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1. 发明申请

US20120296114A1 PREPARATION METHOD OF 4-AMINOMETHYLBENZOIC ACID 有权
标题翻译： 4-氨基乙酰苯甲酸的制备方法
公开(公告)号：US20120296114A1
公开(公告)日：2012-11-22
申请号：US13522465
申请日：2010-12-09
申请人： Woo Sun Kim
发明人： Woo Sun Kim
IPC分类号： C07C227/26
CPC分类号： C07C227/04 , B01J21/18 , B01J23/40 , B01J23/44 , B01J23/75 , C07C249/08 , C07C229/38 , C07C251/48
摘要： The present invention relates to a preparation method of 4-aminomethylbenzoic acid comprising the following steps: preparing 4-carboxylbenzaldehyde or an alkyl ester thereof (methyl 4-formyl benzoate); reacting the 4-carboxylbenzaldehyde or an alkyl ester thereof (methyl 4-formyl benzoate) with hydroxyamine to oximate the same; and contact reducing 4-carboxylbenzaldehyde oxime or an alkyl ester oxime thereof obtained by the oximation, through hydrogen in a sodium hydroxide aqueous solution. Since methyl 4-hydroxyiminomethylbenzoate is reacted as a raw material in the presence of an alkali, hydrogen of a relatively low pressure can be used and a purification process is also simple, thereby enabling preparation of 4-aminomethylbenzoic acid with a low cost and high yield.
摘要翻译：本发明涉及4-氨基甲基苯甲酸的制备方法，包括以下步骤：制备4-羧基苯甲醛或其烷基酯（4-甲酰基苯甲酸甲酯）; 使4-羧基苯甲醛或其烷基酯（4-甲酰基苯甲酸酯）与羟胺反应，使其氧化; 并通过氢氧化钠水溶液中的氢气将通过肟化得到的4-羧基苯甲醛肟或其烷基酯肟接触。由于在碱存在下使4-羟基亚氨基甲基苯甲酸甲酯作为原料反应，所以可以使用相对低压的氢，并且纯化方法也很简单，从而能够以低成本和高产率制备4-氨基甲基苯甲酸。

2. 发明授权

US6053955A Polyether amino acid ester compounds, preparation method and use thereof 失效
标题翻译：聚醚氨基酸酯化合物，其制备方法和用途
公开(公告)号：US6053955A
公开(公告)日：2000-04-25
申请号：US155415
申请日：1998-09-25
申请人： Byung Hyung Lee , Woo Sun Kim , Sang Chul Lim , Ho Young Kwon , Dae Joon Yang
发明人： Byung Hyung Lee , Woo Sun Kim , Sang Chul Lim , Ho Young Kwon , Dae Joon Yang
IPC分类号： C07C227/08 , C07C43/03 , C07C229/24 , C08G65/329 , C08G65/332 , C08G65/333 , C10L1/22 , C10L1/238 , C10L10/00 , C10L10/04 , C10L10/18 , C10L1/18
CPC分类号： C10L1/238 , C07C229/24 , C08G65/329 , C08G65/332 , C08G65/33306 , C10L10/04 , C10L10/06 , F02B2275/18
摘要： The present invention relates to polyether amino acid ester compounds, preparation method and their use as hydrocarbon fuel additives.
摘要翻译： PCT No.PCT / KR97 / 00056 Sec。 371日期：1998年9月25日 102（e）日期1998年9月25日PCT 1997年4月1日PCT公布。公开号WO97 / 36854 日期：1997年10月9日本发明涉及聚醚氨基酸酯化合物，其制备方法及其作为烃类燃料添加剂的用途。

3. 发明授权

US08907127B2 Preparation method of 4-aminomethylbenzoic acid 有权
标题翻译： 4-氨基甲基苯甲酸的制备方法
公开(公告)号：US08907127B2
公开(公告)日：2014-12-09
申请号：US13522465
申请日：2010-12-09
申请人： Woo Sun Kim
发明人： Woo Sun Kim
IPC分类号： C07C227/04 , C07C249/08 , B01J21/18 , B01J23/40 , B01J23/44 , B01J23/75
CPC分类号： C07C227/04 , B01J21/18 , B01J23/40 , B01J23/44 , B01J23/75 , C07C249/08 , C07C229/38 , C07C251/48
摘要： The present invention relates to a preparation method of 4-aminomethylbenzoic acid comprising the following steps: preparing 4-carboxylbenzaldehyde or an alkyl ester thereof (methyl 4-formyl benzoate); reacting the 4-carboxylbenzaldehyde or an alkyl ester thereof (methyl 4-formyl benzoate) with hydroxyamine to oximate the same; and contact reducing 4-carboxylbenzaldehyde oxime or an alkyl ester oxime thereof obtained by the oximation, through hydrogen in a sodium hydroxide aqueous solution. Since methyl 4-hydroxyiminomethylbenzoate is reacted as a raw material in the presence of an alkali, hydrogen of a relatively low pressure can be used and a purification process is also simple, thereby enabling preparation of 4-aminomethylbenzoic acid with a low cost and high yield.
摘要翻译：本发明涉及4-氨基甲基苯甲酸的制备方法，包括以下步骤：制备4-羧基苯甲醛或其烷基酯（4-甲酰基苯甲酸甲酯）; 使4-羧基苯甲醛或其烷基酯（4-甲酰基苯甲酸酯）与羟胺反应，使其氧化; 并通过氢氧化钠水溶液中的氢气将通过肟化得到的4-羧基苯甲醛肟或其烷基酯肟接触。由于在碱存在下使4-羟基亚氨基甲基苯甲酸甲酯作为原料反应，所以可以使用相对低压的氢，并且纯化方法也很简单，从而能够以低成本和高产率制备4-氨基甲基苯甲酸。

