xia , Lifang Liu
IPC分类号： C03C1/00 , C03C4/12 , C03C14/00 , C09K11/77
CPC分类号： C09K11/7792 , C03C4/12 , C03C14/004 , C03C2214/04 , C03C2214/16
摘要： A light-storage self-luminescent glass is disclosed, comprising from 0.01 to 40% of a light-storage self-luminescent material activated by multiple ions and from 99.99 to 60% of a matrix glass; wherein the light-storage self-luminescent material has a particle size from 10 μm to 20 mm, and the matrix glass can be a low melting point glass or a common silicate glass. A process for producing the glass is also disclosed, comprising doping a light-storage self-luminescent material during the forming process of a common silicate glass, or thoroughly mixing low melting point glass powder with a light-storage self-luminescent material, and then heat treating the system at 700-1100° C. to obtain the light-storage self-luminescent glass. The process is simple and the cost is low.
摘要翻译：公开了一种储光自发光玻璃，其包含0.01〜40％的多重离子活化的储光自发光材料和99.99〜60％的基质玻璃; 其中，所述储光自发光材料的粒径为10μm〜20mm，所述基体玻璃可以为低熔点玻璃或普通硅酸盐玻璃。还公开了一种制造玻璃的方法，包括在普通硅酸盐玻璃的成型过程中掺杂储光自发光材料，或将低熔点玻璃粉末与储光自发光材料充分混合，然后在700-1100℃下对系统进行热处理以获得储光自发光玻璃。流程简单，成本低廉。

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