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1. 发明申请

US20120253054A1 METHODS FOR PRODUCING OXIDIZED CYCLIC PHENOL SULFIDES 有权
标题翻译：生产氧化环丙醇硫化物的方法
公开(公告)号：US20120253054A1
公开(公告)日：2012-10-04
申请号：US13523420
申请日：2012-06-14
申请人： Masateru Yasumura , Yoshikazu Aoki , Masami Ito , Masafumi Umekawa , Naohiro Tarumoto
发明人： Masateru Yasumura , Yoshikazu Aoki , Masami Ito , Masafumi Umekawa , Naohiro Tarumoto
IPC分类号： C07D341/00
CPC分类号： C07D341/00
摘要： A method for producing an oxidized cyclic phenol sulfide which comprises the step of oxidizing a cyclic phenol sulfide of the following formula (1) as a raw material: wherein R represents a straight or branched alkyl group having 1 to 6 carbon atoms, and m is an integer from 4 to 8, in a solvent(s) other than a halogenated hydrocarbon in an amount of 2 or more and less than 10 parts by weight per 1 part by weight of the cyclic phenol sulfide, with an oxidizing agent(s) to obtain an oxidized cyclic phenol sulfide of the following formula (2): wherein R represents a straight or branched alkyl group having 1 to 6 carbon atoms, m is an integer from 4 to 8, and n is 1 or 2.
摘要翻译：一种氧化环状苯酚硫化物的制造方法，其特征在于，将下述式（1）所示的环状苯酚硫化物氧化为原料，其中，R表示碳原子数1〜6的直链或支链烷基，m表示 4至8的整数，相对于每1重量份环状苯酚硫化物，其量为2重量份以上且小于10重量份的卤代烃类溶剂，以及氧化剂，得到下述式（2）所示的氧化型环状苯酚硫化物：式中，R表示碳原子数1〜6的直链或支链烷基，m为4〜8的整数，n为1或2。

2. 发明申请

US20110028737A1 METHOD FOR CONTINUOUSLY PRODUCING OXIDIZED CYCLIC PHENOL SULFIDES 有权
标题翻译：连续生产氧化环丙醇硫化物的方法
公开(公告)号：US20110028737A1
公开(公告)日：2011-02-03
申请号：US12867207
申请日：2009-02-16
申请人： Masateru Yasumura , Yoshikazu Aoki , Masami Ito
发明人： Masateru Yasumura , Yoshikazu Aoki , Masami Ito
IPC分类号： C07D341/00
CPC分类号： C07D341/00
摘要： The present invention discloses a method for continuously producing an oxidized cyclic phenol sulfide which comprises the continuous steps of reacting a para-alkyl phenol compound as a raw material with 1.7 to 2.5 molar equivalent of sulfur and 0.25 to 0.75 molar equivalent of an alkali metal reagent per 1 mol of the phenol compound (the first step); and oxidizing a cyclic phenol sulfide of the formula (2) produced by the above reaction with an oxidizing agent(s) in the same reactor as that of the first step and without taking the cyclic phenol sulfide out of the reactor; wherein R represents a straight or branched alkyl group having 1 to 6 carbon atoms, and m is an integer from 4 to 8, to obtain an oxidized cyclic phenol sulfide of the formula (3) (the second step): wherein R represents a straight or branched alkyl group having 1 to 6 carbon atoms, m is an integer from 4 to 8, and n is 1 or 2.
摘要翻译：本发明公开了一种连续生产氧化环状苯酚硫化物的方法，该方法包括以对数烷基酚化合物为原料与1.7〜2.5摩尔当量硫和0.25〜0.75摩尔当量碱金属试剂的连续步骤每1mol酚化合物（第一步）; 和在与第一步骤相同的反应器中用氧化剂氧化由上述反应产生的式（2）的环状苯酚硫化物，而不将环状苯酚硫化物从反应器中取出; 其中R表示具有1至6个碳原子的直链或支链烷基，m为4至8的整数，以获得式（3）（第二步）的氧化环状苯酚硫化物：其中R表示直链或碳原子数为1〜6的支链烷基，m为4〜8的整数，n为1或2。

