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1. 发明授权

US5141652A Water treatment process 失效
标题翻译：水处理工艺
公开(公告)号：US5141652A
公开(公告)日：1992-08-25
申请号：US714211
申请日：1991-06-12
申请人： Robert M. Moore, Jr. , Clarinda M. Whitton , Lawrence H. Shepherd, Jr.
发明人： Robert M. Moore, Jr. , Clarinda M. Whitton , Lawrence H. Shepherd, Jr.
IPC分类号： A01N59/00 , C01B7/01 , C01B11/20 , C02F1/50 , C02F1/76
CPC分类号： C02F1/766 , A01N59/00 , C01B11/20 , C01B7/01 , C02F1/50 , C02F1/76 , C02F2103/023
摘要： This invention relates to a process for reducing the biological activity in water by feeding a solution of BrCl stabilized by a hydrohalic acid or an aqueous halide salt into the water to be treated in an amount sufficient to effect the reduction of biological activity in the water thus treated.
摘要翻译：本发明涉及一种降低水中生物活性的方法，该方法通过将由氢卤酸或卤化水盐稳定的BrCl溶液以足以使水中生物活性降低的量加入待处理水中治疗。

2. 发明授权

US08048435B2 Preparation of concentrated aqueous bromine solutions and biocidal applications thereof 有权
标题翻译：浓缩溴水溶液的制备及其杀菌应用
公开(公告)号：US08048435B2
公开(公告)日：2011-11-01
申请号：US12480021
申请日：2009-06-08
申请人： Robert M. Moore, Jr. , Christopher J. Nalepa
发明人： Robert M. Moore, Jr. , Christopher J. Nalepa
IPC分类号： A01N25/00 , A01N37/00 , A01N41/06 , A61K33/04
CPC分类号： C02F1/766 , A01N59/00 , C02F2303/04 , G09F3/10 , A01N59/02 , A01N25/22 , A01N2300/00
摘要： A process of producing a concentrated liquid biocide formulation is described. Mixed together are (a) bromine and (b) an aqueous solution of alkali metal salt of sulfamic acid having a pH of at least about 12, in amounts such that (i) the active bromine content of the solution is at least about 100,000 ppm (wt/wt), and (ii) the atom ratio of nitrogen to active bromine from (a) and (b) is greater than 1. A continuous process for producing the concentrated liquid biocide composition is provided. This process comprises continuously feeding into mixing apparatus (i) bromine and (ii) an aqueous solution of alkali metal salt of sulfamic acid; the desired product is withdrawn from the mixing apparatus at a rate sufficient to enable the continuous feeding to be maintained. Also described are methods for disinfecting surfaces and for sanitizing bodies of water using a single-feed, bromine-based biocide. These methods use concentrated liquid biocide compositions comprising biocidally active bromine as the biocide.
摘要翻译：描述了生产浓缩液体杀生物剂制剂的方法。混合在一起是（a）溴和（b）具有至少约12的pH的氨基磺酸的碱金属盐的水溶液，其量使得（i）溶液的活性溴含量为至少约100,000ppm （重量/重量），和（ii）（a）和（b）的氮与活性溴的原子比大于1.提供了制备浓缩液体杀生物剂组合物的连续方法。该方法包括连续输入混合装置（ⅰ）溴和（ⅱ）氨基磺酸的碱金属盐水溶液; 以足以使得能够维持连续进料的速率从混合装置中取出所需的产品。还描述了使用单进料溴基杀生物剂消毒表面和消毒水体的方法。这些方法使用包含杀生物活性溴的浓缩液体杀生物剂组合物作为杀生物剂。

