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1. 发明申请

US20100187719A1 PROCESS AND APPARATUS FOR PRODUCTION OF COLORLESS TRANSPARENT RESIN FILM 有权
标题翻译：生产无色透明树脂薄膜的工艺和设备
公开(公告)号：US20100187719A1
公开(公告)日：2010-07-29
申请号：US12622932
申请日：2009-11-20
申请人： Jitsuo OISHI , Sotaro HIRAMATSU , Shuta KIHARA
发明人： Jitsuo OISHI , Sotaro HIRAMATSU , Shuta KIHARA
IPC分类号： B29C39/16 , B29C39/14
CPC分类号： B29C41/26 , B29C41/28 , B29K2079/08 , C08G73/1007 , C08G73/1042 , C08G73/1046 , C08G73/105 , C08G73/1075 , C08G73/1078 , C08J5/18 , C08J2379/08 , C08L79/08 , H05K1/0346 , H05K1/0393 , H05K3/007 , H05K3/227 , H05K2201/0108 , H05K2201/0154 , H05K2203/0156 , H05K2203/0759
摘要： A method for producing a colorless transparent resin film by a solution flow casting method containing: flow-casting an organic solvent solution of a polyamic acid or a polyimide on a support; and drying, the method containing at least the following step (1), step (2) and step (3) in this order, and an apparatus therefor: (1) a step of flow-casting an organic solvent solution of a polyamic acid or polyamide on a support, (2) a step of evaporating the organic solvent while blowing a gas having an oxygen content of from 0.001 to 15% by volume at a temperature of from 100 to 170° C. onto the flow-cast material, and releasing as a self-supporting film from the support, and (3) a step of performing the following step (3-1) and step (3-2) in this order: (3-1) a step of lowering a residual ratio of the organic solvent in the self-supporting film while blowing a gas having an oxygen content of 15% by volume or less at a temperature of from 100 to 250° C. onto the film by using at least one dryer of a type of blowing a heated gas, and (3-2) a step of lowering the residual ratio of the organic solvent in the self-supporting film while blowing a gas having an oxygen content of 5% by volume or less at a temperature of from 150 to 400° C. onto the film by using at least one dryer of a type of blowing a heated gas.
摘要翻译：一种通过溶液流延法生产无色透明树脂膜的方法，包括：在载体上流延浇注聚酰胺酸或聚酰亚胺的有机溶剂溶液; 和干燥，该方法至少依次包含步骤（1），步骤（2）和步骤（3）及其装置：（1）流延聚酰胺酸的有机溶剂溶液的步骤或载体上的聚酰胺，（2）在100〜170℃的温度下将氧含量为0.001〜15体积％的气体吹入流延材料的同时蒸发有机溶剂的步骤，并从支持体释放为自支撑膜，以及（3）按照以下顺序执行以下步骤（3-1）和步骤（3-2）的步骤：（3-1）降低残留物的步骤在100〜250℃的温度下，将氧含量为15体积％以下的气体吹送到薄膜上时，使用至少一种干燥机，将自支撑薄膜中的有机溶剂的比例吹送加热气体，（3-2）在吹入氧含量为5％的气体的同时降低自支撑膜中的有机溶剂的残留率的步骤，通过通过使用至少一种吹入加热气体的干燥器在150至400℃的温度下将体积或更小的量加到薄膜上。

