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1. 发明申请

US20090306444A1 OLIGOMERIZING AND ALKYLATING WITH AN IONIC LIQUID AT A MOLAR RATIO OF OLEFIN TO ISOPARAFFIN OF AT LEAST 0.8 有权
标题翻译：将低聚烯醇与烯丙醇的摩尔比低于至少0.8的异黄酮
公开(公告)号：US20090306444A1
公开(公告)日：2009-12-10
申请号：US12481407
申请日：2009-06-09
申请人： Saleh Elomari , Russell R. Krug
发明人： Saleh Elomari , Russell R. Krug
IPC分类号： C07C2/04
CPC分类号： C10M127/02 , C10G2300/1081 , C10G2300/1088 , C10G2400/10 , C10M105/04 , C10M109/02 , C10M177/00 , C10M2205/0285 , C10N2220/022 , C10N2220/023 , C10N2230/02 , C10N2270/00 , C10M2203/0206
摘要： We provide a process for making a fuel or lubricant component, comprising: performing alkylation and oligomerization by contacting a stream comprising one or more olefins and one or more isoparaffins, wherein a molar ratio of the one or more olefins to the one or more isoparaffins in the stream is at least 0.8, an acidic chloroaluminate ionic liquid catalyst, and a halohalide; and recovering the fuel or lubricant component having a Bromine Number of less than 4. We provide a process comprising performing concurrent alkylation and oligomerization. We also provide a process for making a lubricant component having a kinematic viscosity at 100° C. of at least 6.9 mm2/s, a VI of at least 134, a cloud point less than or equal to −28° C., and a Bromine Number of less than or equal to 6.1.
摘要翻译：我们提供制备燃料或润滑剂组分的方法，包括：通过使包含一种或多种烯烃和一种或多种异链烷烃的物流接触进行烷基化和低聚，其中所述一种或多种烯烃与一种或多种异构烷烃的摩尔比在该物流至少为0.8，一种酸性氯铝酸盐离子液体催化剂和一种卤代卤化物; 并回收溴值小于4的燃料或润滑剂组分。我们提供一种包括进行同时烷基化和低聚反应的方法。我们还提供一种制备润滑剂组分的方法，该组分在100℃下的运动粘度为至少6.9mm 2 / s，VI至少为134，浊点小于或等于-28℃，溴数小于或等于6.1。

2. 发明申请

US20090120838A1 PRODUCTION OF HIGH QUALITY LUBRICANT BRIGHT STOCK 有权
标题翻译：生产高品质润滑剂亮度库存
公开(公告)号：US20090120838A1
公开(公告)日：2009-05-14
申请号：US12191716
申请日：2008-08-14
申请人： Stephen J. Miller , Russell R. Krug
发明人： Stephen J. Miller , Russell R. Krug
IPC分类号： C10G69/02
CPC分类号： C10G65/12 , C10M101/02 , C10M2203/1085 , C10N2230/02 , C10N2230/10
摘要： A process for producing a lubricant bright stock from a very heavy feed obtained from a petroleum crude is disclosed. The bright stock produced by the present process has a reduced cloud point and better oxidation stability relative to bright stocks prepared by conventional methods. The process comprises the steps of providing a petroleum residuum-derived stream; separating the residuum-derived stream at a distillation cut point in the range of 1150° F. to 1300° F., into a heavy fraction and at least one light fraction; hydrocracking the at least one light fraction under conditions to reduce the concentration of sulfur and nitrogen to suitable levels for hydroisomerization dewaxing; and dewaxing at least a portion of the hydrocracked stream under hydroisomerization conditions to produce a lubricant bright stock.
摘要翻译：公开了从由石油原油获得的非常重的原料生产润滑剂光亮原料的方法。本方法生产的光亮料相对于通过常规方法制备的光亮油墨具有降低的浊点和更好的氧化稳定性。该方法包括以下步骤：提供来自石油残渣的流; 将在1150°F至1300°F范围内的蒸馏切割点的残渣衍生物流分离成重馏分和至少一种轻馏分; 在将硫和氮的浓度降低到加氢异构化脱蜡的合适水平的条件下加氢裂化至少一种轻馏分; 并在加氢异构化条件下将至少一部分加氢裂化物流脱蜡以产生润滑剂光亮原料。