4. 发明授权

US6031119A Polyalkylene guanidine salts or polyalkylene biguanidine salts having a branched silane compound, method for preparing same and uses thereof 失效
标题翻译：具有支链硅烷化合物的聚亚烷基胍盐或聚亚烷基双胍盐，其制备方法和用途
公开(公告)号：US6031119A
公开(公告)日：2000-02-29
申请号：US889514
申请日：1997-07-08
申请人： Byung-Hyoung Lee , Woo-Sun Kim , Young-Jun Kim , Sang-Gu Bang , Kwang-Min Lim , Sang-Rak Choi , Keum-Chan Joo
发明人： Byung-Hyoung Lee , Woo-Sun Kim , Young-Jun Kim , Sang-Gu Bang , Kwang-Min Lim , Sang-Rak Choi , Keum-Chan Joo
IPC分类号： A01N55/00 , A01N55/10 , C08G73/00 , C08G73/02 , C08L79/00 , A61K31/155
CPC分类号： C08G73/024 , A01N55/00 , C08G73/00 , C08G73/0253 , C08G73/0293
摘要： Polyalkylene guanidine salts or polyalkylene biguanidine salts having a branched silane compound of formula I show excellent antimicrobial activity and can be applied to various materials including fibers, wood, paper, glass, resins and metals: ##STR1## wherein A is oxyethylene, oxypropylene, oxybutylene, oxystyrene, diphenylsulfone, diphenyl sulfide or alkylamide, which repeating number is 1 to 100,000, or straight or branched alkyl chain containing 1 to 20 carbon atoms;Y represents a blank, HCl, HBr, HI, HNO.sub.3, acetic acid, benzoic acid, dehydroacetic acid, propionic acid, gluconic acid, sorbic acid, phosphoric acid, fumaric acid, maleic acid, carbonic acid, sulfuric acid or para-toluene sulfonic acid;B is a straight or branched alkyl chain containing 0 to 20 carbon atoms;Z is an alkoxy group such as methoxy, ethoxy, propoxy, isopropoxy, butoxy, pentoxy, hexoxy, octoxy or decoxy, chloride, bromide, iodide, acetate, sulfate, or paratoluenesulfonate;X is chloride, bromide, iodide, acetate, sulfate, paratoluenesulfonate, methoxy, ethoxy, propoxy, isopropoxy, butoxy, pentoxy, hexoxy, octoxy, or decoxy;x is 1 or 2;m is an integer of 0 or more; andn is an integer of 1 or more with a proviso that the ratio of m to n ranges from 0.01 to 100 in case of m+n=4 and when m is 0, n is an integer of 4 or more.
摘要翻译：具有式I的支化硅烷化合物的聚亚烷基胍盐或聚亚烷基双胍盐显示出优异的抗微生物活性，并且可以应用于包括纤维，木材，纸，玻璃，树脂和金属在内的各种材料：其中A是氧乙烯，氧丙烯，氧丁烯，氧苯乙烯，重复数为1〜100,000的二苯砜，二苯硫醚或烷基酰胺，或含有1〜20个碳原子的直链或支链烷基链; Y代表空白，HCl，HBr，HI，HNO3，乙酸，苯甲酸，脱氢乙酸，丙酸，葡萄糖酸，山梨酸，磷酸，富马酸，马来酸，碳酸，硫酸或对甲苯磺酸酸; B是含0至20个碳原子的直链或支链烷基链; Z是烷氧基如甲氧基，乙氧基，丙氧基，异丙氧基，丁氧基，戊氧基，己氧基，辛氧基或脱氧，氯化物，溴化物，碘化物，乙酸盐，硫酸盐或对甲苯磺酸盐; X是氯化物，溴化物，碘化物，乙酸盐，硫酸盐，对甲苯磺酸盐，甲氧基，乙氧基，丙氧基，异丙氧基，丁氧基，戊氧基，己氧基，辛氧基或脱氧; x为1或2; m为0以上的整数， n为1以上的整数，条件是在m + n = 4的情况下，m与n的比率为0.01〜100，当m为0时，n为4以上的整数。

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