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1. 发明授权

US5691415A Reinforced elastic body and production process thereof 失效
标题翻译：增强弹性体及其制造方法
公开(公告)号：US5691415A
公开(公告)日：1997-11-25
申请号：US457301
申请日：1995-06-01
申请人： Yasumichi Miyagawa , Kenji Kuwata
发明人： Yasumichi Miyagawa , Kenji Kuwata
IPC分类号： C08F8/38
CPC分类号： C08F8/38
摘要： A reinforced elastic body is disclosed, which comprises a chlorosulfonated polyolefin reinforced with polyester fibers having an adhesive containing an isocyanate compound and/or an epoxy compound and an adhesive composed of a mixture of a resorcin-formaldehyde resin and a 2,3-dichlorobutadiene-containing polymer. Also, a production process of the reinforced elastic body is disclosed, which comprises vulcanizing-adhering polyester fibers treated with an adhesive containing an isocyanate compound and/or an epoxy compound and then treated with an adhesive composed of a mixture of a resorcin-formaldehyde resin and a 2,3-dichlorobutadiene-containing polymer to a chlorosulfonated olefin compounded material.
摘要翻译：公开了一种增强弹性体，其包括用具有含异氰酸酯化合物和/或环氧化合物的粘合剂的聚酯纤维增强的氯磺化聚烯烃和由间苯二酚 - 甲醛树脂和2,3-二氯丁二烯 - 含聚合物。另外，公开了一种增强弹性体的制造方法，其包括用含有异氰酸酯化合物和/或环氧化合物的粘合剂处理的硫化粘合聚酯纤维，然后用由间苯二酚 - 甲醛树脂和含有2,3-二氯丁二烯的聚合物与氯磺化烯烃复合材料。

2. 发明授权

US5449833A Process for the preparation of chlorinated polyolefin and chlorosulfonated polyolefin 失效
标题翻译：制备氯化聚烯烃和氯磺化聚烯烃的方法
公开(公告)号：US5449833A
公开(公告)日：1995-09-12
申请号：US311029
申请日：1994-09-26
申请人： Nobuyuki Ito , Katsushige Okayama , Yoshinori Karasuda , Yasumichi Miyagawa
发明人： Nobuyuki Ito , Katsushige Okayama , Yoshinori Karasuda , Yasumichi Miyagawa
IPC分类号： C08F8/20 , C08F8/38 , C07C17/02 , C07C21/00
CPC分类号： C08F8/20 , C08F8/38
摘要： A novel process for the preparation of a chlorinated polyolefin having excellent low temperature characteristics and brightness is provided which comprises allowing a polyolefin dissolved or suspended in a solvent to undergo chlorination reaction with chlorine gas or chlorinated sulfuryl in the presence of a radical initiator as a catalyst, characterized in that as said solvent there is used 1,1,2-trichloroethane and the temperature is controlled to 90.degree. C. or lower at the process for removing hydrogen chloride and/or sulfur dioxide by-produced during the reaction from the reaction system. A further process for the preparation of a chlorosulfonated polyolefin having excellent low temperature characteristics and brightness is provided which comprises allowing a polyolefin dissolved or suspended in a solvent to undergo chlorosulfonation reaction with chlorine and sulfur dioxide, chlorine and sulfuryl chloride, sulfuryl chloride alone, chlorine, sulfur dioxide and sulfuryl chloride or sulfuryl chloride and sulfur dioxide in the presence of a radical initiator as a catalyst, characterized in that as said solvent there is used 1,1,2-trichloroethane and the temperature is controlled to 90.degree. C. or lower at the process for removing hydrogen chloride and/or sulfur dioxide by-produced during the reaction from the reaction system.
摘要翻译：提供一种制备具有优异的低温特性和亮度的氯化聚烯烃的新方法，其包括使溶解或悬浮在溶剂中的聚烯烃在作为催化剂的自由基引发剂存在下与氯气或氯化硫酰氯进行氯化反应其特征在于，作为所述溶剂使用1,1,2-三氯乙烷，在从反应反应中除去副产的氯化氢和/或二氧化硫的过程中将温度控制在90℃以下。系统。提供了制备具有优异的低温特性和亮度的氯磺化聚烯烃的另一种方法，其包括使溶解或悬浮在溶剂中的聚烯烃与氯和二氧化硫，氯和磺酰氯，仅磺酰氯，氯气进行氯磺化反应，二氧化硫和磺酰氯或磺酰氯和二氧化硫，在自由基引发剂作为催化剂存在下，其特征在于作为所述溶剂使用1,1,2-三氯乙烷，温度控制在90℃或在反应过程中从反应体系中除去副产的氯化氢和/或二氧化硫的过程较低。

