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    • 4. 发明授权
    • Process for increasing the exchange yield in ion exchange processes
    • 提高离子交换过程中交换产量的方法
    • US4198295A
    • 1980-04-15
    • US909943
    • 1978-05-26
    • Sandor Vajna
    • Sandor Vajna
    • B01J47/00B01J47/06B01D15/04
    • B01J47/06B01J47/00
    • A process for increasing the exchange yield in ion exchange processes is disclosed wherein at least one reaction fraction stored with the previous carrying out of the same exchange reaction, a solution of the exchanging ions supplied from outside and water are delivered to a washed ion exchanger bed which is filled with water and which is charged with the ions which are to be exchanged; and after the discharge from the bed of the water and of a solution obtained as product, the same number of reaction fractions with the same volume is collected and stored as the number as that previously supplied, in order to be delivered as previously with the next carrying out of the same exchange reaction in the identical manner and in the same sequence, and wherein displacement occurring in the direction of flow and relatively to one another of those liquid particles which are delivered simultaneously or in immediate succession to the bed is substantially prevented until the discharge from the container of the bed is reached, and the co-ion content of the reaction fraction or fractions is kept constant by keeping constant the volume of the reaction fraction or fractions, of the solution supplied from outside and of the liquids discharged from the system and of the co-ion content of the solution supplied from outside.
    • 公开了一种用于提高离子交换过程中的交换产率的方法,其中至少一个与先前进行相同交换反应的反应级分,从外部供应的交换离子的溶液和水的反应级分输送到洗涤的离子交换床 其中填充有水,并且被带有待交换的离子; 在从床的水和作为产物得到的溶液排出之后,收集和存储相同数量的具有相同体积的反应级分,并按照之前提供的数量存储,以便如前所述用下一个 以相同的方式和相同的顺序进行相同的交换反应,并且其中基本上防止在同时或立即连续送入床的那些液体颗粒的流动方向和彼此相对彼此发生的位移直到 达到从床的容器排出,并保持反应级分或馏分的共离子含量保持恒定,保持从外部供应的溶液的反应级分或馏分的体积和从 该系统和从外部提供的溶液的共离子含量。
    • 5. 发明授权
    • Ion exchange process with counter-current fractional regeneration
    • 离子交换过程与逆流分数再生
    • US4108766A
    • 1978-08-22
    • US818035
    • 1977-07-22
    • Sandor Vajna
    • Sandor Vajna
    • B01J47/00B01J49/00B01D15/06C02B1/76
    • B01J49/00B01J47/00
    • In an ion exchange process wherein an ion exchange bed is successively charged and discharged during an exchange cycle with an ion, here designated as "X" ion, with "Y" being used to designate the replacing ion and "Z" the oppositely charged ion associated with X and Y, by passing aqueous solutions of the ions through the bed, with the flow thereof during charging being in one direction and during discharging in the opposite direction; the improvement with respect to the discharge portion of the cycle starting with the bed charged with X ions and filled with water substantially free of X, Y and Z ions, comprising passing at least four groups of fractions through said bed, as follows:1) a first feed group of fractions, containing X, Y and Z ions, the concentration of Z ions remaining substantially constant, the concentration of X ions successively decreasing downwardly to or near to zero and the concentration of Y ions correspondingly increasing.2) a second feed group of fractions containing Y and Z ions at the concentration of Z ion substantially equal to the concentration of said ions in the previous group and free of X ions, being introduced as feed to the process.3) a third feed group of fractions containing Y and Z ions, the concentration of which successively decrease to or near to zero, and4) a fourth feed group of fractions consisting essentially of pure water free of X, Y and Z ions;And recovering from the bed at least 3 effluent groups of fractions, as follows:A) a first effluent group of fractions which may contain the displaced water content of the bed and contains a solution containing predominantly X ions and minor amounts of Y ions, both associated with Z ions, which group is at least in part removed from the process as product,B) a second effluent group of fractions, identical to the first feed group, andC) a third effluent group of fractions, identical to the third feed group,And collecting the second and third effluent groups and using the same in a subsequent discharge portion of a cycle.The charging portion of the cycle may be improved in the same way.
    • 在离子交换过程中,离子交换床在与离子交换循环期间被连续充电和放电,这里称为“X”离子,“Y”用于表示取代离子,“Z”是相反电荷的离子 通过使离子的水溶液通过床而与X和Y相关联,其中在充电过程中的流动在一个方向上并且在相反方向上排放期间; 相对于以充满X离子填充有基本上不含X,Y和Z离子的水为原料的床开始的循环排出部分的改进,包括使至少四组馏分通过所述床,如下: