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1. 发明授权

US09828309B2 Method for producing monocyclic aromatic hydrocarbons 有权
公开(公告)号：US09828309B2
公开(公告)日：2017-11-28
申请号：US14119281
申请日：2012-05-24
申请人： Shinichiro Yanagawa , Yuichiro Fujiyama , Yasuyuki Iwasa , Ryoji Ida , Masahide Kobayashi , Susumu Yasui , Yoshishige Sugi , Atsushi Fukui , Atsuro Nagumo
发明人： Shinichiro Yanagawa , Yuichiro Fujiyama , Yasuyuki Iwasa , Ryoji Ida , Masahide Kobayashi , Susumu Yasui , Yoshishige Sugi , Atsushi Fukui , Atsuro Nagumo
IPC分类号： C07C4/06 , C10G35/06 , B01D45/12 , B01J8/00 , C10G35/14 , C10G35/04 , C10G35/10 , B01J29/40 , B01J29/70 , B01J29/87
CPC分类号： C07C4/06 , B01D45/12 , B01J8/005 , B01J29/40 , B01J29/70 , B01J29/87 , C10G35/04 , C10G35/065 , C10G35/10 , C10G35/14 , C10G2300/1044 , C10G2300/1048 , C10G2300/301 , C10G2400/30
摘要： Method for producing monocyclic aromatic hydrocarbons includes a cracking and reforming reaction step of obtaining products containing monocyclic aromatic hydrocarbons having 6 to 8 carbon atoms and a heavy fraction having 9 or more carbon atoms by bringing the feedstock oil into contact with a catalyst for producing monocyclic aromatic hydrocarbons containing crystalline aluminosilicate to cause a reaction, a catalyst separation step of separating and removing the catalyst for producing monocyclic aromatic hydrocarbons together with tricyclic aromatic hydrocarbons contained in the products from a mixture of the products and a small amount of the catalyst for producing monocyclic aromatic hydrocarbons carried by the products, both of which are derived in the cracking and reforming reaction step, and a purification and recovery step of purifying and recovering the monocyclic aromatic hydrocarbons having 6 to 8 carbon atoms which are separated from the products formed in the cracking and reforming reaction step.

2. 发明授权

US09567531B2 Fluid catalytic cracking process, and gasoline and liquefied petroleum gas obtained by the process 有权
标题翻译：流化催化裂化过程，以及汽油和液化石油气得到的过程
公开(公告)号：US09567531B2
公开(公告)日：2017-02-14
申请号：US12575503
申请日：2009-10-08
申请人： Yuichiro Fujiyama , Toshiaki Okuhara , Shigeko Okuhara
发明人： Yuichiro Fujiyama , Toshiaki Okuhara
IPC分类号： C10G11/18 , C10G51/02 , C10L1/06 , C10L3/12
CPC分类号： C10G11/18 , C10G51/026 , C10L1/06 , C10L3/12
摘要： The fluid catalytic cracking process according to the present invention includes a first step of feeding a feedstock to a first fluid catalytic cracker, and catalytically cracking the feedstock in the first fluid catalytic cracker, so as to produce a fraction (LCO) having a boiling range of 221 to 343° C. and having a total aromatic content of 40 to 80 volume %; and a second step of feeding an oil to be processed containing the fraction to a second fluid catalytic cracker having a reaction zone, a separation zone, a stripping zone, and a regeneration zone, and catalytically cracking the oil in the reaction zone of the second fluid catalytic cracker, in the presence of a cracking catalyst, at an outlet temperature of the reaction zone of 550 to 750° C., a contact time between the oil and the catalyst of 0.1 to 1 second, and a catalyst/oil ratio of 20 to 40 wt/wt.
摘要翻译：根据本发明的流化催化裂化方法包括将原料进料到第一流化催化裂化器并在第一流化催化裂化器中催化裂化原料的第一步骤，以产生沸点范围的馏分（LCO）的221至343℃，总芳族含量为40至80体积％; 以及第二步骤，将含有该馏分的待处理油被供给到具有反应区，分离区，汽提区和再生区的第二流化催化裂化器，并且在第二流化催化裂化反应区中的油催化裂化流化催化裂化器，在裂化催化剂存在下，反应区出口温度为550-750℃，油与催化剂之间的接触时间为0.1至1秒，催化剂/油比为 20〜40wt / wt。

