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1. 发明授权

US08784991B2 Process for coating metallic surfaces with an aqueous composition, and this composition 有权
标题翻译：用水性组合物涂覆金属表面的方法，以及该组合物
公开(公告)号：US08784991B2
公开(公告)日：2014-07-22
申请号：US13080940
申请日：2011-04-06
申请人： Thomas Kolberg , Manfred Walter , Peter Schubach
发明人： Thomas Kolberg , Manfred Walter , Peter Schubach
IPC分类号： B05D3/10 , C08K3/16 , C08L63/00
CPC分类号： C23C26/00 , B05D3/007 , B05D3/0413 , B05D7/52 , C09D1/00 , C09D5/08 , C23C18/122 , C23C18/1241 , C23C18/14 , C23C22/34 , C23C22/364 , C23C22/365 , C23C22/367 , C23C22/368 , C23C2222/20 , Y02T50/67 , Y10T428/273 , Y10T428/31529 , Y10T428/31663
摘要： A composition and a method for coating metallic surfaces with a silane/silanol/siloxane/polysiloxane-containing composition, whereby the composition contains a) at least one compound selected from the silanes, silanols, siloxanes and polysiloxanes, b) at least two compounds selected from titanium-, hafnium-, zirconium-, aluminum- or boron-containing compounds, optionally c) at least one type of cation selected from cations of metals of the 1st to 3rd and 5th to 8th sub-groups including the lanthanides and the 2nd main group of the periodic table of the elements or at least one corresponding compound, d) at least one organic compound selected from monomers, oligomers, polymers, copolymers and block copolymers or e) at least one substance affecting the pH value, water and optionally at least one organic solvent.
摘要翻译：一种用硅烷/硅烷醇/硅氧烷/聚硅氧烷的组合物涂覆金属表面的组合物和方法，其中组合物含有a）至少一种选自硅烷，硅烷醇，硅氧烷和聚硅氧烷的化合物，b）选择至少两种化合物从钛，铪，锆，铝或硼的化合物任选地，c）至少一种选自第1至第3和第5至第8族金属的阳离子的阳离子，包括镧系元素和第2族元素周期表的主要组分或至少一种相应的化合物，d）至少一种选自单体，低聚物，聚合物，共聚物和嵌段共聚物的有机化合物，或e）至少一种影响pH值的物质，水和任选地至少一种有机溶剂。

2. 发明申请

US20110189488A1 PROCESS FOR COATING METALLIC SURFACES WITH AN AQUEOUS COMPOSITION, AND THIS COMPOSITION 有权
标题翻译：用金属组合物涂覆金属表面的方法，以及该组合物
公开(公告)号：US20110189488A1
公开(公告)日：2011-08-04
申请号：US13080940
申请日：2011-04-06
申请人： Thomas Kolberg , Manfred Walter , Peter Schubach
发明人： Thomas Kolberg , Manfred Walter , Peter Schubach
IPC分类号： B32B15/08 , B05D3/10 , C08K3/16 , C08L63/00
CPC分类号： C23C26/00 , B05D3/007 , B05D3/0413 , B05D7/52 , C09D1/00 , C09D5/08 , C23C18/122 , C23C18/1241 , C23C18/14 , C23C22/34 , C23C22/364 , C23C22/365 , C23C22/367 , C23C22/368 , C23C2222/20 , Y02T50/67 , Y10T428/273 , Y10T428/31529 , Y10T428/31663
摘要： A compositon and a method for coating metallic surfaces with a silane/silanol/siloxane/polysiloxane-containing composition, whereby the composition contains a) at least one compound selected from the silanes, silanols, siloxanes and polysiloxanes, b) at least two compounds selected from titanium-, hafnium-, zirconium-, aluminum- or boron-containing compounds, optionally c) at least one type of cation selected from cations of metals of the 1st to 3rd and 5th to 8th sub-groups including the lanthanides and the 2nd main group of the periodic table of the elements or at least one corresponding compound, d) at least one organic compound selected from monomers, oligomers, polymers, copolymers and block copolymers or e) at least one substance affecting the pH value, water and optionally at least one organic solvent.
摘要翻译：一种用硅烷/硅烷醇/硅氧烷/聚硅氧烷的组合物涂覆金属表面的组合物和方法，其中组合物含有a）至少一种选自硅烷，硅烷醇，硅氧烷和聚硅氧烷的化合物，b）选择至少两种化合物从钛，铪，锆，铝或硼的化合物任选地，c）至少一种选自第1至第3和第5至第8族金属的阳离子的阳离子，包括镧系元素和第2族元素周期表的主要组分或至少一种相应的化合物，d）至少一种选自单体，低聚物，聚合物，共聚物和嵌段共聚物的有机化合物，或e）至少一种影响pH值的物质，水和任选地至少一种有机溶剂。

