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1. 发明申请

US20090038991A1 EXTRACTIVE DISTILLATION PROCESS FOR RECOVERING AROMATICS FROM PETROLEUM STREAMS 有权
标题翻译：从石油回收回收芳烃的提取蒸馏工艺
公开(公告)号：US20090038991A1
公开(公告)日：2009-02-12
申请号：US11837459
申请日：2007-08-10
申请人： KUANG YEU WU , TSUNG-MIN CHIU , TZONG-BIN LIN , HUNG-CHUNG SHEN , YU-MING WU , TUNG-HSIUNG KUO
发明人： KUANG YEU WU , TSUNG-MIN CHIU , TZONG-BIN LIN , HUNG-CHUNG SHEN , YU-MING WU , TUNG-HSIUNG KUO
IPC分类号： C10G51/02 , B01J8/04
CPC分类号： B01D3/40 , C10G7/08
摘要： The present invention relates to a process for recovering polar hydrocarbons from non-polar hydrocarbons, such as aromatics from non-aromatics, naphthenes from paraffins and isoparaffins, or olefins from paraffins and isoparaffins, in feed mixtures containing at least a measurable amount of heavier hydrocarbons. According to the invention, an improved extractive distillation (ED) process is disclosed for recovering aromatic hydrocarbons including benzene, toluene, and xylenes (BTX aromatics) from the C6-C8 petroleum streams containing at least a measurable amount of C9+ hydrocarbons.The invention also relates to an improved ED process for recovering mainly benzene and toluene from the C6-C7 petroleum streams containing at least a measurable amount of C8+ hydrocarbons. This invention is further directed toward the regeneration and recovery of the ED solvent utilized to recover and purify the aromatic hydrocarbons from the petroleum stream containing at least a measurable amount of hydrocarbons heavier than intend feedstock.
摘要翻译：本发明涉及一种从非极性烃中回收极性烃的方法，例如来自非芳族化合物的芳族化合物，来自烷烃和异链烷烃的环烷烃，或来自链烷烃和异链烷烃的烯烃在含有至少可测量量的较重烃。根据本发明，公开了一种改进的萃取蒸馏（ED）方法，用于从含有至少可测量量的C 9+烃的C6-C8石油流中回收包括苯，甲苯和二甲苯（BTX芳族化合物）的芳烃。本发明还涉及一种改进的ED方法，主要从含有至少可测量量的C8 +烃的C6-C7石油流中回收苯和甲苯。本发明进一步涉及用于回收和纯化来自含有至少可测量量的比目标原料重的烃的石油流中的芳烃的ED溶剂的再生和回收。

2. 发明授权

US08900449B2 Magnetic filter for refining and chemical industries 有权
标题翻译：精炼和化工行业的磁性过滤器
公开(公告)号：US08900449B2
公开(公告)日：2014-12-02
申请号：US13419407
申请日：2012-03-13
申请人： Tzong-Bin Lin , Fu-Ming Lee , Jeng-Cheng Lee , Fred G. Tahmassi , Benjamin Poi Chen , Tsung-Min Chiu , Kuang-Yeu Wu
发明人： Tzong-Bin Lin , Fu-Ming Lee , Jeng-Cheng Lee , Fred G. Tahmassi , Benjamin Poi Chen , Tsung-Min Chiu , Kuang-Yeu Wu
IPC分类号： B03C1/02 , B03C1/26 , B03C1/30 , B03C1/28
CPC分类号： B03C1/286 , B03C1/30 , B03C2201/18 , B03C2201/28
摘要： A magnetic filter employs a magnetic core assembly that incorporates a plurality of exchangeable holder sleeves, each enclosing permanent magnets. Neither the sleeves nor magnetic bars are mechanically fixed to the filter housing. The magnet bars and holder sleeves are individually accessible. The number of holder sleeves in the magnetic core assembly is flexible. The magnetic filter in equipped with a screen that partially encloses the elongated holder sleeves to treat streams that contain degradation sludge, iron containing particles or flakes, and non-magnetic polymeric materials. In operation, a feed stream initially contacts the magnetic core assembly where paramagnetic contaminants become deposited onto the exterior surface of the holder sleeves under direct influence of strong magnetic field generated by the magnet bars. The mesh screen cylinder subsequently captures non-magnetic and weakly magnetic contaminants of a certain size before the cleaned stream exits the magnetic filter.
摘要翻译：磁性过滤器采用磁芯组件，其包含多个可更换的保持套筒，每个包封永磁体。袖子和磁条都不是机械地固定在过滤器外壳上。磁棒和保持套可以单独使用。磁芯组件中的保持套筒的数量是灵活的。装有屏幕的磁性过滤器部分地包围细长的保持器套筒以处理含有劣化污泥，含铁颗粒或薄片的流和非磁性聚合材料。在操作中，进料流最初接触磁芯组件，其中顺磁性污染物在由磁棒产生的强磁场的直接影响下沉积到保持器套筒的外表面上。网状筛筒随后在清洁的流离开磁性过滤器之前捕获一定尺寸的非磁性和弱磁性污染物。

