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1. 发明授权

US4714766A Process for the preparation of 2-chlorobenzoxazoles 失效
标题翻译： 2-氯苯并恶唑的制备方法
公开(公告)号：US4714766A
公开(公告)日：1987-12-22
申请号：US885148
申请日：1986-07-14
申请人： Johannes Becherer , Reinhardt Handte , Hans J. Nestler , Ulrich Kussmaul
发明人： Johannes Becherer , Reinhardt Handte , Hans J. Nestler , Ulrich Kussmaul
IPC分类号： C07D263/58 , C07D263/54
CPC分类号： C07D263/58
摘要： The process for the preparation of 2-chlorobenzoxazoles of the formula ##STR1## wherein R.sup.1 and R.sup.2, independently of one another, are hydrogen or halogen comprising reacting a benzoxazolinone of the formula ##STR2## with a molar excess of phosphorus pentachloride.
摘要翻译：制备式“IMAGE”的2-氯苯并恶唑的方法，其中R1和R2彼此独立地是氢或卤素，包括使式“IMAGE”的苯并恶唑啉酮与摩尔过量的五氯化磷反应。

2. 发明授权

US4517370A Process for preparing 2-chlorobenzoxazoles 失效
标题翻译：制备2-氯苯并恶唑的方法
公开(公告)号：US4517370A
公开(公告)日：1985-05-14
申请号：US467742
申请日：1983-02-18
申请人： Johannes Becherer , Klaus Kuhlein , Ulrich Kussmaul
发明人： Johannes Becherer , Klaus Kuhlein , Ulrich Kussmaul
IPC分类号： C07D263/58 , C07D263/54
CPC分类号： C07D263/58
摘要： In the process for preparing 2-chlorobenzoxazoles of the formula ##STR1## wherein each of R.sup.1, R.sup.2, R.sup.3 and R.sup.4 is independently of one another, H, chloro or alkyl having 1 to 4 carbon atoms, which comprises reacting chlorine with 2-mercaptobenzoxazoles of the formula ##STR2## wherein the improvement comprises providing a melt of previously prepared 2-chloro-benzoxazole, adding the 2-mercaptobenzoxazole reactant to the 2-chlorobenzoxazole melt and simultaneously or subsequently passing chlorine into the melt, with the proviso that substituents R.sup.1 to R.sup.4 are identical in both the 2-chlorobenzoxazole melt and the 2-mercaptobenzoxazole reactant.
摘要翻译：在制备式（IMAGE）的2-氯苯并恶唑的方法中，其中R 1，R 2，R 3和R 4各自独立地为H，氯或具有1至4个碳原子的烷基，其包括使氯与2-巯基苯并恶唑其中改进包括提供预先制备的2-氯 - 苯并恶唑的熔体，将2-巯基苯并恶唑反应物加入到2-氯苯并恶唑熔体中，同时或随后将氯进入熔体，条件是取代基R 1 到R4在2-氯苯并恶唑熔体和2-巯基苯并恶唑反应物中都是相同的。

3. 发明授权

US5489647A Hydrophilic, swellable graft polymers 失效
标题翻译：亲水性，可溶胀的接枝聚合物
公开(公告)号：US5489647A
公开(公告)日：1996-02-06
申请号：US977002
申请日：1992-11-16
申请人： Ulrich Kussmaul , Manfred Mayer , Uwe Stuven , Ulrich Riegel , Friedrich Engelhardt
发明人： Ulrich Kussmaul , Manfred Mayer , Uwe Stuven , Ulrich Riegel , Friedrich Engelhardt
IPC分类号： A61L15/00 , A61L15/60 , C08F251/00 , C08F283/06
CPC分类号： C08F251/00 , A61L15/60
摘要： The present invention relates to hydrophilic, swellable graft polymers which comprise, in a random distribution, from 0.5 to 50% by weight of radicals of the general formula I ##STR1## and radicals of the general formula II ##STR2## from 49 to 99% by weight of radicals of the general formula III ##STR3## containing an acid group, and from 0.1 to 2% by weight of radicals of a crosslinking agent which are derived from monomers containing at least two olefinically unsaturated double bonds, where the radicals R.sup.1 to R.sup.4, X and Y and n and m are where X and Y, independently of one another are COCH.sub.3, CH.sub.2 COOR.sup.2, COCH.sub.2 CH.sub.2 COOH ##STR4## n and m, independently of one another, are 2 to 300, R.sup.1 is hydrogen or methyl, R.sup.2, independently of one another, are hydrogen, methyl or ethyl, R.sup.3 is the carboxyl group, the sulphonyl group, the phosphonyl group, which is optionally esterified by means of alkanol having 1 to 4 carbon atoms, or a group of the formula ##STR5## to the preparation thereof, and to the use thereof as absorbents for water and aqueous solutions.
摘要翻译：本发明涉及亲水性，可溶胀的接枝聚合物，其以无规分布包含0.5至50重量％的通式I（I）的基团和通式II的基团（II））49至99重量％的含有酸基团的通式III（III）的基团和0.1至2重量％的衍生自含有至少两个烯属的单体的交联剂的基团不饱和双键，其中基团R 1至R 4，X和Y以及n和m是其中X和Y彼此独立地是COCH 3，CH 2 COOR 2，COCH 2 CH 2 COOH，另一个是2至300，R 1是氢或甲基，R 2，独立地是氢，甲基或乙基，R3是羧基，磺酰基，膦酰基，其任选地通过具有1至4个碳原子的链烷醇酯化，或下式的组：作为水和水溶液的吸收剂。