3. 发明申请

US20080127859A1 Method for Coating Metallic Surfaces with an Aqueous Multi-Component Composition 审中-公开
标题翻译：用多金属组合物涂覆金属表面的方法
公开(公告)号：US20080127859A1
公开(公告)日：2008-06-05
申请号：US11667879
申请日：2005-11-09
申请人： Thomas Kolberg , Manfred Walter , Peter Schubach
发明人： Thomas Kolberg , Manfred Walter , Peter Schubach
IPC分类号： C09D5/08 , B05D3/06 , B05D3/02
摘要： The invention relates to a process for coating metallic surfaces with a composition containing silane/silanol/siloxane/polysiloxane, wherein, in addition to a) at least one compound selected from silanes, silanols, siloxanes and polysiloxanes, b) at least one compound containing titanium, hafnium, zirconium, aluminium and/or boron, and c) at least one type of cation selected from cations of metals of subgroups 1 to 3 and 5 to 8, including lanthanides, and of main group 2 of the periodic table of the elements, and/or at least one corresponding compound, the composition contains at least one substance d) selected from: d1) silicon-free compounds having at least one amino, urea and/or ureido group in each case, d2) anions of nitrite and/or compounds having at least one nitro group, d3) compounds based on peroxide, and d4) phosphorus-containing compounds, anions of at least one phosphate and/or anions of at least one phosphonate, as well as e) water, and f) optionally also at least one organic solvent. The invention further relates to corresponding aqueous compositions.
摘要翻译：本发明涉及一种用含有硅烷/硅烷醇/硅氧烷/聚硅氧烷的组合物涂覆金属表面的方法，其中除了a）至少一种选自硅烷，硅烷醇，硅氧烷和聚硅氧烷的化合物之外，b）至少一种含钛，铪，锆，铝和/或硼，以及c）至少一种阳离子，其选自亚族1至3和5至8族的金属的阳离子，包括镧系元素，以及元素周期表的主族2的阳离子元素和/或至少一种相应的化合物，所述组合物含有至少一种选自以下的物质：d 1）具有至少一个氨基，脲和/或脲基的无硅化合物在每种情况下，基于过氧化物的亚硝酸盐和/或具有至少一个硝基的化合物，d 3 N 3）化合物，d 4，含磷化合物，至少一种磷酸盐的阴离子和/或至少一种膦酸盐的阴离子，以及e）wa 和f）任选地还有至少一种有机溶剂。本发明还涉及相应的含水组合物。

4. 发明授权

US11142655B2 Process for coating metallic surfaces with a multicomponent aqueous composition 有权
公开(公告)号：US11142655B2
公开(公告)日：2021-10-12
申请号：US13006970
申请日：2011-01-14
申请人： Thomas Kolberg , Manfred Walter , Peter Schubach
发明人： Thomas Kolberg , Manfred Walter , Peter Schubach
IPC分类号： C23C22/48 , C09D5/08 , C09D7/61 , C08K3/10 , C08K5/00
摘要： The invention relates to a process for coating metallic surfaces with a composition containing silane/silanol/siloxane/polysiloxane, wherein, in addition to a) at least one compound selected from silanes, silanols, siloxanes and polysiloxanes, b) at least one compound containing titanium, hafnium, zirconium, aluminium and/or boron, and c) at least one type of cation selected from cations of metals of subgroups 1 to 3 and 5 to 8, including lanthanides, and of main group 2 of the periodic table of the elements, and/or at least one corresponding compound, the composition contains at least one substance d) selected from: d1) silicon-free compounds having at least one amino, urea and/or ureido group in each case, d2) anions of nitrite and/or compounds having at least one nitro group, d3) compounds based on peroxide, and d4) phosphorus-containing compounds, anions of at least one phosphate and/or anions of at least one phosphonate, as well as e) water, and f) optionally also at least one organic solvent. The invention further relates to corresponding aqueous compositions.

