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1. 发明申请

US20130144026A1 Method for Making a Thermo-Stable and Transparent Resin 审中-公开
标题翻译：制造热稳定透明树脂的方法
公开(公告)号：US20130144026A1
公开(公告)日：2013-06-06
申请号：US13415983
申请日：2012-03-09
申请人： Wen-Chiung Su , Chi-Fa Hsieh , Yeng-Fong Shih
发明人： Wen-Chiung Su , Chi-Fa Hsieh , Yeng-Fong Shih
IPC分类号： C08G79/08
CPC分类号： C09J183/14 , C08G77/56 , C08G77/80 , C08L63/00
摘要： Disclosed is a method form making a thermo-stable and transparent resin. In the method, at first, polyborosiloxane is syhthesized by hydrolyzing and condensing a boron-containing compound, used as a precursor, and a silane compound. Then, epoxy group-containing polyborosiloxane is synthesized by grafting an epoxy group to the polyborosiloxane. Finally, an epoxy/PGB composite is synthesized by reacting the epoxy group-containing polyborosiloxane with epoxy for consolidation, thus providing a homogenous, stable, net-shaped composite.
摘要翻译：公开了制备热稳定和透明树脂的方法形式。在该方法中，首先通过水解和缩合用作前体的含硼化合物和硅烷化合物来研究聚硼硅氧烷。然后，通过将环氧基接枝到聚硼硅氧烷上来合成含环氧基的聚硼硅氧烷。最后，通过使含环氧基的聚硼硅氧烷与环氧树脂反应来合成环氧/ PGB复合材料，用于固化，从而提供均匀，稳定的网状复合材料。

2. 发明授权

US08173760B2 Dendron, polyurethane with side-chain regular dendron, and producing methods thereof 有权
标题翻译：树枝状树脂，侧链常规树枝状聚氨酯及其制造方法
公开(公告)号：US08173760B2
公开(公告)日：2012-05-08
申请号：US12714515
申请日：2010-02-28
申请人： Wen-Chiung Su , Wei-Ho Ting , Chun-Ming Yeh , Chia-Cheng Chang , Sheng-Hong Dai , Ru-Jong Jeng
发明人： Wen-Chiung Su , Wei-Ho Ting , Chun-Ming Yeh , Chia-Cheng Chang , Sheng-Hong Dai , Ru-Jong Jeng
IPC分类号： C08G18/00
CPC分类号： C07C275/40 , C08G18/10 , C08G18/2825 , C08G18/2895 , C08G18/3228 , C08G18/3275 , C08G18/4825 , C08G18/4854 , C08G18/3831
摘要： Methods for producing dendrons of different generations with hydrophobic functional end-groups, and for producing polyurethanes with the side-chain dendrons are disclosed step-by-step. The dendron with hydrophobic functional end-groups in the polyurethane systems, and the honeycomb-like structure thin films are obtained by a breath-figure process. The structures of dendrons and dendritic side-chain polyurethanes are respectively expressed in the following and the end-groups (R) of the dendron are long alkyl chains or perfluoroalkyl derivatives.
摘要翻译：以疏水性功能性端基生产不同代的树突的方法和用于制备具有侧链枝状突起的聚氨酯的方法逐步公开。在聚氨酯体系中具有疏水性功能性端基的树枝状体和蜂窝状结构薄膜通过呼吸图法获得。树枝状突起和树枝状侧链聚氨酯的结构分别表示如下，树枝状结构基团（R）为长烷基链或全氟烷基衍生物。

3. 发明授权

US08114988B2 Phosphorus-containing benzoxazine resin with various substituents and method for preparing the same 有权
标题翻译：含各种取代基的含磷苯并恶嗪树脂及其制备方法
公开(公告)号：US08114988B2
公开(公告)日：2012-02-14
申请号：US12710623
申请日：2010-02-23
申请人： Wen-Chiung Su , Ching-Hsuan Lin , Po-Wen Cheng
发明人： Wen-Chiung Su , Ching-Hsuan Lin , Po-Wen Cheng
IPC分类号： C08G79/04
CPC分类号： C07F9/657172 , C08G73/22
摘要： The present invention provides a method for preparing a phosphorus-containing bexzoxazine resin having the following structure shown as the formula (I) or (V): wherein, R1˜R4 respectively comprise one selected from the group consisting of hydrogen, C1˜C6 alkyl, C3˜C6 cyclic alkyl, and phenyl.
摘要翻译：本发明提供了制备具有如式（I）或（V）所示结构的含磷苯唑氧氮树脂的方法：其中，R1〜R4分别包括选自氢，C1〜C6烷基，C 3-6环烷基和苯基。

