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1. 发明授权

US09077037B2 Electrode and electrolyte materials for batteries 有权
标题翻译：电池用电极和电解质材料
公开(公告)号：US09077037B2
公开(公告)日：2015-07-07
申请号：US13201238
申请日：2010-02-12
申请人： Shiou-Jyh Hwu , Gregory A. Becht
发明人： Shiou-Jyh Hwu , Gregory A. Becht
IPC分类号： H01M4/131 , H01M4/58 , H01M4/1391 , H01M10/052 , H01M10/0562
CPC分类号： H01M4/5825 , H01M4/131 , H01M4/1391 , H01M10/052 , H01M10/0562 , Y02E60/122
摘要： Disclosed are open-framework solids that possess superior ion-transport properties pertinent to the electrochemical performance of next-generation electrode materials for battery devices. Disclosed compounds including compositions and architectures relevant to electrical energy storage device applications have been developed through integrated solid-state and soft (solution) chemistry studies. The solids can adopt a general formula of AxMy(XO4)z, where A=mono- or divalent electropositive cations (e.g., Li+), M—trivalent transition metal cations (e.g., Fe3+, Mn3+), and X═Si, P, As, or V. Also disclosed are oxo analogs of these materials having the general formulae AaMbOc(PO4)d (a≧b), and more specifically, AnMnO3x(PO4)n-2x, where A=mono- or divalent electropositive cations (e.g., Li+), M is either Fe or Mn, and x is between 0 and n/2.
摘要翻译：公开了具有与用于电池装置的下一代电极材料的电化学性能相关的优异的离子传输性质的开放骨架固体。已经通过集成的固态和软（溶液）化学研究开发了包括与电能存储装置应用相关的组成和结构的公开化合物。固体可以采用AxMy（XO4）z的通式，其中A =单价或二价正电阳离子（如Li +），M-三价过渡金属阳离子（如Fe3 +，Mn3 +）和X = Si，P， As或V.也公开了具有通式AaMbOc（PO4）d（a≥b）的这些材料的氧代类似物，更具体地，AnMnO 3 x（PO 4）n-2x，其中A =单价或二价正电阳离子例如Li +），M是Fe或Mn，x在0和n / 2之间。

2. 发明申请

US20120082902A1 ELECTRODE AND ELECTROLYTE MATERIALS FOR BATTERIES 有权
标题翻译：电极电极和电解质材料
公开(公告)号：US20120082902A1
公开(公告)日：2012-04-05
申请号：US13201238
申请日：2010-02-12
申请人： Shiou-Jyh Hwu , Gregory A. Becht
发明人： Shiou-Jyh Hwu , Gregory A. Becht
IPC分类号： H01M10/0562 , C01B25/45 , H01B1/00
CPC分类号： H01M4/5825 , H01M4/131 , H01M4/1391 , H01M10/052 , H01M10/0562 , Y02E60/122
摘要： Disclosed are open-framework solids that possess superior ion-transport properties pertinent to the electrochemical performance of next-generation electrode materials for battery devices. Disclosed compounds including compositions and architectures relevant to electrical energy storage device applications have been developed through integrated solid-state and soft (solution) chemistry studies. The solids can adopt a general formula of AxMy(XO4)z, where A=mono- or divalent electropositive cations (e.g., Li+), M—trivalent transition metal cations (e.g., Fe3+, Mn3+), and X=Si, P, As, or V. Also disclosed are oxo analogs of these materials having the general formulae AaMbOc(PO4)d (a≧b), and more specifically, AnMnO3x(PO4)n−2x, where A=mono- or divalent electropositive cations (e.g., Li+), M is either Fe or Mn, and x is between 0 and n/2.
摘要翻译：公开了具有与用于电池装置的下一代电极材料的电化学性能相关的优异的离子传输性质的开放骨架固体。已经通过集成的固态和软（溶液）化学研究开发了包括与电能存储装置应用相关的组成和结构的公开化合物。固体可以采用AxMy（XO4）z的通式，其中A =单价或二价正电阳离子（如Li +），M-三价过渡金属阳离子（如Fe3 +，Mn3 +）和X = Si，P， As或V.也公开了具有通式AaMbOc（PO4）d（a≥b）的这些材料的氧代类似物，更具体地，AnMnO 3 x（PO 4）n-2x，其中A =单价或二价正电阳离子例如Li +），M是Fe或Mn，x在0和n / 2之间。

