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1. 发明授权

US5239111A Propylene glycol monomethyl ether propionate compound and the process for the preparation thereof 失效
标题翻译：丙二醇单甲醚丙酸酯化合物及其制备方法
公开(公告)号：US5239111A
公开(公告)日：1993-08-24
申请号：US960736
申请日：1992-10-14
申请人： Tzong-Jeng Chu , Neng-Hui Chu , Peng-Fei Lee
发明人： Tzong-Jeng Chu , Neng-Hui Chu , Peng-Fei Lee
IPC分类号： C07C67/08
CPC分类号： C07C67/08
摘要： A propylene glycol monomethyl ether propionate compound is obtained by the esterification of propylene glycol monomethyl ether with propionic acid at an elevated temperature above 80 .degree.C. in the presence of acidic catalyst and azeotropic agent. This compound is rectified for removing acid residue and moisture in order to yield the desirable product having high purity.
摘要翻译：通过在酸性催化剂和共沸剂存在下，在高于80℃的高温下，丙二醇单甲醚与丙酸的酯化得到丙二醇单甲醚丙酸酯化合物。该化合物被精馏以除去酸残余物和水分，以产生具有高纯度的所需产物。

2. 发明授权

US3950309A Novel thermosetting resins and process for preparing the same comprising reacting a novolak with a titanic acid ester 失效
标题翻译：新型热固性树脂及其制备方法，包括用氨基酸酯反应NOVOLAK
公开(公告)号：US3950309A
公开(公告)日：1976-04-13
申请号：US302207
申请日：1972-10-30
申请人： Tzong Jeng Chu , Susumu Konii
发明人： Tzong Jeng Chu , Susumu Konii
IPC分类号： C08G8/28 , C08G77/52 , C08G79/00 , C08G2/30
CPC分类号： C08G8/28 , C08G77/52 , C08G79/00
摘要： A novel thermosetting resin, the thermoset resin obtained therefrom having such a thermal resistance that the temperature at which the thermoset resin is caused to show a weight loss of 6% by heating at a temperature elevation rate of 10.degree.C. per minute is at least 400.degree.C., is prepared by reacting a specific phenolic resin with a member selected from the group consisting of a silicic acid ester of the formula Si(OR).sub.4 wherein R represents alkyl or aryl, a titanic acid ester of the formula Ti(OR).sub.4 wherein R has the same meaning as defined above and a mixture thereof in the presence of an alkaline catalyst while keeping the reaction system in a molten state, to an extent that 20 - 70 mole %, based on the phenol present in the starting system to be reacted with said member, of phenolic hydroxyl groups in terms of the amount of phenol, remain unreacted. The thus obtained novel resins of the present invention can be easily set or hardened in accordance with the ordinary manner; namely by mixing with a thermohardening agent such as hexamethylenetetramine and then heating, to give thermoset resins having a superior thermal resistance as compared with the conventional phenolic resins. In addition, the thermoset resins obtained from the novel resins of this invention are excellent in mechanical strength, electrical properties and luster of molded articles.

3. 发明授权

US5426214A Propylene glycol monomethyl ether butyrates and isomers, and the process for the preparation thereof 失效
标题翻译：丙二醇单甲醚丁酸酯和异构体及其制备方法
公开(公告)号：US5426214A
公开(公告)日：1995-06-20
申请号：US236712
申请日：1994-04-29
申请人： Tzong-Jeng Chu , Neng-Hui Chu , Huang Kuo-Chu , Chin Y. Lee
发明人： Tzong-Jeng Chu , Neng-Hui Chu , Huang Kuo-Chu , Chin Y. Lee
IPC分类号： C07C69/24 , C08J3/09 , C09D7/00 , C07C67/28 , C07C67/00
CPC分类号： C09D7/001 , C07C69/24 , C08J3/095
摘要： Propylene glycol monomethyl ether butyrates and their isomers are obtained by the esterification of propylene glycol monomethyl ether or its isomer with iso-butyric or n-butyric acid at an elevated temperature above 80.degree. C. in the presence of acidic catalyst and azeotropic agent. These compounds are rectified for removing acid residue and moisture in order to yield the desirable product having high purity.
摘要翻译：丙二醇单甲醚丁酸酯及其异构体是在酸性催化剂和共沸剂存在下，在高于80℃的高温下，通过丙二醇单甲醚或其异构体与异丁酸或正丁酸的酯化得到的。对这些化合物进行精馏以除去酸残余物和水分，以产生具有高纯度的所需产物。

