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1. 发明授权

US4294620A Phthalocyanine formulations 失效
标题翻译：酞菁配方
公开(公告)号：US4294620A
公开(公告)日：1981-10-13
申请号：US116582
申请日：1980-01-29
申请人： Reinhard Sappok , Joachim Kranz
发明人： Reinhard Sappok , Joachim Kranz
IPC分类号： C09B67/00 , C09B67/20 , C09D11/037 , C09B47/08
CPC分类号： C09D11/037 , C09B67/0001 , C09B67/0032
摘要： Phthalocyanine formulations which comprise a mixture of (a) phthalocyanine and (b) from 2 to 20% by weight, based on (a) of one or more urea derivatives of the formula K-(-NHCO-NH-R).sub.2 (I), where K is 1,5-naphthylene or 4,4'-diphenylenemethane, R is alkyl of 12 to 18 carbon atoms, alkenyl of 12 to 18 carbon atoms, 3-(alkoxy of 8 to 18 carbon atoms)-propyl, 2-(alkylamino of 8 to 18 carbon atoms)-ethyl or (CH.sub.2).sub.3 --O--(CH.sub.2 --CH.sub.2 O).sub.n --R.sup.1, R.sup.1 is alkyl of 2 to 8 carbon atoms or phenyl and n is 1, 2, 3 or 4, and which are obtained by milling (a) with (b) in the absence of a grinding medium.When used in printing inks, such as offset printing inks, the formulations give deeply colored prints in very pure hues, with very low graininess of the ink.
摘要翻译：包含（a）酞菁和（b）2-20重量％的（a）一种或多种式K - （ - NHCO-NH-R）2（I）的脲衍生物的混合物的酞菁制剂），其中K为1,5-亚萘基或4,4'-二苯基甲烷，R为12至18个碳原子的烷基，12至18个碳原子的烯基，3-（8至18个碳原子的烷氧基） - 丙基， 2-（8-18个碳原子的烷基氨基） - 乙基或（CH2）3-O-（CH2-CH2O）n-R1，R1是2-8个碳原子的烷基或苯基，n是1,2,3或如图4所示，并且在不存在研磨介质的情况下通过研磨（a）与（b）获得。当用于印刷油墨（如胶版印刷油墨）时，配方以非常纯净的色调给出深色的印刷品，油墨的颗粒度非常低。

2. 发明授权

US4255203A Pigment formulations 失效
标题翻译：颜料配方
公开(公告)号：US4255203A
公开(公告)日：1981-03-10
申请号：US116384
申请日：1980-01-29
申请人： Joachim Kranz , Reinhard Sappok
发明人： Joachim Kranz , Reinhard Sappok
IPC分类号： C09B67/00 , C09B67/20 , C09B67/46 , C09D11/03 , C09C3/02
CPC分类号： C09D11/03 , C09B67/0032 , C09B67/006 , C09B67/0065 , C09B67/0089
摘要： A pigment formulation which comprises (a) a finely divided organic pigment and (b) one or more urea derivatives of the formula K--(NH--CO--NH--R).sub.2, where R is C.sub.12 -C.sub.18 -alkyl, C.sub.12 -C.sub.18 -alkenyl, C.sub.8 -C.sub.18 -alkoxypropyl or --(CH.sub.2).sub.3 --O--(C.sub.2 H.sub.4 O).sub.n --R.sup.1, R.sup.1 is C.sub.2 -C.sub.8 -alkyl or phenyl, n is 1, 2, 3 or 4 and K is 1,5-naphthylene or 4,4'-diphenylenemethane, with or without (c) up to 5% by weight, based on (a and b), of agents conventionally present in pigment formulations.In binder solutions, the pigment formulations give printing inks and paints possessing excellent tinctorial properties.Some of the compounds (b) prevent the conversion of .alpha.-copper phthalocyanine to the .beta.-modification.
摘要翻译：一种颜料制剂，其包含（a）细碎的有机颜料和（b）一种或多种式K-（NH-CO-NH-R）2的脲衍生物，其中R是C 12 -C 18烷基，C 12 -C 18 - 烯基，C 8 -C 18烷氧基丙基或 - （CH 2）3 -O-（C 2 H 4 O）n -R 1，R 1是C 2 -C 8 - 烷基或苯基，n是1,2,3或4，K是1,5- 亚苯基或4,4'-二苯基甲烷，具有或不具有（c）基于（a和b）至多5重量％的常规存在于颜料制剂中的试剂。在粘合剂溶液中，颜料配方给出具有优异着色性能的印刷油墨和油漆。一些化合物（b）防止α-酞菁转变为β-修饰。

3. 发明授权

US4256507A Pigment formulations 失效
标题翻译：颜料配方
公开(公告)号：US4256507A
公开(公告)日：1981-03-17
申请号：US116382
申请日：1980-01-29
申请人： Joachim Kranz , Rudolf Polster , Reinhard Sappok , Alois Wiesenberger
发明人： Joachim Kranz , Rudolf Polster , Reinhard Sappok , Alois Wiesenberger
IPC分类号： C09B69/00 , C09B67/22 , C09B67/00
CPC分类号： C09B67/0036 , C09B67/0034
摘要： Formulations of flavanthrone, pyranthrone, indanthrone, indigo, quinacridone, perylene-3,4,9,10-tetracarboxylic acid dianhydride and perylene-3,4,9,10-tetracarboxylic acid diimide pigments which contain, as additives, one or more compounds of the formula ##STR1## where X is an n-valent radical of a flavanthrone, pyranthrone, indigo, quinacridone, perylene-3,4,9,10-tetracarboxylic acid dianhydride or perylene-3,4,9,10-tetracarboxylic acid diimide pigment, R.sup.1, R.sup.3 and R.sup.4 are hydrogen or chlorine, R.sup.2 is hydrogen, chlorine, carboxyl, bromine, nitro, N-C.sub.1 -C.sub.5 -alkylcarbamyl, N-phenylcarbamyl or benzoylamino and n is 1, 2, 3 or 4.In solutions of surface-coating binders or of surface coatings, the above formulations give very deep colorations, coupled with high gloss and high transparency of the resulting films.
摘要翻译：黄烷酮，吡喃酮，阴丹酮，靛蓝，喹吖啶酮，苝-3,4,9,10-四羧酸二酐和苝-3,4,9,10-四羧酸二酰亚胺颜料的制剂，其包含作为添加剂的一种或多种化合物式（I）其中X是黄烷酮，吡喃酮，靛蓝，喹吖啶酮，苝-3,4,9,10-四羧酸二酐或苝-3,4,9,10的n价基团 - 四羧酸二酰亚胺颜料，R1，R3和R4是氢或氯，R2是氢，氯，羧基，溴，硝基，N-C1-C5-烷基氨基甲酰基，N-苯基氨基甲酰基或苯甲酰基氨基，n是1,2,3或在表面涂层粘合剂或表面涂层的溶液中，上述配方产生非常深的着色，加上所得膜的高光泽度和高透明度。

4. 发明授权

US4069064A Phthalocyanine formulations having high gloss, which are stabilized against recrystallization and against change of modification 失效
标题翻译：具有高光泽度的酞菁制剂，其对于重结晶和改变改变是稳定的
公开(公告)号：US4069064A
公开(公告)日：1978-01-17
申请号：US669842
申请日：1976-03-24
申请人： Robert Nett , Wolf Dieter Fechner , Werner Jettmar , Rudolf Polster , Reinhard Sappok , Eduard Hartmann
发明人： Robert Nett , Wolf Dieter Fechner , Werner Jettmar , Rudolf Polster , Reinhard Sappok , Eduard Hartmann
IPC分类号： C09B47/08 , C09B67/00 , C09B67/22 , C09B47/04
CPC分类号： C09B68/441 , C09B47/08 , C09B67/0032 , C09B67/0035
摘要： A phthalocyanine formulation which is stabilized against recrystallization and change of modification and which contains, as the stabilizer (a) a finely divided phthalocyanine as the pigment and (b) a salt or the corresponding homogeneous mixture of (.alpha.) a phthalocyanine derivative, which carries basic groups ##STR1## (R.sup.1 = H, alkyl of 1 to 20 carbon atoms, unsubstituted or substituted phenyl, --C.sub.2 H.sub.4 --NH).sub.z H or --(C.sub.3 H.sub.6 --NH).sub.z H, z = 1, 2 or 3, and R.sup.2 = H, alkyl of 1 to 6 carbon atoms or cycloalkyl of 6 to 8 carbon atoms) and (.beta.) an aliphatic sulfonic acid of 8 to 20 carbon atoms, a monoalkylbenzenesulfonic acid or dialkylbenzenesulfonic acid where alkyl is of 6 to 20 carbon atoms, or a monoalkylnaphthalenesulfonic acid or dialkylnaphthalenesulfonic acid where alkyl is of 6 to 20 carbon atoms, which acids may be substituted by hydroxyl, the molar ratio of .alpha.:.beta. being from 1:1 to 1:5, and, if desired, one or more organic fluids or solutions of resins in these fluids. The formulations are stable even in aromatic hydrocarbons and produce pure, deep colorations which have high gloss.
摘要翻译：一种稳定的重结晶和改性改性的酞菁配方，其中含有作为稳定剂（a）细分的酞菁作为颜料，和（b）（α）酞菁衍生物的盐或相应的均匀混合物，其携带（R1 = H，1〜20个碳原子的烷基，未取代或取代的苯基，-C2H4-NH）zH或 - （C3H6-NH）zH，z = 1,2或3，R2 = H 1-6个碳原子的烷基或6至8个碳原子的环烷基）和（β）8-20个碳原子的脂族磺酸，一烷基苯磺酸或二烷基苯磺酸，其中烷基为6至20个碳原子，或单烷基萘磺酸或二烷基萘磺酸，其中烷基具有6至20个碳原子，哪些酸可以被羟基取代，α：β的摩尔比为1:1至1:5，如果需要，一种或多种有机流体或这些液体中的树脂溶液。即使在芳香烃中，配方也是稳定的，并产生具有高光泽度的纯色深色。

5. 发明授权

US4298526A Preparation of easily dispersible and deeply colored pigmentary forms 失效
标题翻译：制备容易分散和深色的颜料形式
公开(公告)号：US4298526A
公开(公告)日：1981-11-03
申请号：US94984
申请日：1979-11-16
申请人： Reinhard Sappok , Fritz Guellich , Karl Roth , Alois Wiesenberger
发明人： Reinhard Sappok , Fritz Guellich , Karl Roth , Alois Wiesenberger
IPC分类号： C09B67/04 , C09B67/10 , C09B67/14 , C09B67/20 , C09B47/04
CPC分类号： C09B67/0017 , C09B67/0014
摘要： A process for the preparation of pigmentary forms of phthalocyanine and of insoluble polycyclic compounds, wherein the crude pigment is milled in the presence of one or more acids which have a pK of
摘要翻译：制备颜料形式的酞菁和不溶性多环化合物的方法，其中将粗颜料在一种或多种pK为4.9的酸存在下研磨，并且在研磨条件下不氧化，直至初级颗粒大小为0.1μm，然后在存在或不存在水的情况下，以常规方式在溶剂中完成研磨的材料，并分离颜料。颜料产生非常深的着色，并且非常容易地分散在使用它们的介质中。

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