3. 发明授权

US06869620B2 Production of concentrated biocidal solutions 有权
标题翻译：生产浓缩杀生物溶液
公开(公告)号：US06869620B2
公开(公告)日：2005-03-22
申请号：US10370333
申请日：2003-02-18
申请人： Robert M. Moore, Jr.
发明人： Robert M. Moore, Jr.
IPC分类号： A01N25/02 , A01N59/08 , C01B7/24 , C01B11/20 , A01N59/02 , A01N59/00
CPC分类号： C01B11/20 , A01N59/08 , C01B7/24 , A01N59/02 , A01N59/00 , A01N25/22 , A01N2300/00
摘要： The production process comprises A) forming an acidic aqueous solution comprising alkali metal cations, bromide anions, and sulfamate anions; B) feeding into said aqueous solution a source of alkali metal cations and chlorine-containing bromide oxidant proportioned to keep the resultant aqueous medium acidic and to form an acidic product solution containing at least about 5 wt % of active bromine, and C) raising the pH of the aqueous product solution with water-soluble base to at least about 10.
摘要翻译：制备方法包括：A）形成包含碱金属阳离子，溴离子和氨基磺酸根阴离子的酸性水溶液; B）向所述水溶液中加入成比例的碱金属阳离子和含氯溴化物氧化物源，以使所得水性介质保持酸性并形成含有至少约5重量％活性溴的酸性产物溶液，和C）将具有水溶性碱的水溶液的pH至少为约10。

4. 发明授权

US06511682B1 Concentrated aqueous bromine solutions and their preparation 有权
标题翻译：浓缩溴水溶液及其制备
公开(公告)号：US06511682B1
公开(公告)日：2003-01-28
申请号：US09506911
申请日：2000-02-18
申请人： Robert M. Moore, Jr. , Christopher J. Nalepa
发明人： Robert M. Moore, Jr. , Christopher J. Nalepa
IPC分类号： A01N3900
CPC分类号： C02F1/766 , A01N59/00 , C02F2303/04 , A01N2300/00
摘要： Described is a process of producing a concentrated liquid biocide formulation. Mixed together are (a) bromine chloride or bromine and (b) an aqueous solution of alkali metal salt of sulfamic acid having a pH of at least about 7, in amounts such that (i) the active bromine content of the solution is at least about 100,000 ppm (wt/wt), and (ii) the atom ratio of nitrogen to active bromine from (a) and (b) is greater than 1 when bromine is used and is greater than 0.93 when bromine chloride is used. Use of bromine chloride as the source of the active bromine in the process is preferred because in the resulting aqueous compositions, all of the bromine of the bromine chloride is made available as active bromine in solution. In other words, the chlorine of the bromine chloride is converted in the process to dissolved alkali metal chloride salt, thereby liberating all of the bromine in the biocidal composition as active bromine capable of providing biocidal activity.
摘要翻译：描述了生产浓缩液体杀生物剂制剂的方法。混合在一起是（a）溴化氯或溴，和（b）具有至少约7的pH的氨基磺酸的碱金属盐的水溶液，其量使得（i）溶液的活性溴含量至少为大约100,000ppm（wt / wt），和（ii）当使用溴时，（a）和（b）的氮与活性溴的原子比大于1，并且当使用溴氯化物时大于0.93。在该方法中使用溴氯化物作为活性溴的来源是优选的，因为在所得含水组合物中溴溴化物的溴全部作为活性溴在溶液中得到。换句话说，溴化氯的氯在该过程中转化为溶解的碱金属氯化物盐，从而释放杀生物组合物中的全部溴作为能够提供杀生物活性的活性溴。

5. 发明授权

US5000879A Melting point enhancement of partially brominated diphenyl oxide mixtures 失效
标题翻译：部分溴化二苯醚混合物的熔点增强
公开(公告)号：US5000879A
公开(公告)日：1991-03-19
申请号：US387776
申请日：1989-08-01
申请人： Robert M. Moore, Jr. , David R. Brackenridge
发明人： Robert M. Moore, Jr. , David R. Brackenridge
IPC分类号： C07C41/36 , C07C43/29
CPC分类号： C07C41/36
摘要： This invention relates to a process for increasing the melting point of partially brominated diphenyl oxide mixtures having an average bromine content of 7.2 to 7.7. The process comprises: forming a slurry comprised of C.sub.1 -C.sub.4 alkanol and the mixture; maintaining the slurry until the melting point increase which is sought is obtained; and separating the so-treated mixture from the slurry.
摘要翻译：本发明涉及一种提高平均溴含量为7.2至7.7的部分溴化二苯醚混合物的熔点的方法。该方法包括：形成由C1-C4链烷醇和混合物组成的浆料; 保持浆料直到获得所需的熔点增加; 并将如此处理的混合物与浆料分离。

6. 发明授权

US08409630B2 Continuous processes for preparing concentrated aqueous liquid biocidal compositions 有权
标题翻译：用于制备浓缩的含水液体杀生物剂组合物的连续方法
公开(公告)号：US08409630B2
公开(公告)日：2013-04-02
申请号：US09785890
申请日：2001-02-16
申请人： Robert M. Moore, Jr. , Christopher J. Nalepa
发明人： Robert M. Moore, Jr. , Christopher J. Nalepa
IPC分类号： A01N59/02 , A61K31/185
CPC分类号： C02F1/766 , A01N59/00 , C02F2303/04 , G09F3/10 , A01N59/02 , A01N25/22 , A01N2300/00
摘要： The process involves (a) continuously forming bromine chloride from separate feed streams of bromine and chlorine by maintaining said streams under automatic feed rate control whereby the streams are continuously proportioned to come together in equimolar amounts to form bromine chloride; (b) continuously forming an aqueous product having an active bromine content of at least 100,000 ppm (wt/wt), a pH of at least 7, and an atom ratio of nitrogen to active bromine greater than 0.93:1 by continuously feeding into mixing apparatus separate feed streams of (1) bromine chloride formed in (a), and (2) an aqueous solution of alkali metal salt of sulfamic acid, under automatic feed rate control whereby the feed streams are continuously proportioned to come together in amounts that produce an aqueous product having an active bromine content of at least 100,000 ppm (wt/wt), a pH of at least 7, and an atom ratio of nitrogen to active bromine from (1) and (2) greater than 0.93:1; and, (c) withdrawing said aqueous product from said mixing apparatus at a rate sufficient to enable the continuous feeding in (a) and (b) to be maintained.
摘要翻译：该方法包括（a）通过在自动进料速率控制下将所述物流保持在连续成比例的范围内，以等摩尔量混合形成溴氯化物，从溴和氯的不同进料流中连续形成溴氯化物; （b）连续地形成活性溴含量为至少100,000ppm（wt / wt），pH至少为7，氮与活性溴的原子比大于0.93:1的含水产物，在（a）中形成的（1）溴化氯和（2）氨基磺酸的碱金属盐的水溶液的分离的进料流，在进料速率控制下，使进料流连续成比例，以产生的量活性溴含量至少为100,000ppm（wt / wt），pH至少为7，氮与活性溴的原子比（1）和（2）大于0.93:1的含水产物; 和（c）以足以使（a）和（b）中的连续进料保持的速率从所述混合装置中取出所述含水产物。

7. 发明申请

US20110262873A1 USE OF COMPOUNDS CONTAINING HALOGEN AND NITROGEN FOR REDUCING MERCURY EMISSIONS DURING COAL COMBUSTION 审中-公开
标题翻译：使用含有卤素和氮气的化合物，用于在煤炭燃烧期间减少汞排放
公开(公告)号：US20110262873A1
公开(公告)日：2011-10-27
申请号：US12667282
申请日：2007-07-03
申请人： Christopher J. Nalepa , Robert M. Moore, JR. , Jennifer Moore
发明人： Christopher J. Nalepa , Robert M. Moore, JR. , Jennifer Moore
IPC分类号： F23B90/00 , C10L5/00 , B01D53/64
CPC分类号： C10L10/02 , B01D53/64 , B01D2257/602 , C10L9/10 , F23J7/00 , F23K1/00
摘要： Processes and systems are provided for using bromine and/or bromide-containing compounds derived from a nitrogen-containing compound, such as ammonia, sulfamic acid, or one or more salts thereof, to reduce mercury emissions during coal combustion.
摘要翻译：提供了使用衍生自含氮化合物如氨，氨基磺酸或其一种或多种盐的溴和/或溴化物的化合物的方法和系统，以减少煤燃烧期间的汞排放。