3. 发明申请

US20140200378A1 METHOD FOR PRODUCING MONOCYCLIC AROMATIC HYDROCARBONS 有权
标题翻译：生产单环芳香烃的方法
公开(公告)号：US20140200378A1
公开(公告)日：2014-07-17
申请号：US14119281
申请日：2012-05-24
申请人： Shinichiro Yanagawa , Yuichiro Fujiyama , Yasuyuki Iwasa , Ryoji Ida , Masahide Kobayashi , Susumu Yasui , Yoshishige Sugi , Atsushi Fukui , Atsuro Nagumo
发明人： Shinichiro Yanagawa , Yuichiro Fujiyama , Yasuyuki Iwasa , Ryoji Ida , Masahide Kobayashi , Susumu Yasui , Yoshishige Sugi , Atsushi Fukui , Atsuro Nagumo
IPC分类号： C07C4/06
CPC分类号： C07C4/06 , B01D45/12 , B01J8/005 , B01J29/40 , B01J29/70 , B01J29/87 , C10G35/04 , C10G35/065 , C10G35/10 , C10G35/14 , C10G2300/1044 , C10G2300/1048 , C10G2300/301 , C10G2400/30
摘要： Method for producing monocyclic aromatic hydrocarbons includes a cracking and reforming reaction step of obtaining products containing monocyclic aromatic hydrocarbons having 6 to 8 carbon atoms and a heavy fraction having 9 or more carbon atoms by bringing the feedstock oil into contact with a catalyst for producing monocyclic aromatic hydrocarbons containing crystalline aluminosilicate to cause a reaction, a catalyst separation step of separating and removing the catalyst for producing monocyclic aromatic hydrocarbons together with tricyclic aromatic hydrocarbons contained in the products from a mixture of the products and a small amount of the catalyst for producing monocyclic aromatic hydrocarbons carried by the products, both of which are derived in the cracking and reforming reaction step, and a purification and recovery step of purifying and recovering the monocyclic aromatic hydrocarbons having 6 to 8 carbon atoms which are separated from the products formed in the cracking and reforming reaction step.
摘要翻译：制备单环芳烃的方法包括裂解和重整反应步骤，通过使原料油与用于制备单环芳族化合物的催化剂接触，得到含有6至8个碳原子的单环芳烃和具有9个或更多个碳原子的重馏分的产物含有结晶硅铝酸盐的碳氢化合物引起反应的催化剂分离步骤，用于分离和除去产物中含有的三环芳烃与单一芳族烃的混合物和少量用于制备单环芳族化合物的催化剂由裂解和重整反应步骤中衍生的产物携带的烃和净化回收步骤，其纯化和回收与裂化中形成的产物分离的具有6至8个碳原子的单环芳烃和重整反应步骤。

4. 发明授权

US08101132B2 Mixing apparatus 有权
标题翻译：混合装置
公开(公告)号：US08101132B2
公开(公告)日：2012-01-24
申请号：US12373103
申请日：2007-07-10
申请人： Yuichiro Fujiyama , Toshiaki Okuhara , Shigeko Okuhara, legal representative
发明人： Yuichiro Fujiyama , Toshiaki Okuhara
IPC分类号： B01J8/08 , B01F15/00
CPC分类号： B01F5/045 , B01F3/12 , B01F5/0256 , B01F5/205 , B01J8/003 , B01J8/004
摘要： To provide a mixing device capable of effectively mixing stock oil with a catalyst, while increasing the amount of throughput, the relations of 8.0≧Q×(W/D)/(u1+u2), Q=300 to 2000 [kg/m2s], W/D=0.2 to 0.5, u1=5 to 300 [m/s], and u2=5 to 300 [m/s] are satisfied when a mass flow per unit area of a moving bed is Q [kg/nes], the difference between an outer diameter and an inner diameter of the moving bed is W [m], an inner diameter of a reaction tube is D [m], a linear velocity of a horizontal component of the stock oil at a jet orifice of the internal stock oil injection nozzle u1 [m/s], and a linear velocity of a horizontal component of the stock oil at a jet orifice of the external stock oil injection nozzle u2 [m/s].
摘要翻译：为了提供能够有效地混合原油与催化剂的混合装置，在增加生产量的同时，8.0≥Q×（W / D）/（u1 + u2），Q = 300〜2000 [kg / m 2 ]，当移动床的每单位面积质量流量为Q [kg / s]时，W / D = 0.2〜0.5，u1 = 5〜300 [m / s]，u2 = 5〜300 [m / nes]，移动床的外径和内径之差为W [m]，反应管的内径为D [m]，喷射时原油的水平分量的线速度内部原油喷射喷嘴u1 [m / s]的孔口和外部原油喷射喷嘴u2 [m / s]的喷射口处的原料油的水平分量的线速度。

