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    • 3. 发明授权
    • Column packing material and method for producing the same
    • 柱填料及其制造方法
    • US07329386B2
    • 2008-02-12
    • US10398564
    • 2002-08-30
    • Atsushi KobayashiKazuko TakezawaHideki TakasakiTaketoshi KandaIsao TanakaTomoko KimuraYutaka Ohtsu
    • Atsushi KobayashiKazuko TakezawaHideki TakasakiTaketoshi KandaIsao TanakaTomoko KimuraYutaka Ohtsu
    • G01N30/56
    • B01J20/3227B01J20/286B01J20/3204B01J20/3217B01J20/3244B01J20/3272Y10T428/31612Y10T428/31663
    • The first subject of this invention is a column packing material comprising: a silica gel having a silanol group; a first chemical modification group which is bound to said silanol group; a silicone polymer for coating the surface of said silica gel; and, a trimethylsilyl group which is bound to the silanol group on said silicone polymer and/or the silanol group on said silica gel. The second subject of this invention is a method for producing a column packing material comprising the following steps (A) to (C): (A) a step for introducing a first chemical modification group into a silanol group on the surface of a silica gel by reacting the silica gel with a silane coupling agent having said first chemical modification group; (B) a step for forming a silicone polymer coating on the surface of said silica gel by polymerizing one or more silicone compounds on the surface of the silica gel after step (A); and, (C) a step for trimethylsilylating a silanol group on said silicone polymer and/or a silanol group on said silica gel using an end-capping agent after step (B).
    • 本发明的第一主题是柱填充材料,其包括:具有硅烷醇基团的硅胶; 与所述硅烷醇基团结合的第一化学修饰基团; 用于涂覆所述硅胶表面的硅氧烷聚合物; 和与所述硅氧烷聚合物上的硅烷醇基和/或所述硅胶上的硅烷醇基结合的三甲基甲硅烷基。 本发明的第二个课题是制备柱填充材料的方法,其包括以下步骤(A)至(C):(A)将第一化学修饰基团引入到硅胶表面的硅烷醇基中的步骤 使所述硅胶与具有所述第一化学修饰基团的硅烷偶联剂反应; (B)通过在步骤(A)之后在硅胶表面上聚合一种或多种硅氧烷化合物,在所述硅胶表面上形成硅氧烷聚合物涂层的步骤; 和(C)在步骤(B)之后使用封端剂在所述硅胶上的所述硅氧烷聚合物和/或硅烷醇基上硅烷醇化甲硅烷基化步骤。