2. 发明授权

US06884366B2 Process for producing oxygen absorbing polyamide resin composition and oxygen absorbing polyamide resin composition produced by the process 有权
标题翻译：通过该方法制备吸氧性聚酰胺树脂组合物和氧吸收性聚酰胺树脂组合物的制造方法
公开(公告)号：US06884366B2
公开(公告)日：2005-04-26
申请号：US10384733
申请日：2003-03-11
申请人： Ryoji Otaki , Sotaro Hiramatsu
发明人： Ryoji Otaki , Sotaro Hiramatsu
IPC分类号： B32B27/34 , C08G69/04 , C08G69/26 , C08G69/28 , C09K3/00 , C08K3/32
CPC分类号： C08G69/28 , B32B27/34 , C08G69/04 , C08G69/265
摘要： In the process for producing an oxygen absorbing polyamide resin composition of the present invention, a diamine component containing 70 mol % or higher of m-xylylenediamine is polycondensed with a dicarboxylic acid component containing 50 mol % or higher of adipic acid in the presence of a phosphorus compound. A compound or complex containing at least one metal selected from the group consisting of transition metals of Group VIII of the Periodic Table, manganese, copper and zinc is added to reaction system either prior to initiation of the polycondensation reaction or during the polycondensation reaction such that a ratio (P/M) of a concentration of phosphorus P (mmol/g) in the phosphorus compound contained in the polyamide resin composition to a concentration of the metal M (mmol/g) in the polyamide resin composition is 0.02 to 1.0.
摘要翻译：在本发明的吸氧性聚酰胺树脂组合物的制造方法中，含有70摩尔％以上的间苯二甲胺的二胺成分与含有50摩尔％以上的己二酸的二羧酸成分缩聚，磷化合物。在开始缩聚反应之前或在缩聚反应期间，或者在缩聚反应期间，或者在缩聚反应期间，在反应体系中加入选自元素周期表第Ⅷ族过渡金属，锰，铜和锌中的至少一种金属的化合物或络合物，聚酰胺树脂组合物中所含的磷化合物中磷的浓度P（mmol / g）与聚酰胺树脂组合物中的金属浓度M（mmol / g）的比例（P / M）为0.02〜1.0。

3. 发明授权

US08357322B2 Process and apparatus for production of colorless transparent resin film 有权
标题翻译：无色透明树脂薄膜的生产工艺及装置
公开(公告)号：US08357322B2
公开(公告)日：2013-01-22
申请号：US12622932
申请日：2009-11-20
申请人： Jitsuo Oishi , Sotaro Hiramatsu , Shuta Kihara
发明人： Jitsuo Oishi , Sotaro Hiramatsu , Shuta Kihara
IPC分类号： B29D7/00
CPC分类号： B29C41/26 , B29C41/28 , B29K2079/08 , C08G73/1007 , C08G73/1042 , C08G73/1046 , C08G73/105 , C08G73/1075 , C08G73/1078 , C08J5/18 , C08J2379/08 , C08L79/08 , H05K1/0346 , H05K1/0393 , H05K3/007 , H05K3/227 , H05K2201/0108 , H05K2201/0154 , H05K2203/0156 , H05K2203/0759
摘要： A method for producing a colorless transparent resin film by a solution flow casting method containing: flow-casting an organic solvent solution of a polyamic acid or a polyimide on a support; and drying, the method containing at least the following step (1), step (2) and step (3) in this order, and an apparatus therefor: (1) a step of flow-casting an organic solvent solution of a polyamic acid or polyamide on a support, (2) a step of evaporating the organic solvent while blowing a gas having an oxygen content of from 0.001 to 15% by volume at a temperature of from 100 to 170° C. onto the flow-cast material, and releasing as a self-supporting film from the support, and (3) a step of performing the following step (3-1) and step (3-2) in this order: (3-1) a step of lowering a residual ratio of the organic solvent in the self-supporting film while blowing a gas having an oxygen content of 15% by volume or less at a temperature of from 100 to 250° C. onto the film by using at least one dryer of a type of blowing a heated gas, and (3-2) a step of lowering the residual ratio of the organic solvent in the self-supporting film while blowing a gas having an oxygen content of 5% by volume or less at a temperature of from 150 to 400° C. onto the film by using at least one dryer of a type of blowing a heated gas.
摘要翻译：一种通过溶液流延法生产无色透明树脂膜的方法，包括：在载体上流延浇注聚酰胺酸或聚酰亚胺的有机溶剂溶液; 和干燥，该方法至少依次包含步骤（1），步骤（2）和步骤（3）及其装置：（1）流延聚酰胺酸的有机溶剂溶液的步骤或载体上的聚酰胺，（2）在100〜170℃的温度下将氧含量为0.001〜15体积％的气体吹入流延材料的同时蒸发有机溶剂的步骤，并从支持体释放为自支撑膜，以及（3）按照以下顺序执行以下步骤（3-1）和步骤（3-2）的步骤：（3-1）降低残留物的步骤在100〜250℃的温度下，将氧含量为15体积％以下的气体吹送到薄膜上时，使用至少一种干燥机，将自支撑薄膜中的有机溶剂的比例吹送加热气体，（3-2）在吹入氧含量为5％的气体的同时降低自支撑膜中的有机溶剂的残留率的步骤，通过通过使用至少一种吹入加热气体的干燥器在150至400℃的温度下将体积或更小的量加到薄膜上。

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