3. 发明申请

US20130240455A1 Magnetic Filter for Refining and Chemical Industries 有权
标题翻译：炼油化工行业磁性过滤器
公开(公告)号：US20130240455A1
公开(公告)日：2013-09-19
申请号：US13419407
申请日：2012-03-13
申请人： Tzong-Bin Lin , Fu-Ming Lee , Jeng-Cheng Lee , Fred G. Tahmassi , Benjamin Poi Chen , Tsung-Min Chiu , Kuang-Yeu Wu
发明人： Tzong-Bin Lin , Fu-Ming Lee , Jeng-Cheng Lee , Fred G. Tahmassi , Benjamin Poi Chen , Tsung-Min Chiu , Kuang-Yeu Wu
IPC分类号： B03C1/30 , B03C1/02
CPC分类号： B03C1/286 , B03C1/30 , B03C2201/18 , B03C2201/28
摘要： A magnetic filter employs a magnetic core assembly that incorporates a plurality of exchangeable holder sleeves, each enclosing permanent magnets. Neither the sleeves nor magnetic bars are mechanically fixed to the filter housing. The magnet bars and holder sleeves are individually accessible. The number of holder sleeves in the magnetic core assembly is flexible. The magnetic filter in equipped with a screen that partially encloses the elongated holder sleeves to treat streams that contain degradation sludge, iron containing particles or flakes, and non-magnetic polymeric materials. In operation, a feed stream initially contacts the magnetic core assembly where paramagnetic contaminants become deposited onto the exterior surface of the holder sleeves under direct influence of strong magnetic field generated by the magnet bars. The mesh screen cylinder subsequently captures non-magnetic and weakly magnetic contaminants of a certain size before the cleaned stream exits the magnetic filter.
摘要翻译：磁性过滤器采用磁芯组件，其包含多个可更换的保持套筒，每个包封永磁体。袖子和磁条都不是机械地固定在过滤器外壳上。磁棒和保持套可以单独使用。磁芯组件中的保持套筒的数量是灵活的。装有屏幕的磁性过滤器部分地包围细长的保持器套筒以处理含有劣化污泥，含铁颗粒或薄片的流和非磁性聚合材料。在操作中，进料流最初接触磁芯组件，其中顺磁性污染物在由磁棒产生的强磁场的直接影响下沉积到保持器套筒的外表面上。网状筛筒随后在清洁的流离开磁性过滤器之前捕获一定尺寸的非磁性和弱磁性污染物。

4. 发明授权

US07871514B2 Extractive distillation processes using water-soluble extractive solvents 有权
标题翻译：使用水溶性萃取溶剂的萃取蒸馏方法
公开(公告)号：US07871514B2
公开(公告)日：2011-01-18
申请号：US12316405
申请日：2008-12-12
申请人： Fu-Ming Lee , Tzong-Bin Lin , Jyh-Haur Hwang , Hung-Chung Shen , Kuang-Yeu Wu , Tsung-Min Chiu , Zong-Ying Chen , Tung-Hsiung Kuo , Yu-Ming Wu
发明人： Fu-Ming Lee , Tzong-Bin Lin , Jyh-Haur Hwang , Hung-Chung Shen , Kuang-Yeu Wu , Tsung-Min Chiu , Zong-Ying Chen , Tung-Hsiung Kuo , Yu-Ming Wu
IPC分类号： C07C7/00
CPC分类号： B01D3/40 , C10G7/08 , C10G2400/30
摘要： Extractive distillation processes whereby water-soluble extractive distillation (ED) solvents are regenerated and recovered employ improved operations of the extractive distillation column (EDC) so that polar hydrocarbons are recovered and purified from mixtures containing polar and less polar hydrocarbons and measurable amounts of hydrocarbons that are heavier than intended feedstock and/or polymers that are generated in the ED process. The improved process can effectively remove and recover the heavy hydrocarbons and/or remove polymer contaminants from the solvent in a closed solvent circulating loop through mild operating conditions with no additional process energy being expended. With the improved process, the overhead reflux of the EDC may be eliminated to further reduce energy consumption and to enhance the loading and performance within the upper portion of the EDC, especially when two liquid phases exists therein.
摘要翻译：萃取蒸馏方法，其中水溶性萃取蒸馏（ED）溶剂被再生和回收利用萃取蒸馏塔（EDC）的改进操作，使极性烃从含有极性和极性较小的烃的混合物中回收和纯化，比在ED过程中产生的预期原料和/或聚合物重。改进的方法可以在封闭的溶剂循环回路中通过温和的操作条件有效地除去和回收重质烃和/或从溶剂中除去聚合物污染物，而不需要额外的工艺能量消耗。通过改进的方法，可以消除EDC的顶部回流以进一步降低能量消耗并增强EDC上部的负载和性能，特别是当存在两个液相时。

5. 发明申请

US20130228447A1 Extractive Distillation Process For Benzene Recovery 有权
标题翻译：萃取蒸馏工艺用于苯回收
公开(公告)号：US20130228447A1
公开(公告)日：2013-09-05
申请号：US13410286
申请日：2012-03-01
申请人： Kuang-Yeu Wu , Tzong-Bin Lin , Fu-Ming Lee , Tsung-Min Chiu , Jeng-Cheng Lee
发明人： Kuang-Yeu Wu , Tzong-Bin Lin , Fu-Ming Lee , Tsung-Min Chiu , Jeng-Cheng Lee
IPC分类号： B01D3/40
CPC分类号： B01D3/40 , C07C7/08 , C07C15/04
摘要： Recovering high purity benzene from hydrocarbon feedstock containing aromatics and non-aromatics is implemented by simple and low-cost modifications to conventional extractive distillation columns (EDCs). Methyl cyclohexane (MCH) that is generated through non-selective hydrogenation of toluene in hydrodesulfurization (HDS) units is a major contaminant in benzene production. To meet MCH specifications, often times the extractive distillation (ED) process for recovering purified benzene is operated with excessive benzene loss to the overhead raffinate stream, producing a lower quality non-aromatic product. Novel techniques (1) remove operational constrictions of the HDS unit on MCH production, thus lengthening the catalyst life and (2) allow the EDC to drive essentially any amount of MCH away from the bottom benzene product without concerns with benzene loss to the overhead raffinate stream and (3) recover benzene from the overhead raffinate stream to upgrade the quality of non-aromatic product and increase the benzene product recovery.
摘要翻译：通过对常规萃取蒸馏塔（EDC）的简单且低成本的改进来实现从芳族化合物和非芳族化合物的烃原料中回收高纯度苯。通过在加氢脱硫（HDS）单位中甲苯的非选择性氢化产生的甲基环己烷（MCH）是苯生产中的主要污染物。为了满足MCH规范，通常多次用于回收纯化苯的萃取蒸馏（ED）方法对顶部萃余液流具有过量的苯损失，产生较低质量的非芳族产物。新技术（1）消除了HDS单元在MCH生产中的操作限制，从而延长了催化剂寿命，（2）允许EDC将基本上任意数量的MCH从底部苯产品中驱出，而不考虑苯损失到塔顶残液流和（3）从塔顶残液流回收苯，提高非芳香族产品的质量，提高苯产品回收率。