4. 发明授权

US4401603A Process for the preparation of aryl isocyanide-dichlorides 失效
标题翻译：芳基异氰化物 - 二氯化物的制备方法
公开(公告)号：US4401603A
公开(公告)日：1983-08-30
申请号：US394253
申请日：1982-07-01
申请人： Dieter Ferchland , Ulrich Kussmaul , Manfred Langer , Rolf Muller
发明人： Dieter Ferchland , Ulrich Kussmaul , Manfred Langer , Rolf Muller
IPC分类号： C07C241/00 , C07C67/00 , C07C291/10 , C07C119/00
CPC分类号： C07C251/00
摘要： An improved process for preparation of arylisocyanide dichloride by chlorinating N-arylformamide in the presence of thionyl chloride wherein the improvement comprises preparing the N-arylformamide by formylation of an arylamine having 6 to 12 aryl carbon atoms with a formylating agent in an inert solvent.removing excess formylating agent and by-products of the formylation thereby leaving the N-arylformamide in the form of a solution or suspension in the inert solvent and chlorinating the N-arylformamide in solution or suspension with a chlorinating agent in the presence of thionyl chloride.
摘要翻译：通过在亚硫酰氯存在下氯化N-芳基甲酰胺来改进制备芳基异氰化物二氯化物的改进方法，其中改进包括通过在惰性溶剂中用甲酰化剂将具有6-12个芳基碳原子的芳基胺甲酰化制备N-芳基甲酰胺。

5. 发明授权

US4677209A Process for the preparation of 2-mercaptobenzoxazoles 失效
标题翻译： 2-巯基苯并恶唑的制备方法
公开(公告)号：US4677209A
公开(公告)日：1987-06-30
申请号：US844603
申请日：1986-03-27
申请人： Ulrich Kussmaul , Manfred Langer , Kuno Reh , Johannes Becherer , Herbert Wille , Rolf Muller
发明人： Ulrich Kussmaul , Manfred Langer , Kuno Reh , Johannes Becherer , Herbert Wille , Rolf Muller
IPC分类号： C07D263/58
CPC分类号： C07D263/58
摘要： 2-Mercaptobenzoxazoles of the formula ##STR1## wherein R is hydrogen or halogen and M is hydrogen or a metal atom, are prepared by reacting an ortho-aminophenol or metal salts thereof, with an alkali metal trithiocarbonate in aqueous solution.
摘要翻译：其中R为氢或卤素，M为氢或金属原子的式为“IMAGE”的2-巯基苯并恶唑通过其邻氨基苯酚或其金属盐与碱金属三硫代碳酸酯在水溶液中反应来制备。

6. 发明授权

US4564682A Process for the preparation of heterocyclic phenyl ethers 失效
标题翻译：制备杂环苯基醚的方法
公开(公告)号：US4564682A
公开(公告)日：1986-01-14
申请号：US583713
申请日：1984-02-27
申请人： Ulrich Kussmaul , Johannes Becherer , Reinhard Handte , Rolf Muller
发明人： Ulrich Kussmaul , Johannes Becherer , Reinhard Handte , Rolf Muller
IPC分类号： C07D235/26 , C07D263/58 , C07D277/68
CPC分类号： C07D263/58 , C07D235/26 , C07D277/68
摘要： A compound of the formula ##STR1## is reacted with a phenol of the formula ##STR2## in the presence of an acid to produce a heterocyclic phenyl ether of the formula ##STR3## wherein each R is independently selected from halogen, trifluoromethyl, nitro, cyano, alkyl having 1 to 4 carbon atoms, alkoxy having 1 to 4 carbon atoms or alkylthio having 1 to 4 carbon atoms;A is oxygen, sulfur or N-alkyl having 1 to 4 carbon atoms; andn is a number from 0 to 3.
摘要翻译：在酸存在下，将式“IMAGE”或“IMAGE”的化合物与式IMA的化合物反应，得到式IMA的杂环苯基醚，其中每个R独立地选自卤素，三氟甲基，硝基，氰基，具有1至4个碳原子的烷基，具有1至4个碳原子的烷氧基或具有1至4个碳原子的烷硫基; A是氧，硫或具有1至4个碳原子的N-烷基; n为0〜3的数。

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