3. 发明申请

US20050008556A1 Salt-templated microporous solids 失效
公开(公告)号：US20050008556A1
公开(公告)日：2005-01-13
申请号：US10755872
申请日：2004-01-12
申请人： Shiou-Jyh Hwu , Qun Huang , Mutlu Ulutagay
发明人： Shiou-Jyh Hwu , Qun Huang , Mutlu Ulutagay
IPC分类号： B01J29/84 , C01B37/00 , C01B39/06 , C01B39/08 , C01B39/10 , C01B39/50 , C01B39/54 , C01B25/45 , B01J8/00 , B01J23/00 , B01J23/02 , B01J23/06 , B01J27/14 , C01G28/02
CPC分类号： C01B39/06 , B01J29/84 , C01B37/00 , C01B37/002 , C01B39/08 , C01B39/10 , C01B39/50 , C01B39/54
摘要： The present invention is directed to open-framework and microporous solids particularly well suited for use in catalysis and ion exchange. The microporous solids are constructed by using a salt template which can be readily removed without destroying the framework of the micropore. Various microporous solids can be formed having different geometric structures depending upon the templating salt used and the concentration. Examples of two compounds include Na2Cs[Mn3(P2O7)2]Cl(1) and K2.02Cs2.90[Cu3(P2O7)2]C12.92(2). Compound 1 crystallizes in the space group C2/c with a=21.210(8), b=5.272(2), c=13.924(2)Å, beta=119.04(2), and Z=4. Compound 2 crystallizes in the space group 14/mcm with a=b=18.001(3), c=13.530(4)Å, and Z=8. Both compounds have 3-D (Mn, Cu)-P-O frameworks. For 1, two MnO4, two MnO5 polyhedra and four PO4 tetrahedra form small tunnels where Cs+ and Cl− ions reside. For 2, CuO4 and P2O7 groups form two different tunnels, one is similar to that in 1 (ca. 5.3 Å in diameter) while the other formed by eight CuO4 polyhedra and eight PO4 tetrahedra has an approximate diameter of 12 Å.

4. 发明授权

US06719955B1 Salt-templated microporous solids 失效
标题翻译：盐模微孔固体
公开(公告)号：US06719955B1
公开(公告)日：2004-04-13
申请号：US09439522
申请日：1999-11-12
申请人： Shiou-Jyh Hwu , Qun Huang , Mutlu Ulutagay
发明人： Shiou-Jyh Hwu , Qun Huang , Mutlu Ulutagay
IPC分类号： C01B3900
CPC分类号： C01B39/06 , B01J29/84 , C01B37/00 , C01B37/002 , C01B39/08 , C01B39/10 , C01B39/50 , C01B39/54
摘要： The invention is directed to open-framework and microporous solids well suited for use in catalysis and ion exchange. The microporous solids are constructed by using a salt template which can be readily removed without destroying the framework of the micropore. Various microporous solids can be formed having different geometric structures depending upon the templating salt used and the concentration. Examples of two compounds include Na2Cs[Mn3(P2O7)2]Cl and K2.02Cs2.90[Cu3(P2O7)2]Cl2.92. Both compounds have 3-D (Mn,Cu)—P—O frameworks.
摘要翻译：本发明涉及非常适合用于催化和离子交换的开放框架和微孔固体。通过使用可以容易地除去的盐模板来构建微孔固体，而不会破坏微孔的骨架。根据所使用的模板盐和浓度，可以形成具有不同几何结构的各种微孔固体。两种化合物的实例包括Na2C [Mn3（P2O7）2] Cl和K2.02C2.90 [Cu3（P2O7）2] Cl2.92。两种化合物都具有3-D（Mn，Cu）-P-O骨架。

5. 发明授权

US07097772B2 Method of purifying a waste stream using a microporous composition 失效
标题翻译：使用微孔组合物纯化废物流的方法
公开(公告)号：US07097772B2
公开(公告)日：2006-08-29
申请号：US11084884
申请日：2005-03-21
申请人： Shiou-Jyh Hwu , Qun Huang , Mutlu Ulutagay
发明人： Shiou-Jyh Hwu , Qun Huang , Mutlu Ulutagay
IPC分类号： B01J49/00
CPC分类号： C01B39/06 , B01J29/84 , C01B37/00 , C01B37/002 , C01B39/08 , C01B39/10 , C01B39/50 , C01B39/54
摘要： The invention is directed to open-framework and microporous solids well suited for use in catalysis and ion exchange. The microporous solids are constructed by using a salt template which can be readily removed without destroying the framework of the micropore. Various microporous solids can be formed having different geometric structures depending upon the templating salt used and the concentration. Examples of two compounds include Na2Cs[Mn3(P2O7)2]Cl and K2.02Cs2.90[Cu3(P2O7)2]Cl2.92. Both compounds have 3-D (Mn, Cu)-P-O frameworks.
摘要翻译：本发明涉及非常适合用于催化和离子交换的开放框架和微孔固体。通过使用可以容易地除去的盐模板来构建微孔固体，而不会破坏微孔的骨架。根据所使用的模板盐和浓度，可以形成具有不同几何结构的各种微孔固体。两种化合物的实例包括Na 2 C 3 [Mn 3 N 2（N 2 O 7）2 C 1和K 2 O 2 C 2 O 2·C 2 O 2·C 3 N 2（P 2 N 2） / SUB>）2 2.92。两种化合物都具有3-D（Mn，Cu）-P-O骨架。