3. 发明授权

US07195706B2 Finished lubricating comprising lubricating base oil with high monocycloparaffins and low multicycloparaffins 有权
标题翻译：成品润滑剂包括润滑基础油与高单环烷烃和低多环烷烃
公开(公告)号：US07195706B2
公开(公告)日：2007-03-27
申请号：US10743932
申请日：2003-12-23
申请人： Susan M. Abernathy , David C. Kramer , John M. Rosenbaum , Stephen J. Miller , Russell R. Krug , James N. Ziemer , Robert J. Farina , Mark L. Sztenderowicz
发明人： Susan M. Abernathy , David C. Kramer , John M. Rosenbaum , Stephen J. Miller , Russell R. Krug , James N. Ziemer , Robert J. Farina , Mark L. Sztenderowicz
IPC分类号： C10G73/38 , C10G71/00 , C10M101/00
CPC分类号： C10M177/00 , C10G2400/10 , C10M169/04 , C10M2205/173 , C10N2220/02 , C10N2230/02 , C10N2230/06 , C10N2230/36 , C10N2230/40 , C10N2240/04 , C10N2240/042 , C10N2240/10 , C10N2270/00 , Y10S208/95
摘要： A process for manufacturing a finished lubricant by: a) performing Fischer-Tropsch synthesis on syngas to provide a product stream; b) isolating from said product stream a substantially paraffinic wax feed having less than about 30 ppm total nitrogen and sulfur, and less than about 1 wt % oxygen; c) dewaxing said feed by hydroisomerization dewaxing using a shape selective intermediate pore size molecular sieve comprising a noble metal hydrogenation component, wherein the hydroisomerization temperature is between about 600° F. (315° C.) and about 750° F. (399° C.), to produce an isomerized oil; and d) hydrofinishing said isomerized oil, whereby a lubricating base oil is produced having specific desired properties; and e) blending the lubricating base oil with at least one lubricant additive.
摘要翻译：一种通过以下步骤制造成品润滑剂的方法：a）在合成气上进行费 - 托合成以提供产物流; b）从所述产物流中分离具有小于约30ppm总氮和硫以及小于约1重量％氧的基本上石蜡的蜡进料; c）使用包含贵金属氢化组分的形状选择性中孔分子筛通过加氢异构化脱蜡来脱蜡所述进料，其中加氢异构化温度在约600°F（315℃）至约750°F（399° C.），以产生异构化油; 和d）加氢精制所述异构化油，从而制得具有特定所需性能的润滑基础油; 和e）将润滑基础油与至少一种润滑剂添加剂混合。

4. 发明授权

US06949180B2 Low toxicity Fischer-Tropsch derived fuel and process for making same 失效
标题翻译：低毒费托衍生燃料及其制备方法
公开(公告)号：US06949180B2
公开(公告)日：2005-09-27
申请号：US10625011
申请日：2003-07-22
申请人： Russell R. Krug , Stephen J. Miller , Russell D. White , David R. Johnson , Christopher A. Simmons , James Arthur Rutherford
发明人： Russell R. Krug , Stephen J. Miller , Russell D. White , David R. Johnson , Christopher A. Simmons , James Arthur Rutherford
IPC分类号： C07C1/04 , C08G20060101 , C10G47/00 , C10L1/00 , C10L1/04 , C10L1/08
CPC分类号： C10L1/08 , Y10S208/95
摘要： A method for preparing low toxicity Fischer-Tropsch fuels suitable for use in a diesel engine and Fischer-Tropsch derived fuel compositions having low toxicity suitable for use in diesel engines characterized by a boiling range distribution wherein the 5 weight percent point is at a temperature of 570 degrees F. or less and the 95 weight percent point is at or above a temperature of 680 degrees F.; a kinematic viscosity at 40 degrees C. of less than 5.5 cSt; and a cloud point of less than −18 degrees C.
摘要翻译：一种制备适用于柴油发动机的低毒费 - 托燃料的方法和适用于特点为沸程分布的柴油发动机的低毒性的费 - 托衍生燃料组合物，其中5重量％点处于 570华氏度以下，95重量％以上的温度为或高于680华氏度。 40℃下的运动粘度小于5.5cSt; 浊点小于-18摄氏度

5. 发明授权

US06841711B2 Process for making a lube base stock from a lower molecular weight feedstock in a catalytic distillation unit 失效
标题翻译：在催化蒸馏装置中由低分子量原料制备润滑油基料的方法
公开(公告)号：US06841711B2
公开(公告)日：2005-01-11
申请号：US09758667
申请日：2001-01-11
申请人： Russell R. Krug , Dennis J. O'Rear
发明人： Russell R. Krug , Dennis J. O'Rear
IPC分类号： C10G50/02 , C10G57/02 , C10M107/10 , C10M177/00 , C07C2/08
CPC分类号： C10M177/00 , C10G50/02 , C10G57/02 , C10M107/10 , C10N2270/00 , Y10S208/95
摘要： A process for making a lube base stock wherein an olefinic feedstock is contacted with an oligomerization catalyst in a catalytic distillation unit to produce a product having a higher number average molecular weight than the olefinic feedstock. That product is separated zone in the catalytic distillation unit into a light byproduct fraction and a heavy product fraction that includes hydrocarbons in a lube base stock range.
摘要翻译：一种制备润滑油基料的方法，其中烯烃原料与催化蒸馏单元中的低聚催化剂接触以产生具有比烯烃原料更高数均分子量的产物。该产物在催化蒸馏单元中分离成轻质副产物馏分和在润滑油基料范围内包括烃的重质产物馏分。

6. 发明授权

US06562230B1 Synthesis of narrow lube cuts from Fischer-Tropsch products 失效
标题翻译：从费 - 托产品合成窄润滑油
公开(公告)号：US06562230B1
公开(公告)日：2003-05-13
申请号：US09469574
申请日：1999-12-22
申请人： Dennis O'Rear , Russell R. Krug
发明人： Dennis O'Rear , Russell R. Krug
IPC分类号： C10G6902
CPC分类号： C10G2/30
摘要： A process for preparing hydrocarbons in the lube base oil range, lube base oils and lube oil compositions from a fraction with an average molecular weight above a target molecular weight and a fraction with an average molecular weight below a target molecular weight via molecular averaging is described. The fractions can be obtained, for example, from Fischer-Tropsch reactions, and/or obtained from the distillation of crude oil. Molecular averaging converts the fractions to a product with a desired molecular weight, for use in preparing a lube oil composition. The product can optionally be isomerized to lower the pour point, and also can be blended with suitable additives for use as a lube oil composition.
摘要翻译：描述了在润滑油基础油范围内制备烃的方法，润滑油基础油和润滑油组合物由平均分子量高于目标分子量的馏分和通过分子平均的平均分子量低于目标分子量的级分描述。馏分可以例如从费 - 托反应获得，和/或从蒸馏原油获得。分子平均法将馏分转化成具有所需分子量的产物，用于制备润滑油组合物。该产物可以任选地被异构化以降低倾点，并且还可以与合适的添加剂共混以用作润滑油组合物。