4. 发明申请

US20110118423A1 DEVELOPMENT OF A CROSS-LINKED EPOXY RESIN WITH FLAME-RETARDANT PROPERTIES 有权
标题翻译：开发具有阻燃性能的交联环氧树脂
公开(公告)号：US20110118423A1
公开(公告)日：2011-05-19
申请号：US13011911
申请日：2011-01-23
申请人： WEN-CHIUNG SU , Chun-Ku Liu , Ru-Jong Jeng , Shenghong A. Dai , Ching-Hsuan Lin
发明人： WEN-CHIUNG SU , Chun-Ku Liu , Ru-Jong Jeng , Shenghong A. Dai , Ching-Hsuan Lin
IPC分类号： C08G59/14
CPC分类号： C08G59/1477 , C08G59/184 , C08G59/5033 , C08L63/00
摘要： The invention discloses a cross-linked epoxy resin with flame-retardant properties and method for producing the same. The polymeric material of the invention includes an epoxy resin, a curing agent and a modification agent. Particularly, the modification agent is a derivative of 9,10-Dihydro-9-oxa-10-phosphaphenanthrene 10-oxide (DOPO). Moreover, the curing agent is 4,4′-diaminodiphenyl methane (DDM), or tris(4-aminophenyl)amine (NNH).
摘要翻译：本发明公开了具有阻燃性的交联型环氧树脂及其制造方法。本发明的聚合物材料包括环氧树脂，固化剂和改性剂。特别地，改性剂是9,10-二氢-9-氧杂-10-磷杂菲10氧化物（DOPO）的衍生物。此外，固化剂是4,4'-二氨基二苯基甲烷（DDM）或三（4-氨基苯基）胺（NNH）。

5. 发明授权

US07825274B2 Bisbiphenylacylphosphine oxide and preparation method therefore 有权
公开(公告)号：US07825274B2
公开(公告)日：2010-11-02
申请号：US12141380
申请日：2008-06-18
申请人： Wen-Chiung Su , Chang-Chih Lin , Ching-Shang Sheng
发明人： Wen-Chiung Su , Chang-Chih Lin , Ching-Shang Sheng
IPC分类号： C07F9/02
CPC分类号： C07F9/657172
摘要： A bisbiphenylacylphosphine oxide of formula (I) and its preparation method are provided. The formula of —Ar— is First, 10-chloro-9,10-dihydro-9-oxa-10-phosphaphenanthrene (CDOP) is prepared by using 2-phenylphenol, and then is esterified to synthesize 6-methoxy-(6H)-dibenz[c,e][1,2]oxa-phosphorin (MDOP). Next, acid chloride compounds are added for performing the Arbuzov reaction to synthesize bisbiphenylacylphosphine oxide. CDOP is hydrolyzed to be derived into 9,10-dihydro-9-oxa-10-phosphaphen-anthrene-10-oxide (DOPO), and then DOPO reacts with arylaldehyde to form secondary alcohol. Therefore, bisbiphenylacylphosphine oxide is prepared by using secondary alcohol under oxidation. Also, under a coupling reaction, DOPO reacts with the acid chloride compounds by using a Lewis acid as a catalyst to prepare bisbiphenylacylphosphine oxide.