3. 发明授权

US07860436B2 Image forming apparatus with toner supplying roller 有权
标题翻译：具有调色剂供应辊的图像形成装置
公开(公告)号：US07860436B2
公开(公告)日：2010-12-28
申请号：US11808880
申请日：2007-06-13
申请人： Tetsuo Sano , Yohei Nakade , Ichiro Demizu , Yoshikazu Aoki , Yuusuke Okuno , Takuya Okada
发明人： Tetsuo Sano , Yohei Nakade , Ichiro Demizu , Yoshikazu Aoki , Yuusuke Okuno , Takuya Okada
IPC分类号： G03G15/08 , G03G15/09 , G03G13/08 , B05C1/08 , F16C13/00
CPC分类号： G03G15/0808
摘要： A developing device has a developer bearing member, a housing adapted to accommodate a developer, and a supply roller adapted to supply the developer within the housing for the developer bearing member. The supply roller has an outer circumferencial foam layer made of resin or rubber. The foam layer has an air permeability of 150-200 ml/cm2/s, a hardness of 50-200 N, and an average cell density of 20-40 per 25 mm width.
摘要翻译：显影装置具有显影剂承载构件，适于容纳显影剂的壳体和适于将显影剂供应到用于显影剂承载构件的壳体内的供应辊。供料辊具有由树脂或橡胶制成的外周边泡沫层。泡沫层的透气度为150-200ml / cm 2 / s，硬度为50-200N，平均泡孔密度为25-40mm宽。

4. 发明授权

US07820832B2 Oxidized mixed cyclic phenol sulfides, and charge control agents and toners using the same 有权
标题翻译：氧化混合环状苯酚硫化物，以及使用其的电荷控制剂和调色剂
公开(公告)号：US07820832B2
公开(公告)日：2010-10-26
申请号：US12481112
申请日：2009-06-09
申请人： Masateru Yasumura , Masami Ito , Naohiro Tarumoto , Yoshikazu Aoki , Masafumi Umekawa , Masaki Okubo , Hideyuki Otsuka , Jun Watanabe
发明人： Masateru Yasumura , Masami Ito , Naohiro Tarumoto , Yoshikazu Aoki , Masafumi Umekawa , Masaki Okubo , Hideyuki Otsuka , Jun Watanabe
IPC分类号： C07D339/08
CPC分类号： G03G9/09775 , C07D341/00 , G03G9/08748 , G03G9/08771
摘要： The present invention discloses an oxidized mixed cyclic phenol sulfide which is a mixture of the oxidized cyclic phenol sulfide wherein m is 8 and the oxidized cyclic phenol sulfide wherein m is an integer other than 8, the oxidized cyclic phenol sulfide being represented by the following formula (1): wherein R is a straight or branched alkyl group having 1 to 6 carbon atoms, m is an integer from 4 to 9, and n is 1 or 2; or an oxidized cyclic phenol sulfide of formula (1) wherein m is 8. The present invention also discloses a charge control agent which comprises the above sulfide(s) as the active ingredient; and a toner which comprises the charge control agent, a coloring agent and a binder resin. This charge control agent is particularly useful for color toners, and it speeds up charging risetime, and has a high charge amount and charging characteristics excellent in environmental stability. Further, the charge control agent is safe since it does not have any problem with the waste regulations.
摘要翻译：本发明公开了氧化型环状苯酚硫化物，其为m为8的氧化型环状苯酚硫化物和m为8以外的整数的氧化型环状苯酚硫化物的混合物，氧化型环状苯酚硫化物由下式（1）表示：其中R是具有1-6个碳原子的直链或支链烷基，m是4至9的整数，n是1或2; 或式（1）的氧化环状苯酚硫化物，其中m为8.本发明还公开了一种电荷控制剂，其包含上述硫化物作为活性成分; 以及包含电荷控制剂，着色剂和粘合剂树脂的调色剂。该电荷控制剂对于彩色调色剂特别有用，并且其加速时间上升，并且具有高的电荷量和环境稳定性优良的充电特性。此外，充电控制剂是安全的，因为废物规定没有任何问题。