4. 发明授权

US5321152A Propylene glycol monomethyl ether propionate compounds and the process for the preparation thereof 失效
标题翻译：丙二醇单甲醚丙酸酯化合物及其制备方法
公开(公告)号：US5321152A
公开(公告)日：1994-06-14
申请号：US105320
申请日：1993-08-02
申请人： Tzong-Jeng Chu , Neng-Hui Chu , Peng-Fei Lee
发明人： Tzong-Jeng Chu , Neng-Hui Chu , Peng-Fei Lee
IPC分类号： C07C67/08 , C07C67/10
CPC分类号： C07C67/08
摘要： Propylene glycol monomethyl ether propionate compounds are obtained by the esterification of propylene glycol monomethyl ether with propionic acid at an elevated temperature above 80.degree. C. in the presence of acidic catalyst and azeotropic agent. The compounds are rectified for removing acid residue and moisture in order to yield the desirable product having high purity.
摘要翻译：丙二醇单甲醚丙酸酯化合物是通过在酸性催化剂和共沸剂存在下，在高于80℃的高温下，丙二醇单甲醚与丙酸酯化得到的。精馏该化合物以除去酸残余物和水分，以产生具有高纯度的所需产物。

5. 发明授权

US4055546A Novel thermosetting resins and process for preparing the same 失效
标题翻译：新型热固性树脂及其制备方法
公开(公告)号：US4055546A
公开(公告)日：1977-10-25
申请号：US646671
申请日：1976-01-05
申请人： Tzong Jeng Chu , Susumu Konii
发明人： Tzong Jeng Chu , Susumu Konii
IPC分类号： C08G8/28 , C08G77/52 , C08G79/00 , C08G10/04
CPC分类号： C08G77/52 , C08G79/00 , C08G8/28
摘要： A novel thermosetting resin, the thermoset resin obtained therefrom having such a thermal resistance that the temperature at which the thermoset resin is caused to show a weight loss of 6% by heating at a temperature elevation rate of 10.degree. C. per minute is at least 400.degree. C., is prepared by reacting a specific phenolic resin with a member selected from the group consisting of a silicic acid ester of the formula Si(OR).sub.4 wherein R represents alkyl or aryl and a mixture of a silicic acid ester of the formula as defined above and a titanic acid ester of the formula Ti(OR).sub.4 wherein R has the same meaning as defined above in the presence of an alkaline catalyst while keeping the reaction system in a molten state, to an extent that 20- 70 mole %, based on the phenol present in the starting system to be reacted with said member, of phenolic hydroxyl groups in terms of the amount of phenol, remain unreacted. The thus obtained novel resins of the present invention can be easily set or hardened in accordance with the ordinary manner; namely by mixing with a thermohardening agent such as hexamethylenetetramine and then heating, to give thermoset resins having a superior thermal resistance as compared with the conventional phenolic resins. In addition, the thermoset resins obtained from the novel resins of this invention are excellent in mechanical strength, electrical properties and luster of molded articles.
摘要翻译：一种新型的热固性树脂，由其获得的热固性树脂具有这样的耐热性，使得热固性树脂的温度以每分钟10℃的升温速度加热显示出6％的重量损失，至少为通过使特定的酚醛树脂与选自由式Si（OR）4的硅酸酯（其中R表示烷基或芳基）和硅酸酯的混合物式（Ti）（OR）4的钛酸酯，其中R在碱性催化剂的存在下具有与上述相同的含义，同时保持反应体系处于熔融状态，至20-70℃ 基于与所述成员反应的起始体系中存在的苯酚，以苯酚的量计，酚羟基的摩尔％保持未反应。由此得到的本发明的新型树脂可以按照常规方式容易地固化或硬化; 即通过与诸如六亚甲基四胺的热硬化剂混合，然后加热，得到与常规酚醛树脂相比具有优异耐热性的热固性树脂。此外，由本发明的新型树脂得到的热固性树脂的机械强度，电性能和成型品的光泽性优异。

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