3. 发明授权

US5912079A Treating agent for bonding, treated polyester fiber, elastic body and processes for their production 失效
标题翻译：用于粘合，处理的聚酯纤维，弹性体及其生产方法的处理剂
公开(公告)号：US5912079A
公开(公告)日：1999-06-15
申请号：US992458
申请日：1997-12-17
申请人： Yasumichi Miyagawa , Kenji Kuwata
发明人： Yasumichi Miyagawa , Kenji Kuwata
IPC分类号： C08J5/06 , D06M15/227 , D06M15/41 , D06M15/693 , D06N3/00 , D06N3/04 , D06N3/12 , D02G3/00 , B05D1/36 , C08K3/20
CPC分类号： C08J5/06 , D06M15/227 , D06M15/41 , D06M15/693 , D06N3/0002 , D06N3/045 , D06N3/12 , C08J2323/34 , D06M2200/50 , Y10T428/2933 , Y10T428/2969
摘要： A treating agent for bonding a polyester fiber and a chlorosulfonated polyolefin compound, which consists of a resorcinol/formaldehyde/latex mixture, wherein:1) the molar ratio of the resorcinol to the formaldehyde is from 1/0.1 to 1/5,2) the polymer component of the latex is a 2,3-dichlorobutadiene-containing polymer,3) the weight ratio of the solid content of the latex to the sum of the resorcinol and the formaldehyde is from 1/100 to 1/1,4) the amount of the 2,3-dichlorobutadiene-containing polymer solid content of the latex in the resorcinol/formaldehyde/latex mixture is from 5 to 50 wt %, and5) the amount of a surfactant in the resorcinol/formaldehyde/latex mixture is from 0.5 to 2.5 wt %.
摘要翻译：一种用于粘合聚酯纤维和氯磺化聚烯烃化合物的处理剂，其由间苯二酚/甲醛/胶乳混合物组成，其中：1）间苯二酚与甲醛的摩尔比为1 / 0.1至1/5,2）胶乳的聚合物组分是含2,3-二氯丁二烯的聚合物，3）胶乳的固体含量与间苯二酚和甲醛的总和的重量比为1/100至1/1,4）间苯二酚/甲醛/胶乳混合物中胶乳的含2,3-二氯丁二烯的聚合物固体含量的量为5-50wt％，和5）间苯二酚/甲醛/胶乳混合物中的表面活性剂的量为为0.5〜2.5重量％。