6. 发明申请

US20080255381A1 BISBIPHENYLACYLPHOSPHINE OXIDE AND PREPARATION METHOD THEREFORE 有权
公开(公告)号：US20080255381A1
公开(公告)日：2008-10-16
申请号：US12141354
申请日：2008-06-18
申请人： Wen-Chiung Su , Chang-Chih Lin , Ching-Shang Sheng
发明人： Wen-Chiung Su , Chang-Chih Lin , Ching-Shang Sheng
IPC分类号： C07F9/40
CPC分类号： C07F9/657172
摘要： A bisbiphenylacylphosphine oxide of formula (I) and its preparation method are provided. The formula of —Ar— is First, 10-chloro-9,10-dihydro-9-oxa-10-phosphaphenanthrene (CDOP) is prepared by using 2-phenylphenol, and then is esterified to synthesize 6-methoxy-(6H)-dibenz[c,e][1,2]oxa-phosphorin (MDOP). Next, acid chloride compounds are added for performing the Arbuzov reaction to synthesize bisbiphenylacylphosphine oxide. CDOP is hydrolyzed to be derived into 9,10-dihydro-9-oxa-10-phosphaphen-anthrene-10-oxide (DOPO), and then DOPO reacts with arylaldehyde to form secondary alcohol. Therefore, bisbiphenylacylphosphine oxide is prepared by using secondary alcohol under oxidation. Also, under a coupling reaction, DOPO reacts with the acid chloride compounds by using a Lewis acid as a catalyst to prepare bisbiphenylacylphosphine oxide.

7. 发明授权

US07250509B1 Method for preparing melamine salt of pentaerypolyol phosphoric acid 有权
标题翻译：五酸多元醇磷酸三聚氰胺盐的制备方法
公开(公告)号：US07250509B1
公开(公告)日：2007-07-31
申请号：US11443293
申请日：2006-05-31
申请人： Yu-Sheng Lin , Wen-Chiung Su , Chong Ma , Yuen-Hsin Peng
发明人： Yu-Sheng Lin , Wen-Chiung Su , Chong Ma , Yuen-Hsin Peng
IPC分类号： C07D251/54 , C07F9/6571
CPC分类号： C07F9/65748 , C07D251/54 , C08K5/0066 , C08K5/5205
摘要： A method for preparing a melamine salt of pentaerypolyol phosphoric acid is provided. The method comprises the following steps of: ball milling a mixture of pentaerypolyol and phosphorus pentoxide (P2O5) under a solvent-free reacting environment to obtain a pentaerypolyol phosphoric acid, and ball milling a mixture of a pentaerypolyol phosphoric acid and melamine without organic solvent reacting environment to obtain a melamine salt of pentaerypolyol phosphoric acid.
摘要翻译：提供了制备五元醇多磷酸的三聚氰胺盐的方法。该方法包括以下步骤：在无溶剂的反应环境下将五元多元醇和五氧化二磷（P 2 O 5 O 5）的混合物球磨，得到五元醇多元醇磷酸，并在没有有机溶剂反应环境的情况下球磨五聚多元醇磷酸和三聚氰胺的混合物，得到五元醇多磷酸的三聚氰胺盐。