8. 发明申请

US20090246295A1 PREPARATION OF CONCENTRATED AQUEOUS BROMINE SOLUTIONS AND BIOCIDAL APPLICATIONS THEREOF 有权
标题翻译：浓缩水杨酸溶液的制备及其生物应用
公开(公告)号：US20090246295A1
公开(公告)日：2009-10-01
申请号：US12480021
申请日：2009-06-08
申请人： Robert M. Moore, JR. , Christopher J. Nalepa
发明人： Robert M. Moore, JR. , Christopher J. Nalepa
IPC分类号： A01N59/02 , A01P1/00
CPC分类号： C02F1/766 , A01N59/00 , C02F2303/04 , G09F3/10 , A01N59/02 , A01N25/22 , A01N2300/00
摘要： A process of producing a concentrated liquid biocide formulation is described. Mixed together are (a) bromine and (b) an aqueous solution of alkali metal salt of sulfamic acid having a pH of at least about 12, in amounts such that (i) the active bromine content of the solution is at least about 100,000 ppm (wt/wt), and (ii) the atom ratio of nitrogen to active bromine from (a) and (b) is greater than 1. A continuous process for producing the concentrated liquid biocide composition is provided. This process comprises continuously feeding into mixing apparatus (i) bromine and (ii) an aqueous solution of alkali metal salt of sulfamic acid; the desired product is withdrawn from the mixing apparatus at a rate sufficient to enable the continuous feeding to be maintained. Also described are methods for disinfecting surfaces and for sanitizing bodies of water using a single-feed, bromine-based biocide. These methods use concentrated liquid biocide compositions comprising biocidally active bromine as the biocide.
摘要翻译：描述了生产浓缩液体杀生物剂制剂的方法。混合在一起是（a）溴和（b）具有至少约12的pH的氨基磺酸的碱金属盐的水溶液，其量使得（i）溶液的活性溴含量为至少约100,000ppm （重量/重量），和（ii）（a）和（b）的氮与活性溴的原子比大于1.提供了制备浓缩液体杀生物剂组合物的连续方法。该方法包括连续输入混合装置（ⅰ）溴和（ⅱ）氨基磺酸的碱金属盐水溶液; 以足以使得能够维持连续进料的速率从混合装置中取出所需的产品。还描述了使用单进料溴基杀生物剂消毒表面和消毒水体的方法。这些方法使用包含杀生物活性溴的浓缩液体杀生物剂组合物作为杀生物剂。

9. 发明授权

US06652889B2 Concentrated aqueous bromine solutions and their preparation and use 有权
公开(公告)号：US06652889B2
公开(公告)日：2003-11-25
申请号：US09974622
申请日：2001-10-09
申请人： Robert M. Moore, Jr. , Christopher J. Nalepa
发明人： Robert M. Moore, Jr. , Christopher J. Nalepa
IPC分类号： A01N3900
CPC分类号： A01N59/00 , C02F1/766 , C02F2303/04 , A01N2300/00
摘要： Described is a process of producing a concentrated liquid biocide formulation. Mixed together are (a) bromine chloride or bromine and (b) an aqueous solution of alkali metal salt of sulfamic acid having a pH of at least about 7, in amounts such that (i) the active bromine content of the solution is at least about 100,000 ppm (wt/wt), and (ii) the atom ratio of nitrogen to active bromine from (a) and (b) is greater than 1 when bromine is used and is greater than 0.93 when bromine chloride is used. Use of bromine chloride as the source of the active bromine in the process is preferred because in the resulting aqueous compositions, all of the bromine of the bromine chloride is made available as active bromine in solution. In other words, the chlorine of the bromine chloride is converted in the process to dissolved alkali metal chloride salt, thereby liberating all of the bromine in the biocidal composition as active bromine capable of providing biocidal activity.

10. 发明授权

US06551624B2 Production of concentrated biocidal solutions 有权
公开(公告)号：US06551624B2
公开(公告)日：2003-04-22
申请号：US10120334
申请日：2002-04-10
申请人： Robert M. Moore, Jr.
发明人： Robert M. Moore, Jr.
IPC分类号： A01N5902
CPC分类号： C01B11/20 , A01N59/08 , C01B7/24 , A01N59/02 , A01N59/00 , A01N25/22 , A01N2300/00
摘要： The production process comprises A) forming an acidic aqueous solution comprising alkali metal cations, bromide anions, and sulfamate anions; B) feeding into said aqueous solution a source of alkali metal cations and chlorine-containing bromide oxidant proportioned to keep the resultant aqueous medium acidic and to form an acidic product solution containing at least about 5 wt % of active bromine; and C) raising the pH of the aqueous product solution with water-soluble base to at least about 10.

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