5. 发明授权

US07729383B2 Multiplexer and multiplexing method 失效
标题翻译：多路复用和复用方法
公开(公告)号：US07729383B2
公开(公告)日：2010-06-01
申请号：US11783326
申请日：2007-04-09
申请人： Yoshikazu Aoki
发明人： Yoshikazu Aoki
IPC分类号： H04J3/24
CPC分类号： H04N21/4341 , H04N21/23406 , H04N21/2368 , H04N21/2401 , H04N21/44004
摘要： A multiplexer according to an embodiment of the present invention multiplexes a video ES and an audio ES to generate a transport stream TS, and includes a video buffer, an audio buffer, and a multiplexing unit. A multiplexing unit executes simulation of a buffer occupation necessary for a video ES upon decoding the TS, and controls multiplexing of the video ES not to cause overflow of a buffer based on the simulation result. In the simulation, a predetermined time Δt is divided by N ((main buffer leak rate/system clock frequency)×N (N is an integer)=integer), the remainder R is carried over to the next calculation, and a current main buffer leak data amount is calculated by integer arithmetic based on the integral quotient.
摘要翻译：根据本发明的实施例的多路复用器复用视频ES和音频ES以生成传输流TS，并且包括视频缓冲器，音频缓冲器和复用单元。复用单元在对TS解码时执行视频ES所需的缓冲器占用的模拟，并且基于模拟结果控制视频ES的复用不引起缓冲器的溢出。在模拟中，将预定时间＆Dgr; t除以N（（主缓冲器泄漏率/系统时钟频率）×N（N是整数）=整数），将余数R转移到下一次计算，当前主缓冲区泄漏数据量通过基于积分商的整数运算来计算。

6. 发明申请

US20090088575A1 Process For Producing N,N'-Carbonyldiimidazole 有权
标题翻译：制备N，N'-羰基二咪唑的方法
公开(公告)号：US20090088575A1
公开(公告)日：2009-04-02
申请号：US11547524
申请日：2005-03-29
申请人： Yoshikazu Aoki , Norimasa Yokoyama , Masateru Yasumura
发明人： Yoshikazu Aoki , Norimasa Yokoyama , Masateru Yasumura
IPC分类号： C07D403/06
CPC分类号： C07D233/54 , Y02P20/582
摘要： The present invention provides a process for producing N,N′-carbonyldiimidazole, comprising: reacting phosgene, diphosgene, or triphosgene with imidazole in an inert solvent to produce N,N′-carbonyldiimidazole; to imidazole hydrochloride yielded as a by-product in the above step, adding a gaseous or liquid basic compound represented by the below-shown general formula (1) in an inert solvent to conduct neutralization reaction; and circulating the imidazole thus generated to use it as a starting material for N,N′-carbonyldiimidazole production.In the general formula (1), R1, R2, and R3 each independently represents a hydrogen atom, a methyl group, or an ethyl group. The CDI produced by the production process of the invention is a compound useful in the fields of synthesis of pharmaceutical agents, synthesis of agricultural chemicals, peptide synthesis, and the like, e.g., intermolecular condensation reactions, intramolecular condensation reactions for synthesizing N-carboxylic anhydrides, production of activated esters, and the like. The compound is especially suitable for use in applications where colorlessness is required.
摘要翻译：本发明提供了制备N，N'-羰基二咪唑的方法，其包括：将光气，二光气或三光气与咪唑在惰性溶剂中反应以产生N，N'-羰基二咪唑; 在上述步骤中作为副产物产生的咪唑盐酸盐，在惰性溶剂中加入由下述通式（1）表示的气态或液态碱性化合物进行中和反应; 并使由此产生的咪唑循环使用其作为N，N'-羰基二咪唑生产的起始原料。在通式（1）中，R 1，R 2和R 3各自独立地表示氢原子，甲基或乙基。通过本发明的制造方法制备的CDI是可用于药物合成，农药合成，肽合成等领域的化合物，例如分子间缩合反应，用于合成N-羧酸酐的分子内缩合反应，活性酯的制备等。该化合物特别适用于需要无色性的应用。