6. 发明授权

US08246815B2 Methods for regeneration of solvents for extractive processes 有权
标题翻译：萃取过程溶剂再生方法
公开(公告)号：US08246815B2
公开(公告)日：2012-08-21
申请号：US12854150
申请日：2010-08-10
申请人： Kuang-Yeu Wu , Tzong-Bin Lin , Fu-Ming Lee , Tsung-Min Chiu , Jyh-Haur Hwang , Hung-Chung Shen
发明人： Kuang-Yeu Wu , Tzong-Bin Lin , Fu-Ming Lee , Tsung-Min Chiu , Jyh-Haur Hwang , Hung-Chung Shen
IPC分类号： C10G51/02
CPC分类号： C07C7/08 , C07D333/48 , C10G21/28 , C10G2300/1081 , C10G2300/1088 , C10G2300/1096 , C10G2300/44 , C10G2300/805 , C07C15/04 , C07C15/06
摘要： An improved solvent regeneration system for extractive distillation and liquid-liquid extraction processes capable of effectively removing heavy hydrocarbons and polymeric materials that otherwise develop in a closed solvent loop. The improved process employs a light hydrocarbon displacement agent, which is at least partially soluble in the solvent to squeeze the heavy hydrocarbons and polymeric materials out of the solvent, with virtually no additional energy requirement. It has been demonstrated that the light non-aromatic hydrocarbons in the raffinate stream generated from the extractive distillation or the liquid-liquid extractive process for aromatic hydrocarbons recovery can displace not only the heavy non-aromatic hydrocarbons but also the heavy aromatic hydrocarbons from the extractive solvent, especially when the aromatic hydrocarbons in the solvent are in the C10+ molecular weight range.
摘要翻译：用于萃取蒸馏和液 - 液萃取方法的改进的溶剂再生系统，其能够有效地除去否则在密闭的溶剂回路中发展的重质烃和聚合材料。改进的方法采用轻质烃置换剂，其至少部分可溶于溶剂以将重质烃和聚合物材料挤出溶剂，实际上无需额外的能量需求。已经证明，从萃取蒸馏或用于芳族烃回收的液 - 液萃取过程产生的萃余液流中的轻非芳族烃不仅可以取代重非芳族烃，而且可以取代萃取物中的重芳香烃溶剂，特别是当溶剂中的芳烃为C10 +分子量范围时。

7. 发明授权

US07879225B2 Energy efficient and throughput enhancing extractive process for aromatics recovery 有权
标题翻译：能量效率和通量提高芳烃回收的萃取过程
公开(公告)号：US07879225B2
公开(公告)日：2011-02-01
申请号：US12217676
申请日：2008-07-08
申请人： Fu-Ming Lee , Kuang-Yeu Wu , Tsung-Min Chiu , Zong-Ying Chen , Jyh-Haur Hwang , Tzong-Bin Lin , Hung-Chung Shen , Tung-Hsiung Kuo , Yu-Ming Wu
发明人： Fu-Ming Lee , Kuang-Yeu Wu , Tsung-Min Chiu , Zong-Ying Chen , Jyh-Haur Hwang , Tzong-Bin Lin , Hung-Chung Shen , Tung-Hsiung Kuo , Yu-Ming Wu
IPC分类号： C10G21/28
CPC分类号： C10G21/06 , C10G21/28 , C10G2300/4056
摘要： An energy efficient, high throughput process for aromatics recovery can be readily implemented by revamping existing sulfolane solvent extraction facilities, or constructing new ones, so as to incorporate unique process operations involving liquid-liquid extraction and extractive distillation. Current industrial sulfolane solvent based liquid-liquid extraction processes employ a liquid-liquid extraction column, an extractive stripping column, a solvent recovery column, a raffinate wash column, and a solvent regenerator. The improved process for aromatic hydrocarbon recovery from a mixture of aromatic and non-aromatic hydrocarbons requires transformation of the extractive stripping column into a modified extractive distillation column. The revamping incorporates the unique advantages of liquid-liquid extraction and extractive distillation into one process to significantly reduce energy consumption and increase process throughput. The revamp entails essentially only piping changes and minor equipment adjustments of the original liquid-liquid extraction facility, and is therefore, reversible.
摘要翻译：通过改进现有的环丁砜溶剂萃取设备或构建新的环丁砜溶剂萃取设备，可以容易地实现能量效率高的芳烃回收方法，从而引入独特的工艺操作，包括液 - 液萃取和萃取蒸馏。当前工业环丁砜溶剂型液 - 液萃取方法采用液 - 液萃取柱，萃取汽提塔，溶剂回收塔，萃余液洗涤塔和溶剂再生器。从芳烃和非芳烃的混合物中回收芳烃的改进方法需要将萃取汽提塔转化为改进的萃取蒸馏塔。改造将液 - 液萃取和萃取蒸馏的独特优势融入到一个过程中，以显着降低能耗并提高生产能力。改造只需要对原液 - 液萃取设备进行管道更换和小型设备调整，因此是可逆的。