7. 发明授权

US4721603A Separation of reacted hydrocarbons and catalyst in fluidized catalytic cracking 失效
标题翻译：反应的烃和催化剂在流化催化裂化中的分离
公开(公告)号：US4721603A
公开(公告)日：1988-01-26
申请号：US689956
申请日：1985-01-09
申请人： Russell R. Krug , Peter C. Schmidt
发明人： Russell R. Krug , Peter C. Schmidt
IPC分类号： B01J8/00 , C10G11/18 , B01J8/18
CPC分类号： B01J8/005 , C10G11/18
摘要： A specific baffle arrangement within a catalytic reactor improves separation of gaseous hydrocarbon reaction products from catalyst within the reactor vessel of a fluidized catalytic cracker unit. The catalytic reactor vessel includes an outer generally cylindrical shell having a stripping zone arranged at the lower end of the vessel. An inlet riser conduit forming a primary reaction zone extends generally within the shell from the lower end of the vessel to a location near the top of the vessel. A shroud surrounds the upper end of the riser conduit and forms an annular outlet for downwardly discharging a mixtrue of hydrocarbon and catalyst. An annular catalyst disengaging riser baffle for deflecting the mixture from the outlet toward the wall of the vessel is arranged on the outside of the riser conduit below the annular outlet and above the stripping zone. Still further, an annular catalyst disengaging wall baffle is arranged on the inside of the shell for again deflecting the mixture, now mostly catalyst, generally downwardly and toward the stripping zone of the vessel. Preferably, the riser baffle and the wall baffle are arrnaged within the shell such that the baffles in concert with the annular discharge outlet form a partial cyclone separating zone between the baffles to thereby improve the separation of hydrocarbon vapors from the catalyst. This cyclone action promotes early disengagement of hydrocarbon vapor from the catalyst and reduces undesirable catalyst carryover in the vapor to conventional cyclones through which the hydrocarbon products are recovered. At the same time, undesirable secondary cracking reactions in the dilute phase are minimized by lowering the concentration of spent catalyst in the dilute phase.
摘要翻译：催化反应器内的特定的挡板装置改善气态烃反应产物与流化催化裂化装置的反应器容器内的催化剂的分离。催化反应器容器包括外部大致圆柱形的外壳，其具有布置在容器下端的剥离区。形成初级反应区的入口提升管通常在壳体内从容器的下端延伸到靠近容器顶部的位置。护罩围绕提升管道的上端并形成用于向下排出烃和催化剂混合物的环形出口。将环形催化剂脱离提升管挡板用于将混合物从出口朝向容器的壁偏转设置在提升管道的外部，在环形出口下方和汽提区域之上。此外，环形催化剂分离壁挡板布置在壳体的内部，用于再次使混合物（现在主要是催化剂）大体向下并且朝向容器的汽提区域偏转。优选地，提升板挡板和壁挡板在壳体内被布置，使得与环形排出口一致的挡板在挡板之间形成部分旋风分离区，从而改进烃蒸气与催化剂的分离。这种旋风作用促进了烃蒸气从催化剂的早期脱离，并减少了蒸气中不期望的催化剂在常规旋流器中的滞留，通过这些旋风分离器回收烃产物。同时，通过降低稀释相中废催化剂的浓度，使稀相中不期望的二次裂化反应最小化。

8. 发明授权

US4500423A Separation of reacted hydrocarbons and catalyst in fluidized catalytic cracking 失效
标题翻译：反应的烃和催化剂在流化催化裂化中的分离
公开(公告)号：US4500423A
公开(公告)日：1985-02-19
申请号：US503781
申请日：1983-06-13
申请人： Russell R. Krug , Peter C. Schmidt
发明人： Russell R. Krug , Peter C. Schmidt
IPC分类号： B01J8/00 , C10G11/18
CPC分类号： C10G11/18 , B01J8/005
摘要： The present invention relates to a baffle arrangement that improves separation of gaseous hydrocarbon reaction products from catalyst within the reactor vessel of a fluidized catalytic cracker unit. The catalytic reactor vessel includes an outer generally cylindrical shell having a stripping zone arranged at the lower end of the vessel. An inlet riser conduit forming a primary reaction zone extends generally within the shell from the lower end of the vessel to a location near the top of the vessel. A shroud surrounds the upper end of the riser conduit and forms an annular outlet for downwardly discharging a mixture of hydrocarbon and catalyst. According to the present invention, an annular catalyst disengaging riser baffle for deflecting the mixture from the outlet toward the wall of the vessel is arranged on the outside of the riser conduit below the annular outlet and above the stripping zone. Still further, in the preferred embodiment an annular catalyst disengaging wall baffle is arranged on the inside of the shell for again deflecting the mixture, now mostly catalyst, generally downwardly and toward the stripping zone of the vessel. Preferably, the riser baffle and the wall baffle are arranged within the shell such that the baffles in concert with the annular discharge outlet form a partial cyclone separating zone. This cyclone action promotes early disengagement of hydrocarbon vapor from the catalyst and reduces undesirable catalyst carryover in the vapor to conventional cyclones through which the hydrocarbon products are recovered.
摘要翻译：本发明涉及一种改进气态烃反应产物与流化催化裂化装置的反应容器内的催化剂分离的挡板装置。催化反应器容器包括外部大致圆柱形的外壳，其具有布置在容器下端的剥离区。形成初级反应区的入口提升管通常在壳体内从容器的下端延伸到靠近容器顶部的位置。护罩围绕提升管道的上端并形成用于向下排出烃和催化剂混合物的环形出口。根据本发明，在环形出口下方和汽提区上方的提升管道的外侧设置有用于将混合物从出口向容器的壁偏转的环形催化剂分离提升管挡板。此外，在优选实施例中，环形催化剂分离壁挡板布置在壳体的内部，用于再次使混合物（现在主要是催化剂）大体向下并且朝向容器的汽提区域偏转。优选地，提升板挡板和壁挡板布置在壳体内，使得与环形排出口一致的挡板形成部分旋风分离区。这种旋风作用促进了烃蒸气从催化剂的早期脱离，并减少了蒸气中不期望的催化剂在常规旋流器中的滞留，通过这些旋风分离器回收烃产物。