7. 发明申请

US20090035678A1 MIXED CYCLIC PHENOL SULFIDES, AND CHARGE CONTROL AGENTS AND TONERS USING THE SAME 有权
标题翻译：混合循环酚醛硫酸盐，以及充电控制剂和使用它的调色剂
公开(公告)号：US20090035678A1
公开(公告)日：2009-02-05
申请号：US12240520
申请日：2008-09-29
申请人： Masateru Yasumura , Masami Ito , Naohiro Tarumoto , Yoshikazu Aoki , Masafumi Umekawa , Masaki Okubo , Hideyuki Otsuka , Jun Watanabe
发明人： Masateru Yasumura , Masami Ito , Naohiro Tarumoto , Yoshikazu Aoki , Masafumi Umekawa , Masaki Okubo , Hideyuki Otsuka , Jun Watanabe
IPC分类号： G03G9/00 , C07D341/00
CPC分类号： G03G9/09733 , C07D341/00 , G03G9/08711 , G03G9/0904 , G03G9/09758 , G03G9/09775
摘要： The present invention discloses a mixed cyclic phenol sulfide which is a mixture of the cyclic phenol sulfide wherein m is 8 and the cyclic phenol sulfide wherein m is an integer other than 8, the cyclic phenol sulfide being represented by the following formula (1): wherein R is a straight or branched alkyl group having 1 to 6 carbon atoms, and m is an integer from 4 to 9; or a cyclic phenol sulfide of formula (1) wherein m is 8. The present invention also discloses a charge control agent which comprises the above sulfide(s) as the active ingredient; and a toner which comprises the charge control agent, a coloring agent and a binder resin. This charge control agent is particularly useful for color toners, and it speeds up charging risetime, and has a high charge amount and charging characteristics excellent in the environmental stability. Further, the charge control agent is safe since it does not have any problem with the waste regulations.
摘要翻译：本发明公开了一种混合环状苯酚硫化物，其中m为8的环状苯酚硫化物和m为8以外的环状苯酚硫化物的混合物，环状苯酚硫化物由下式（1）表示：其中R是具有1至6个碳原子的直链或支链烷基，m是4至9的整数; 或式（1）的环状苯酚硫化物，其中m为8.本发明还公开了一种电荷控制剂，其包含上述硫化物作为活性成分; 以及包含电荷控制剂，着色剂和粘合剂树脂的调色剂。该电荷控制剂对于彩色调色剂特别有用，并且其加速电荷上升时间，并且具有高的电荷量和环境稳定性优良的充电特性。此外，充电控制剂是安全的，因为废物规定没有任何问题。

8. 发明申请

US20130296578A1 SURFACE-MODIFIED SILICA POWDER AND METHOD FOR PRODUCING THE SAME, AS WELL AS TONER COMPOSITION FOR ELECTROPHOTOGRAPHY 有权
标题翻译：表面改性二氧化硅粉末及其制造方法，作为用于电子照相的聚碳酸酯组合物
公开(公告)号：US20130296578A1
公开(公告)日：2013-11-07
申请号：US13980203
申请日：2012-02-03
申请人： Yuki Amano , Naohiro Naito , Hisao Okada , Masaki Okubo , Yoshikazu Aoki , Hideyuki Otsuka
发明人： Yuki Amano , Naohiro Naito , Hisao Okada , Masaki Okubo , Yoshikazu Aoki , Hideyuki Otsuka
IPC分类号： C07F7/02
CPC分类号： C07F7/02 , C01B33/18 , C01P2006/40 , C09C1/3063 , C09C1/3081 , C09C1/309 , G03G9/09716 , G03G9/09725
摘要： Provided by the present invention is a surface-modified silica powder, characterized in that the said powder is obtained by surface treatment of a silica powder with one or two or more of a compound (A) and with an aminosilane (B), wherein the fixing rate of the compound (A) and the aminosilane (B) is a total of 50% or more, the hydrophobic rate is 80% or more, and the triboelectrostatic charge amount is 200 μC/g or less in its absolute value. The surface-modified silica powder of the present invention can stabilize many properties including fluidity and electrostatic properties while can significantly reduce problems such as fogging and decrease in image quality without significantly deteriorating characteristics of a developing agent and so forth when this is used as an external additive.
摘要翻译：本发明提供一种表面改性二氧化硅粉末，其特征在于，所述粉末是通过用一种或两种以上的化合物（A）和氨基硅烷（B）进行二氧化硅粉末的表面处理得到的，其中，化合物（A）和氨基硅烷（B）的定影率总共为50％以上，疏水率为80％以上，摩擦电位静电电荷的绝对值为200μC/ g以下。本发明的表面改性二氧化硅粉末可以稳定包括流动性和静电特性的许多性能，同时可以显着降低诸如起雾和降低图像质量的问题，而不会显着降低显影剂等的特性，当将其用作外部添加剂。