8. 发明申请

US20070173659A1 Bisbiphenylacylphosphine oxide and preparation method therefore 有权
标题翻译：二苯基酰基氧化膦及其制备方法
公开(公告)号：US20070173659A1
公开(公告)日：2007-07-26
申请号：US11337441
申请日：2006-01-24
申请人： Wen-Chiung Su , Chang-Chih Lin , Ching-Shang Sheng
发明人： Wen-Chiung Su , Chang-Chih Lin , Ching-Shang Sheng
IPC分类号： C07F9/02
CPC分类号： C07F9/657172
摘要： A bisbiphenylacylphosphine oxide of formula (I) and its preparation method are provided. The formula of —Ar— is First, 10-chloro-9,10-dihydro-9-oxa-10-phosphaphenanthrene (CDOP) is prepared by using 2-phenylphenol, and then is esterified to synthesize 6-methoxy-(6H)-dibenz[c,e][1,2]oxa-phosphorin (MDOP). Next, acid chloride compounds are added for performing the Arbuzov reaction to synthesize bisbiphenylacylphosphine oxide. CDOP is hydrolyzed to be derived into 9,10-dihydro-9-oxa-10-phosphaphen-anthrene-10-oxide (DOPO), and then DOPO reacts with arylaldehyde to form secondary alcohol. Therefore, bisbiphenylacylphosphine oxide is prepared by using secondary alcohol under oxidation. Also, under a coupling reaction, DOPO reacts with the acid chloride compounds by using a Lewis acid as a catalyst to prepare bisbiphenylacylphosphine oxide.
摘要翻译：提供式（I）的双联苯酰基氧化膦及其制备方法。 -Ar-的配方是通过使用2-苯基苯酚制备10-氯-9,10-二氢-9-氧杂-10-磷杂菲（CDOP），然后酯化合成6-甲氧基 - （6H） - 二苯并[c，e] [1,2]氧杂 - 磷杂（MDOP）。接下来，加入酰氯化合物进行Arbuzov反应以合成双联苯基酰基氧化膦。将CDOP水解成9,10-二氢-9-氧杂-10-磷杂蒽-10-氧化物（DOPO），然后DOPO与芳基醛反应形成仲醇。因此，通过使用仲醇在氧化下制备双联苯基酰基氧化膦。此外，在偶联反应中，DOPO通过使用路易斯酸作为催化剂与酰基氯化合物反应以制备双联苯基酰基氧化膦。

9. 发明申请

US20130123457A1 Low-k, Flame-Retardant, Bi-Functional Benzoxazine and Method for Making the Same 有权
标题翻译：低k，阻燃剂，双功能苯并恶嗪及其制备方法
公开(公告)号：US20130123457A1
公开(公告)日：2013-05-16
申请号：US13396891
申请日：2012-02-15
申请人： Wen-Chiung Su , Ching-Hsuan Lin , Hung-Tse Lin , Feng-Jen Wang
发明人： Wen-Chiung Su , Ching-Hsuan Lin , Hung-Tse Lin , Feng-Jen Wang
IPC分类号： C08G59/02 , C07F9/6571
CPC分类号： C07D413/10 , C07F9/657172 , C08G14/06 , C08G59/4071 , C08G59/5046
摘要： Disclosed is a method for making a low-k, flame-retardant, bi-functional benzoxazine. The method includes the steps of dissolving phosphoric diamine with various functional groups, phenolic adamantane and paraformaldehyde in a solvent at 72° C. to 88° C. for 7 to 9 hours, and cooling and introducing the solution in n-hexane to separate the low-k, flame-retardant, phosphoric, bi-functional benzoxazine.
摘要翻译：公开了制备低k阻燃双功能苯并恶嗪的方法。该方法包括以下步骤：将各种官能团的磷二胺，酚金刚烷和多聚甲醛溶解在溶剂中，在72〜88℃下反应7〜9小时，冷却并将溶液引入正己烷中，低k，阻燃，磷酸，双功能苯并恶嗪。

10. 发明申请

US20130053529A1 Bridged Bis(Alkoxysilane) or Silsesquioxane Compound Having Benzoxazine-Containing Group 有权
标题翻译：桥联双（烷氧基硅烷）或含有苯并嗪的硅倍半氧烷化合物
公开(公告)号：US20130053529A1
公开(公告)日：2013-02-28
申请号：US13222015
申请日：2011-08-31
申请人： Wen-Chiung Su , Ying-Ling Liu
发明人： Wen-Chiung Su , Ying-Ling Liu
IPC分类号： C08G77/18 , C07F7/10
CPC分类号： C08G77/52 , C07F7/0838 , C07F7/1804 , C08G77/54
摘要： A benzoxazine-bridged compound is provided. The compound has a low dielectric constant, a high mechanic strength and a high glass transition temperature. The compound has a highly cross-linked structure with a yellow-light photoluminescent emission. Characterization of the present disclosure has been conducted with Fourier transform infrared, nuclear magnetic resonance, molecular mass and elemental analysis.
摘要翻译：提供苯并恶嗪桥接化合物。该化合物具有低介电常数，高机械强度和高玻璃化转变温度。该化合物具有黄色光致发光发射的高度交联结构。利用傅里叶变换红外，核磁共振，分子量和元素分析进行了本公开的表征。

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