6. 发明申请

US20050180909A1 Salt-templated microporous solids 失效
标题翻译：盐模微孔固体
公开(公告)号：US20050180909A1
公开(公告)日：2005-08-18
申请号：US11084884
申请日：2005-03-21
申请人： Shiou-Jyh Hwu , Qun Huang , Mutlu Ulutagay
发明人： Shiou-Jyh Hwu , Qun Huang , Mutlu Ulutagay
IPC分类号： B01J29/84 , C01B37/00 , C01B39/06 , C01B39/08 , C01B39/10 , C01B39/50 , C01B39/54 , C01B25/45
CPC分类号： C01B39/06 , B01J29/84 , C01B37/00 , C01B37/002 , C01B39/08 , C01B39/10 , C01B39/50 , C01B39/54
摘要： The present invention is directed to open-framework and microporous solids particularly well suited for use in catalysis and ion exchange. The microporous solids are constructed by using a salt template which can be readily removed without destroying the framework of the micropore. Various microporous solids can be formed having different geometric structures depending upon the templating salt used and the concentration. Examples of two compounds include Na2Cs[Mn3(P2O7)2]Cl(1) and K2.02Cs2.90[Cu3(P2O7)2]C12.92(2). Compound 1 crystallizes in the space group C2/c with a=21.210(8), b=5.272(2), c=13.924(2)Å, beta=119.04(2), and Z=4. Compound 2 crystallizes in the space group 14/mcm with a=b=18.001(3), c=13.530(4)Å, and Z=8. Both compounds have 3-D (Mn, Cu)—P—O frameworks. For 1, two MnO4, two MnO5 polyhedra and four PO4 tetrahedra form small tunnels where Cs+ and Cl− ions reside. For 2, CuO4 and P2O7 groups form two different tunnels, one is similar to that in 1 (ca. 5.3 Å in diameter) while the other formed by eight CuO4 polyhedra and eight PO4 tetrahedra has an approximate diameter of 12 Å.
摘要翻译：本发明涉及特别适用于催化和离子交换的开放框架和微孔固体。通过使用可以容易地除去的盐模板来构建微孔固体，而不会破坏微孔的骨架。根据所使用的模板盐和浓度，可以形成具有不同几何结构的各种微孔固体。两种化合物的实例包括Na2C [Mn3（P2O7）2] Cl（1）和K2.02C2.90 [Cu3（P2O7）2] C12.92（2）。化合物1在空间群C2 / c中结晶，a = 21.210（8），b = 5.272（2），c = 13.924（2），β= 119.04（2），Z = 4。化合物2在空间群14 / mcm中结晶，a = b = 18.001（3），c = 13.530（4），Z = 8。两种化合物都具有3-D（Mn，Cu）-P-O骨架。对于1，两个MnO4，两个MnO5多面体和四个PO4四面体形成Cs +和Cl-离子存在的小隧道。对于2，CuO 4和P 2 O 7组形成两个不同的隧道，一个类似于1（直径约5.3），而由八个CuO 4多面体和八个PO 4四面体形成的另一个具有大约12的直径。

7. 发明授权

US06890500B2 Salt-templated microporous solids 失效
标题翻译：盐模微孔固体
公开(公告)号：US06890500B2
公开(公告)日：2005-05-10
申请号：US10755872
申请日：2004-01-12
申请人： Shiou-Jyh Hwu , Qun Huang , Mutlu Ulutagay
发明人： Shiou-Jyh Hwu , Qun Huang , Mutlu Ulutagay
IPC分类号： B01J29/84 , C01B37/00 , C01B39/06 , C01B39/08 , C01B39/10 , C01B39/50 , C01B39/54 , B01J8/00 , C01B21/00 , C01B39/00
CPC分类号： C01B39/06 , B01J29/84 , C01B37/00 , C01B37/002 , C01B39/08 , C01B39/10 , C01B39/50 , C01B39/54
摘要： The invention is directed to open-framework and microporous solids well suited for use in catalysis and ion exchange. The microporous solids are constructed by using a salt template which can be readily removed without destroying the framework of the micropore. Various microporous solids can be formed having different geometric structures depending upon the templating salt used and the concentration. Examples of two compounds include Na2Cs[Mn3(P2O7)2]Cl and K2.02Cs2.90[Cu3(P2O7)2]Cl2.92. Both compounds have 3-D (Mn, Cu)—P—O frameworks.
摘要翻译：本发明涉及非常适合用于催化和离子交换的开放框架和微孔固体。通过使用可以容易地除去的盐模板来构建微孔固体，而不会破坏微孔的骨架。根据所使用的模板盐和浓度，可以形成具有不同几何结构的各种微孔固体。两种化合物的实例包括Na 2 C 3 [Mn 3 N 2（N 2 O 7）2 C 1和K 2 O 2 C 2 O 2·C 2 O 2·C 3 N 2（P 2 N 2） / SUB>）2 2.92。两种化合物都具有3-D（Mn，Cu）-P-O骨架。

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