9. 发明授权

US08115040B2 Composition of a superior lubricant or lubricant blendstock 有权
标题翻译：优异的润滑剂或润滑剂共混物的组成
公开(公告)号：US08115040B2
公开(公告)日：2012-02-14
申请号：US12261388
申请日：2008-10-30
申请人： Saleh Elomari , Russell R. Krug
发明人： Saleh Elomari , Russell R. Krug
IPC分类号： C10M171/02 , C10M171/04
CPC分类号： C10M109/02 , C07C2527/125 , C07C2531/02 , C10G2300/1081 , C10G2300/1088 , C10G2300/301 , C10G2300/302 , C10G2300/304 , C10G2400/10 , C10M105/04 , C10M127/02 , C10M177/00 , C10M2205/0285 , C10N2220/022 , C10N2220/023 , C10N2230/02 , C10N2270/00 , C10M2203/0206
摘要： A composition of a superior lubricant or lubricant component having a very high VI, a low cloud point, a difference between the T90 and T10 boiling points of at least 250° F. by SIMDIST, and a very low Bromine Number.
摘要翻译：具有非常高的VI，低浊点，SIMDIST的T90和T10沸点至少250°F之间的差异以及非常低的溴值的优异润滑剂或润滑剂组分的组合物。

10. 发明授权

US07973205B2 Process to make a lubricant component by oligomerizing and alkylating at a molar ratio of olefin to isoparaffin of at least 0.8 有权
标题翻译：通过烯烃与异链烷烃的摩尔比低聚和烷基化制备润滑剂组分的方法至少为0.8
公开(公告)号：US07973205B2
公开(公告)日：2011-07-05
申请号：US12763866
申请日：2010-04-20
申请人： Saleh Elomari , Russell R. Krug
发明人： Saleh Elomari , Russell R. Krug
IPC分类号： C07C2/52 , C07C2/08
CPC分类号： C10M127/02 , C10G2300/1081 , C10G2300/1088 , C10G2400/10 , C10M105/04 , C10M109/02 , C10M177/00 , C10M2205/0285 , C10N2220/022 , C10N2220/023 , C10N2230/02 , C10N2270/00 , C10M2203/0206
摘要： We provide a process to make a lubricant component, comprising: a. oligomerizing a feed comprising one or more olefins in an ionic liquid oligomerization zone, at oligomerization conditions, to form an oligomer; and b. alkylating the oligomer in the presence of an isoparaffin, in an ionic liquid alkylation zone, at alkylation conditions including a molar ratio of one or more olefins and one or more isoparaffins of at least 0.8, to form an alkylated oligomeric product that is a lubricant component having a kinematic viscosity at 100° C. of at least 6.9 mm2/s, a VI of at least 134, a cloud point less than or equal to −28° C., and a Bromine Number of less than or equal to 6.1.
摘要翻译：我们提供一种制备润滑剂组分的方法，包括：a。在低聚条件下使包含一种或多种烯烃的进料在离子液体低聚区域低聚，形成低聚物; 和b。在异烷烃存在下，在离子液体烷基化区，烷基化条件下烷基化低聚物，包括一种或多种烯烃和一种或多种异链烷烃的摩尔比为至少0.8，形成作为润滑剂组分的烷基化低聚产物在100℃下的运动粘度为至少6.9mm 2 / s，VI至少为134，浊点小于或等于-28℃，溴值小于或等于6.1。

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