5. 发明授权

US08083824B2 Gas-solid separator 有权
标题翻译：气固分离器
公开(公告)号：US08083824B2
公开(公告)日：2011-12-27
申请号：US12373136
申请日：2007-07-05
申请人： Yuichiro Fujiyama , Toshiaki Okuhara , Shigeko Okuhara, legal representative
发明人： Yuichiro Fujiyama , Toshiaki Okuhara
IPC分类号： B01D45/00
CPC分类号： B01D45/12 , B04C5/06 , B04C5/081 , B04C5/12 , B04C5/13 , C10G11/18 , Y10S55/30
摘要： A gas-solid separator has: an inner cylinder 10 having a closed lower end 11 and an opened upper end 1, and extending in a vertical direction; and an outer cylinder 2 that coaxially covers the inner cylinder 10 from the outside and has a gas vent port 6 formed on the upper end side and communicating with an exterior, wherein a plurality of axially extending long holes 4 are formed on a side surface on the lower end 11 side of the inner cylinder 10 in a circumferential direction, one of long side edge parts of each of the long holes 4 is provided with a guide blade 5 that protrudes outward and is inclined circumferentially so as to cover the long hole 4, and in a section of the outer cylinder 2 that surrounds the plurality of long holes 4 of the inner cylinder 10, an inner diameter D1 of a lower part is larger than an inner diameter D2 of an upper part.
摘要翻译：气固分离器具有：内筒10，其具有封闭的下端11和敞开的上端1，并沿垂直方向延伸; 以及从外部同轴地覆盖内筒10并具有形成在上端侧并与外部连通的排气口6的外筒2，其中在侧面上形成有多个轴向延伸的长孔4 内圆筒10的下端部11的圆周方向上，长孔部4的长边缘部分之一设置有向外突出并沿周向倾斜的导向叶片5，以覆盖长孔4 ，并且在外筒2的包围内筒10的多个长孔4的部分中，下部的内径D1大于上部的内径D2。

6. 发明授权

US08070846B2 Method of designing gas-solid separator 有权
标题翻译：气固分离器设计方法
公开(公告)号：US08070846B2
公开(公告)日：2011-12-06
申请号：US12373084
申请日：2007-07-05
申请人： Yuichiro Fujiyama , Toshiaki Okuhara , Shigeko Okuhara, legal representative , Akira Uchiura
发明人： Yuichiro Fujiyama , Toshiaki Okuhara , Akira Uchiura
IPC分类号： B01D47/00
CPC分类号： B01D45/12 , B01D45/06 , B04C5/06 , B04C5/081 , B04C5/103 , B04C5/12 , B04C5/13 , Y10S55/03
摘要： A method for operating a gas-solid separator that has: an inner cylinder 10 having a closed lower end 11 and an opened upper end 1, and extending in a vertical direction; an outer cylinder 2 that coaxially covers the inner cylinder 10 from the outside and has a gas vent port 6 formed on the upper end side of the inner cylinder and communicating with an exterior; and a plurality of axially extending long holes 4 having a length L[m] and formed on a side surface on the lower end 11 side of the inner cylinder 10 in a circumferential direction, one of long side edge parts of each of the long holes being provided with a guide blade 5 that protrudes outward and is inclined circumferentially so as to cover the long hole 4, wherein the length L of each long hole 4 is defined such as to satisfy an expression of non-dimensional Stokes number St=(ρpdp2/(18μ))·U/L≧0.3, where U[m/s] represents a cross-sectional average linear velocity of a mixture of gas and solid particles that is supplied downward from the opening 1 of the inner cylinder 4, ρp[kg/m3] a particle density of the solid particles, dp[m] an average particle diameter of the solid particles, and μ[Pa·s] a viscosity of the gas.
摘要翻译：一种操作气固分离器的方法，该气固分离器具有：内筒10，其具有封闭的下端11和敞开的上端1，并沿垂直方向延伸; 外筒2，其从外部同轴地覆盖内筒10，并且具有形成在内筒的上端侧并与外部连通的排气口6; 以及沿圆周方向形成在内筒10的下端11侧的侧面上的具有长度L [m]的多个轴向延伸的长孔4，每个长孔的长边缘部分之一设置有向外突出并沿圆周方向倾斜以覆盖长孔4的导向叶片5，其中每个长孔4的长度L被定义为满足无量纲斯托克斯数St =（＆rgr ; pdp2 /（18μ））·U /L≥0.3，其中U [m / s]表示从内筒4的开口1向下供给的气体和固体颗粒的混合物的截面平均线速度，固体颗粒的颗粒密度，固体颗粒的平均粒径dp [m]，气体的粘度μ[Pa·s]，p [kg / m3]。

7. 发明申请

US20110024907A1 SEMICONDUCTOR DEVICE AND METHOD OF MANUFACTURING THE SAME 审中-公开
标题翻译：半导体器件及其制造方法
公开(公告)号：US20110024907A1
公开(公告)日：2011-02-03
申请号：US12838446
申请日：2010-07-17
申请人： Yuichiro FUJIYAMA
发明人： Yuichiro FUJIYAMA
IPC分类号： H01L23/48 , H01L21/768
CPC分类号： H01L23/485 , H01L21/31053 , H01L21/3212 , H01L21/76816 , H01L21/76819 , H01L21/7684 , H01L21/76885 , H01L21/823475 , H01L23/5226 , H01L23/544 , H01L29/665 , H01L29/7833 , H01L2223/54426 , H01L2223/54453 , H01L2924/0002 , H01L2924/00
摘要： To provide a technique capable of improving the reliability on electric properties of a semiconductor device by devising the shape of the upper surface of a plug. A plug of the present invention has an upwardly convex dome-like shape in which the upper surface thereof projects from the surface (upper surface) of a contact interlayer insulating film. That is, the plug has the upper surface of an upwardly convex dome-like shape, wherein the height of the top edge portion of a barrier conductive film is larger than that of the upper surface of the contact interlayer insulating film, and the height of the top edge portion of a tungsten film is larger than that of the top edge portion of the barrier conductive film.
摘要翻译：提供通过设计插头的上表面的形状来提供能够提高半导体器件的电性能的可靠性的技术。本发明的塞子具有向上凸起的圆顶状，其上表面从接触层间绝缘膜的表面（上表面）突出。也就是说，插头具有向上凸起的穹顶形状的上表面，其中阻挡导电膜的顶部边缘部分的高度大于接触层间绝缘膜的上表面的高度，钨膜的上边缘部分大于阻挡导电膜的顶部边缘部分。

8. 发明申请

US20100186356A1 GAS-SOLID SEPARATOR 有权
标题翻译：气固分离器
公开(公告)号：US20100186356A1
公开(公告)日：2010-07-29
申请号：US12373072
申请日：2007-07-05
申请人： Yuichiro Fujiyama , Toshiaki Okuhara , Shigeko Okuhara
发明人： Yuichiro Fujiyama , Toshiaki Okuhara , Shigeko Okuhara
IPC分类号： B01D45/12 , B01D45/08 , B04C3/00
CPC分类号： B01D45/12 , B04C5/06 , C10G11/18 , C10G70/04 , Y10S55/30
摘要： A gas-solid separator has: an inner cylinder 10 having a closed lower end 11 and an opened upper end 1, and extending in a vertical direction; and an outer cylinder 2 that coaxially covers the inner cylinder 10 from the outside and has a gas vent port 6 formed on the upper end side of the inner cylinder and communicating with an exterior, wherein a plurality of axially extending long holes 4 are formed on a side surface on the lower end 11 side of the inner cylinder 10 in a circumferential direction, one of long side edge parts of each of the long holes 4 is provided with a guide blade 5 that protrudes outward and is inclined circumferentially so as to cover the long hole 4, and a part between the long holes 4 of the inner cylinder 10 is concaved in a center direction of the inner cylinder 10.
摘要翻译：气固分离器具有：内筒10，其具有封闭的下端11和敞开的上端1，并沿垂直方向延伸; 以及从外部同轴地覆盖内筒10并具有形成在内筒的上端侧并与外部连通的排气口6的外筒2，其中多个轴向延伸的长孔4形成在在内筒10的下端11侧的周向的侧面上，长孔4的长边缘部之一设置有向外突出并且周向倾斜的导向叶片5，以覆盖内筒10的长孔4之间的长孔4在内筒10的中心方向凹陷。