8. 发明授权

US07666299B2 Extractive distillation process for recovering aromatics from petroleum streams 有权
标题翻译：从石油流中回收芳族化合物的萃取蒸馏方法
公开(公告)号：US07666299B2
公开(公告)日：2010-02-23
申请号：US11837459
申请日：2007-08-10
申请人： Kuang-Yeu Wu , Tsung-Min Chiu , Tzong-Bin Lin , Hung-Chung Shen , Yu-Ming Wu , Tung-Hsiung Kuo
发明人： Kuang-Yeu Wu , Tsung-Min Chiu , Tzong-Bin Lin , Hung-Chung Shen , Yu-Ming Wu , Tung-Hsiung Kuo
IPC分类号： C10G51/02
CPC分类号： B01D3/40 , C10G7/08
摘要： A process for recovering polar hydrocarbons from non-polar hydrocarbons, such as aromatics from non-aromatics, naphthenes from paraffins and isoparaffins, or olefins from paraffins and isoparaffins, in feed mixtures containing at least a measurable amount of heavier hydrocarbons. This improved extractive distillation (ED) process recovers aromatic hydrocarbons including benzene, toluene, and xylenes from the C6-C8 petroleum streams containing a measurable amount of C9+ hydrocarbons. The ED process also recovers benzene and toluene from the C6-C7 petroleum streams containing a measurable amount of C8+ hydrocarbons. The ED solvent utilized to recover and purify the aromatic hydrocarbons from the petroleum stream with a heavier than intended feedstock of hydrocarbons is also regenerated and recovered.
摘要翻译：一种从非极性烃中回收极性烃的方法，例如来自非芳族化合物的芳族化合物，来自烷烃和异链烷烃的环烷烃，或来自链烷烃和异链烷烃的烯烃在含有至少可测量量的较重烃的进料混合物中。这种改进的萃取蒸馏（ED）方法从含有可测量量的C 9+烃的C6-C8石油流中回收包括苯，甲苯和二甲苯的芳族烃。 ED方法还从含有可测量量的C8 +烃的C6-C7石油流中回收苯和甲苯。用于从石油流中回收和纯化比预期的烃类原料重的芳烃的ED溶剂也被再生和回收。