9. 发明授权

US08263786B2 Methods for producing cyclic phenol sulfides 有权
标题翻译：环状苯酚硫化物的制备方法
公开(公告)号：US08263786B2
公开(公告)日：2012-09-11
申请号：US12439121
申请日：2007-08-29
申请人： Masateru Yasumura , Yoshikazu Aoki , Masami Ito , Masafumi Umekawa , Naohiro Tarumoto
发明人： Masateru Yasumura , Yoshikazu Aoki , Masami Ito , Masafumi Umekawa , Naohiro Tarumoto
IPC分类号： C07D341/00
CPC分类号： C07D341/00
摘要： The object of the present invention is, in methods for producing cyclic phenol sulfides, to provide methods for producing a number of more macrocyclic products, which comprise the steps of producing a mixture of cyclic phenol sulfides from an inexpensive raw material in one step without inducing the reduction in yield of a cyclic quatromer; and easily separating and purifying a single component from the mixture of cyclic phenol sulfides.The present invention discloses methods for producing a cyclic phenol sulfide which comprises the step of reacting a phenol compound as a raw material, in a one-step reaction, with 1.7 to 2.5 molar equivalent of sulfur and 0.25 to 0.75 molar equivalent of an alkali metal reagent per 1 mol of the phenol compound to obtain a mixture of cyclic phenol sulfide wherein m=4 and at least one kind(s) of cyclic phenol sulfide wherein m=5 to 9, or each separate cyclic phenol sulfide comprised in the mixture.
摘要翻译：本发明的目的在于提供环状苯酚硫化物的制造方法，提供多种大环化合物的制造方法，其特征在于，在一个步骤中，从一价廉的原料制造环状苯酚硫化物的混合物，循环四聚体的产率降低; 并且容易地从环状苯酚硫化物的混合物中分离和纯化单一组分。本发明公开了一种环状苯酚硫化物的制造方法，其特征在于，在一步反应中，使作为原料的酚化合物与1.7〜2.5摩尔当量的硫和0.25〜0.75摩尔当量的碱金属试剂，每1mol酚化合物，得到m = 4的环状苯酚硫化物和m = 5〜9的至少一种环状苯酚硫化物或混合物中所含的各自分离的环状苯酚硫化物的混合物。

10. 发明授权

US08222428B2 Method for continuously producing oxidized cyclic phenol sulfides 有权
标题翻译：连续生产氧化型环状苯酚硫化物的方法
公开(公告)号：US08222428B2
公开(公告)日：2012-07-17
申请号：US12867207
申请日：2009-02-16
申请人： Masateru Yasumura , Yoshikazu Aoki , Masami Ito
发明人： Masateru Yasumura , Yoshikazu Aoki , Masami Ito
IPC分类号： C07D341/00
CPC分类号： C07D341/00
摘要： The present invention discloses a method for continuously producing an oxidized cyclic phenol sulfide which comprises the continuous steps of reacting a para-alkyl phenol compound as a raw material with 1.7 to 2.5 molar equivalent of sulfur and 0.25 to 0.75 molar equivalent of an alkali metal reagent per 1 mol of the phenol compound (the first step); and oxidizing a cyclic phenol sulfide of the formula (2) produced by the above reaction with an oxidizing agent(s) in the same reactor as that of the first step and without taking the cyclic phenol sulfide out of the reactor: wherein R represents a straight or branched alkyl group having 1 to 6 carbon atoms, and m is an integer from 4 to 8, to obtain an oxidized cyclic phenol sulfide of the formula (3) (the second step): wherein R represents a straight or branched alkyl group having 1 to 6 carbon atoms, m is an integer from 4 to 8, and n is 1 or 2.
摘要翻译：本发明公开了一种连续生产氧化环状苯酚硫化物的方法，该方法包括以对数烷基酚化合物为原料与1.7〜2.5摩尔当量硫和0.25〜0.75摩尔当量碱金属试剂的连续步骤每1mol酚化合物（第一步）; 和在与第一步骤相同的反应器中用氧化剂氧化由上述反应生成的式（2）的环状苯酚硫化物，而不将环状苯酚硫化物从反应器中取出：其中R表示具有1至6个碳原子的直链或支链烷基，m为4至8的整数，得到式（3）（第二步）的氧化环状苯酚硫化物：其中R表示直链或支链烷基具有1至6个碳原子，m为4至8的整数，n为1或2。

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