4. 发明授权

US6025043A Joint boot obtained from chlorosulfonated ethylene-alpha-olefin copolymer composition 有权
标题翻译：由氯磺化乙烯-α-烯烃共聚物组合物得到的接头靴
公开(公告)号：US6025043A
公开(公告)日：2000-02-15
申请号：US267358
申请日：1999-03-15
申请人： Yasumichi Miyagawa , Mitsuhiro Kamezawa , Hideyoshi Nakamura , Masahiro Watanuki
发明人： Yasumichi Miyagawa , Mitsuhiro Kamezawa , Hideyoshi Nakamura , Masahiro Watanuki
IPC分类号： C08K5/17 , C08K5/00 , C08K5/34 , C08K5/3415 , C08K5/38 , C08K5/40 , C08L23/34 , F16D3/84
CPC分类号： C08K5/0025 , Y10T428/1352 , Y10T428/1386 , Y10T428/139
摘要： A chlorosulfonated ethylene-.alpha.-olefin copolymer composition comprising a chlorosulfonated ethylene-.alpha.-olefin copolymer, a thiuram compound, a bismaleimide compound, a nickel dialkyldithiocarbamate, and a diarylmonoamine compound, and a motorcar joint boot obtained by molding and vulcanizing the chlorosulfonated ethylene-.alpha.-olefin copolymer composition. The copolymer composition is excellent in the tensile characteristics at room temperature and low temperature, in the compression set under a low-temperature atmosphere, and in the fatigue resistance.
摘要翻译：包含氯磺化乙烯-α-烯烃共聚物，秋兰姆化合物，双马来酰亚胺化合物，二烷基二硫代氨基甲酸镍和二芳基一胺化合物的氯磺化乙烯-α-烯烃共聚物组合物和通过将氯磺化乙烯-α-烯烃共聚物 α-烯烃共聚物组合物。共聚物组成在室温低温下的拉伸特性，低温环境下的压缩永久变形和耐疲劳性优异。

5. 发明授权

US5219967A Acrylic copolymer rubber 失效
标题翻译：丙烯酸共聚物橡胶
公开(公告)号：US5219967A
公开(公告)日：1993-06-15
申请号：US730748
申请日：1991-07-16
申请人： Yasumichi Miyagawa , Mitsuhiro Kamezawa , Toshiya Higashino , Takashi Yamamoto , Shinji Ozoe
发明人： Yasumichi Miyagawa , Mitsuhiro Kamezawa , Toshiya Higashino , Takashi Yamamoto , Shinji Ozoe
IPC分类号： C08F16/14 , C08F18/02 , C08F20/32 , C08F20/34 , C08F216/14 , C08F218/08 , C08F220/10 , C08F220/18 , C08F220/32 , C08F220/34 , C08F220/36
CPC分类号： C08F220/34 , C08F220/18 , C08F220/36
摘要： An acrylic copolymer rubber which is a random copolymer of(A) a cyano group-containing acrylate or methacrylate of the following formula (I): ##STR1## wherein R.sup.1 is hydrogen or methyl, and R.sup.2 is --C.sub.n H.sub.2n -- or --CH.sub.2 CH.sub.2 --0--CH.sub.2 CH.sub.2 --, wherein n is an integer of from 2 to 4,(B) at least one of ethyl acrylate and n-butyl acrylate, and(C) at least one of glycidyl methacrylate and allyl glycidyl ether, or vinyl chloroacetate,wherein the amounts of units derived from the above (A), (B) and (C) in said copolymer are from 5 to 70% by weight, from 20 to 94.5% by weight and from 0.5 to 10% by weight, respectively, and which has a Mooney viscosity ML.sub.1+4 (100.degree. C.) of at least 5.

6. 发明授权

US5916977A Chlorosulfonated ethylene-.alpha.-olefin copolymer composition 失效
标题翻译：氯磺化乙烯-α-烯烃共聚物组合物
公开(公告)号：US5916977A
公开(公告)日：1999-06-29
申请号：US722560
申请日：1996-09-27
申请人： Yasumichi Miyagawa , Mitsuhiro Kamezawa , Hideyoshi Nakamura , Masahiro Watanuki
发明人： Yasumichi Miyagawa , Mitsuhiro Kamezawa , Hideyoshi Nakamura , Masahiro Watanuki
IPC分类号： C08K5/17 , C08K5/00 , C08K5/34 , C08K5/3415 , C08K5/38 , C08K5/40 , C08L23/34 , C08F8/36 , C08F8/38
CPC分类号： C08K5/0025 , Y10T428/1352 , Y10T428/1386 , Y10T428/139
摘要： A chlorosulfonated ethylene-.alpha.-olefin copolymer composition comprising a chlorosulfonated ethylene-.alpha.-olefin copolymer, a thiuram compound, a bismaleimide compound, a nickel dialkyldithiocarbamate, and a diarylmonoamine compound, and a motorcar joint boot obtained by molding and vulcanizing the chlorosulfonated ethylene-.alpha.-olefin copolymer composition. The copolymer composition is excellent in the tensile characteristics at room temperature and low temperature, in the compression set under a low-temperature atmosphere, and in the fatigue resistance.
摘要翻译：包含氯磺化乙烯-α-烯烃共聚物，秋兰姆化合物，双马来酰亚胺化合物，二烷基二硫代氨基甲酸镍和二芳基一胺化合物的氯磺化乙烯-α-烯烃共聚物组合物和通过将氯磺化乙烯-α-烯烃共聚物 α-烯烃共聚物组合物。共聚物组成在室温低温下的拉伸特性，低温环境下的压缩永久变形和耐疲劳性优异。