9. 发明授权

US5904837A Process for fluid catalytic cracking of oils 失效
标题翻译：油的流化催化裂化方法
公开(公告)号：US5904837A
公开(公告)日：1999-05-18
申请号：US944195
申请日：1997-10-03
申请人： Yuichiro Fujiyama
发明人： Yuichiro Fujiyama
IPC分类号： C10G11/18 , C10G11/00
CPC分类号： C10G11/18
摘要： A process for the fluid catalytic cracking of oils, wherein an oil is brought into contact with catalyst particles using a fluid catalytic cracking reactor under the following conditions: a) a reaction zone outlet temperature of 580 to 630.degree. C., catalyst/oil ratio of 15 to 50 wt./wt., contact time of 0.1 to 3.0 sec.; b) a catalyst-concentrated phase temperature in the regenerating zone of 670 to 800.degree. C.; and c) a temperature of regenerated catalyst to be forwarded into the reaction zone of 610 to 665.degree. C.; thereby producing light fraction olefins. The process increases the cracking rate of heavy fractions of oils while producing a lessened amount of dry gases generated by the overcracking of light fractions to obtain light fraction olefins in a high yield.
摘要翻译：一种用于流体催化裂化油的方法，其中在下列条件下使用流化催化裂化反应器使油与催化剂颗粒接触：a）反应区出口温度为580至630℃，催化剂/油比为15〜50重量/重量，接触时间为0.1〜3.0秒。 b）再生区的催化剂浓缩相温度为670〜800℃。和c）再生催化剂的温度进入610至665℃的反应区; 从而生产轻馏分烯烃。该方法提高了重馏分油的裂解率，同时产生了轻馏分过度裂解产生的干气减少量，从而以高产率获得轻馏分烯烃。

10. 发明授权

US09862654B2 Method for producing xylene 有权
公开(公告)号：US09862654B2
公开(公告)日：2018-01-09
申请号：US14119302
申请日：2012-05-24
申请人： Shinichiro Yanagawa , Yuichiro Fujiyama , Yasuyuki Iwasa , Ryoji Ida , Susumu Yasui , Yoshishige Sugi , Atsushi Fukui , Akira Utatsu
发明人： Shinichiro Yanagawa , Yuichiro Fujiyama , Yasuyuki Iwasa , Ryoji Ida , Susumu Yasui , Yoshishige Sugi , Atsushi Fukui , Akira Utatsu
IPC分类号： C07C2/70 , C10G35/06 , C07C6/12 , C10G45/64 , C10G69/04 , C10G11/05 , C10G29/20
CPC分类号： C07C2/70 , C07C6/126 , C07C2529/87 , C10G11/05 , C10G29/205 , C10G35/065 , C10G45/64 , C10G69/04 , C10G2300/301 , C10G2400/30 , C07C15/08
摘要： A method for producing xylene from feedstock oil includes a cracking/reforming reaction step of bringing the feedstock oil into contact with a catalyst to produce monocyclic aromatic hydrocarbons; a separation/recovery step of separating and recovering, from a product obtained by the cracking/reforming reaction step, a fraction A containing monocyclic aromatic hydrocarbons having a 10 vol % distillation temperature of 75° C. or higher and a 90 vol % distillation temperature of 140° C. or lower, a xylene fraction containing xylene, and a fraction B containing monocyclic aromatic hydrocarbons having a 10 vol % distillation temperature of 145° C. or higher and a 90 vol % distillation temperature of 215° C. or lower; and a xylene conversion step of bringing a mixed fraction obtained by mixing the fractions A and B with each other into contact with a catalyst containing a solid acid to convert the mixed fraction into xylene.

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