9. 发明申请

US20090255853A1 Novel energy efficient and throughput enhancing extractive process for aromatics recovery 有权
标题翻译：用于芳烃回收的新型能量效率和通量提高萃取方法
公开(公告)号：US20090255853A1
公开(公告)日：2009-10-15
申请号：US12217676
申请日：2008-07-08
申请人： Fu-Ming Lee , Kuang-Yeu Wu , Tsung-Min Chiu , Zong-Ying Chen , Jyh-Haur Hwang , Tzong-Bin Lin , Hung-Chung Shen , Tung-Hsiung Kuo , Yu-Ming Wu
发明人： Fu-Ming Lee , Kuang-Yeu Wu , Tsung-Min Chiu , Zong-Ying Chen , Jyh-Haur Hwang , Tzong-Bin Lin , Hung-Chung Shen , Tung-Hsiung Kuo , Yu-Ming Wu
IPC分类号： C10G21/28
CPC分类号： C10G21/06 , C10G21/28 , C10G2300/4056
摘要： An energy efficient, high throughput process for aromatics recovery can be readily implemented by revamping existing sulfolane solvent extraction facilities, or constructing new ones, so as to incorporate unique process operations involving liquid-liquid extraction and extractive distillation. Current industrial sulfolane solvent based liquid-liquid extraction processes employ a liquid-liquid extraction column, an extractive stripping column, a solvent recovery column, a raffinate wash column, and a solvent regenerator. The improved process for aromatic hydrocarbon recovery from a mixture of aromatic and non-aromatic hydrocarbons requires transformation of the extractive stripping column into a modified extractive distillation column. The revamping incorporates the unique advantages of liquid-liquid extraction and extractive distillation into one process to significantly reduce energy consumption and increase process throughput. The revamp entails essentially only piping changes and minor equipment adjustments of the original liquid-liquid extraction facility, and is therefore, reversible.
摘要翻译：通过改进现有的环丁砜溶剂萃取设备或构建新的环丁砜溶剂萃取设备，可以容易地实现能量效率高的芳烃回收方法，从而引入独特的工艺操作，包括液 - 液萃取和萃取蒸馏。当前工业环丁砜溶剂型液 - 液萃取方法采用液 - 液萃取柱，萃取汽提塔，溶剂回收塔，萃余液洗涤塔和溶剂再生器。从芳烃和非芳烃的混合物中回收芳烃的改进方法需要将萃取汽提塔转化为改进的萃取蒸馏塔。改造将液 - 液萃取和萃取蒸馏的独特优势融入到一个过程中，以显着降低能耗并提高生产能力。改造只需要对原液 - 液萃取设备进行管道更换和小型设备调整，因此是可逆的。

10. 发明申请

US20090105514A1 Extractive distillation processes using water-soluble extractive solvents 有权
标题翻译：使用水溶性萃取溶剂的萃取蒸馏方法
公开(公告)号：US20090105514A1
公开(公告)日：2009-04-23
申请号：US12316405
申请日：2008-12-12
申请人： Fu-Ming Lee , Tzong-Bin Lin , Jyh-Haur Hwang , Hung-Chung Shen , Kuang-Yeu Wu , Tsung-Min Chiu , Zong-Ying Chen , Tung-Hsiung Kuo , Yu-Ming Wu
发明人： Fu-Ming Lee , Tzong-Bin Lin , Jyh-Haur Hwang , Hung-Chung Shen , Kuang-Yeu Wu , Tsung-Min Chiu , Zong-Ying Chen , Tung-Hsiung Kuo , Yu-Ming Wu
IPC分类号： C07C7/00
CPC分类号： B01D3/40 , C10G7/08 , C10G2400/30
摘要： Extractive distillation processes whereby water-soluble extractive distillation (ED) solvents are regenerated and recovered employ improved operations of the extractive distillation column (EDC) so that polar hydrocarbons are recovered and purified from mixtures containing polar and less polar hydrocarbons and measurable amounts of hydrocarbons that are heavier than intended feedstock and/or polymers that are generated in the ED process. The improved process can effectively remove and recover the heavy hydrocarbons and/or remove polymer contaminants from the solvent in a closed solvent circulating loop through mild operating conditions with no additional process energy being expended. With the improved process, the overhead reflux of the EDC may be eliminated to further reduce energy consumption and to enhance the loading and performance within the upper portion of the EDC, especially when two liquid phases exists therein.
摘要翻译：萃取蒸馏方法，其中水溶性萃取蒸馏（ED）溶剂被再生和回收利用萃取蒸馏塔（EDC）的改进操作，使极性烃从含有极性和极性较小的烃的混合物中回收和纯化，比在ED过程中产生的预期原料和/或聚合物重。改进的方法可以在封闭的溶剂循环回路中通过温和的操作条件有效地除去和回收重质烃和/或从溶剂中除去聚合物污染物，而不需要额外的工艺能量消耗。通过改进的方法，可以消除EDC的顶部回流以进一步降低能量消耗并增强EDC上部的负载和性能，特别是当存在两个液相时。

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