7. 发明授权

US5766762A Treating agent for bonding, treated polyester fiber, elastic body and processes for their production 失效
公开(公告)号：US5766762A
公开(公告)日：1998-06-16
申请号：US815578
申请日：1997-03-12
申请人： Yasumichi Miyagawa , Kenji Kuwata
发明人： Yasumichi Miyagawa , Kenji Kuwata
IPC分类号： C08J5/06 , D06M15/227 , D06M15/41 , D06M15/693 , D06N3/00 , D06N3/04 , D06N3/12 , B32B27/34 , C08K3/20
CPC分类号： C08J5/06 , D06M15/227 , D06M15/41 , D06M15/693 , D06N3/0002 , D06N3/045 , D06N3/12 , C08J2323/34 , D06M2200/50 , Y10T428/2933 , Y10T428/2969
摘要： A treating agent for bonding a polyester fiber and a chlorosulfonated polyolefin compound, which consists of a resorcinol/formaldehyde/latex mixture, wherein: 1) the molar ratio of the resorcinol to the formaldehyde is from 1/0.1 to 1/5, 2) the polymer component of the latex is a 2,3-dichlorobutadiene-containing polymer, 3) the weight ratio of the solid content of the latex to the sum of the resorcinol and the formaldehyde is from 1/100 to 1/1, 4) the amount of the 2,3-dichlorobutadiene-containing polymer solid content of the latex in the resorcinol/formaldehyde/latex mixture is from 5 to 50 wt %, and 5) the amount of a surfactant in the resorcinol/formaldehyde/latex mixture is from 0.5 to 2.5 wt %.

8. 发明授权

US5378766A Process for the preparation of chlorinated polyolefin and chlorosulfonated polyolefin 失效
公开(公告)号：US5378766A
公开(公告)日：1995-01-03
申请号：US156904
申请日：1993-11-24
申请人： Nobuyuki Ito , Katsushige Okayama , Toshinori Karasuda , Yasumichi Miyagawa
发明人： Nobuyuki Ito , Katsushige Okayama , Toshinori Karasuda , Yasumichi Miyagawa
IPC分类号： C08F8/20 , C08F8/38 , C08F8/00
CPC分类号： C08F8/20 , C08F8/38
摘要： A novel process for the preparation of a chlorinated polyolefin having excellent low temperature characteristics and brightness is provided which comprises allowing a polyolefin dissolved or suspended in a solvent to undergo chlorination reaction with chlorine gas or chlorinated sulfuryl in the presence of a radical initiator as a catalyst, characterized in that as said solvent there is used 1,1,2-trichloroethane and the temperature is controlled to 90.degree. C. or lower at the process for removing hydrogen chloride and/or sulfur dioxide by-produced during the reaction from the reaction system. A further process for the preparation of a chlorosulfonated polyolefin having excellent low temperature characteristics and brightness is provided which comprises allowing a polyolefin dissolved or suspended in a solvent to undergo chlorosulfonation reaction with chlorine and sulfur dioxide, chlorine and sulfuryl chloride, sulfuryl chloride alone, chlorine, sulfur dioxide and sulfuryl chloride or sulfuryl chloride and sulfur dioxide in the presence of a radical initiator as a catalyst, characterized in that as said solvent there is used 1,1,2-trichloroethane and the temperature is controlled to 90.degree. C. or lower at the process for removing hydrogen chloride and/or sulfur dioxide by-produced during the reaction from the reaction system.

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