5. 发明申请

US20110180186A1 METHOD AND SOLUTION FOR COATING METALLIC SURFACES WITH A PHOSPHATING SOLUTION CONTAINING HYDROGEN PEROXIDE, METALLIC OBJECT PRODUCED AND USE OF THE OBJECT 审中-公开
标题翻译：用含有过氧化氢的金属溶液涂覆金属表面的方法和解决方案，制造金属物体和使用物体
公开(公告)号：US20110180186A1
公开(公告)日：2011-07-28
申请号：US13081823
申请日：2011-04-07
申请人： Thomas Nitschke , Rudiger Rein , Eckart Schönfelder , Peter Schubach , Jürgen Specht
发明人： Thomas Nitschke , Rudiger Rein , Eckart Schönfelder , Peter Schubach , Jürgen Specht
IPC分类号： C23C22/07 , B32B15/04
CPC分类号： C23C22/364 , C23C22/16 , C23C22/182 , C23C22/184 , C23C22/365 , C23C22/73 , Y02T50/67
摘要： A method for the treatment or pre-treatment of surfaces of metal objects by means of an acidic, aqueous solution containing zinc and phosphate. The phosphating solution contains between 0.1-10 g/L, zinc, 4-50 g/L phosphate calculated as PO4, between 0.03-3 g/L, of at least one guanidine compound comprising at least one nitro group calculated as nitroguanidine, and between 0.001-0.9 g/L hydrogen peroxide and has a temperature of less than 80° C. The corresponding acidic, aqueous composition and finished products are also disclosed.
摘要翻译：一种通过含锌和磷酸盐的酸性水溶液处理或预处理金属物体表面的方法。磷酸盐溶液含有0.1-10g / L，以PO4计算的锌，4-50g / L磷酸盐，0.03-3g / L之间的至少一种包含至少一个以硝基胍计算的硝基的胍化合物，以及在0.001-0.9g / L过氧化氢之间并具有小于80℃的温度。还公开了相应的酸性水性组合物和成品。

6. 发明申请

US20060278307A1 Method and solution for coating metal surfaces with a posphating solution containing water peroxide, produced metal object and use of said object 审中-公开
标题翻译：用含有过氧化氢，产生的金属物体和所述物体的使用的喷射溶液涂覆金属表面的方法和解决方案
公开(公告)号：US20060278307A1
公开(公告)日：2006-12-14
申请号：US10555929
申请日：2004-05-17
申请人： Thomas Nitschke , Rudiger Rein , Eckart Schonfeler , Peter Schubach , Jurgen Specht
发明人： Thomas Nitschke , Rudiger Rein , Eckart Schonfeler , Peter Schubach , Jurgen Specht
IPC分类号： C23C22/07 , C23C22/34
CPC分类号： C23C22/364 , C23C22/16 , C23C22/182 , C23C22/184 , C23C22/365 , C23C22/73 , Y02T50/67
摘要： The invention relates to a method for the treatment or pre-treatment of surfaces of metal objects by means of an acidic, aqueous solution containing zinc and phosphate. Said invention is characterised in that the phosphating solution contains between 0.1-10 g/L zinc, 4-50 g/L phosphate calculated as PO4, between 0.03-3 g/L of at least one guanidine compound comprising at least one nitro group calculated as nitroguanidine, and between 0.001-0.9 g/L hydrogen peroxide and has a temperature of less than 80° C. The invention also relates to a corresponding acidic, aqueous composition.
摘要翻译：本发明涉及一种通过含锌和磷酸盐的酸性水溶液处理或预处理金属物体表面的方法。本发明的特征在于磷酸盐溶液含有0.1-10g / L锌，4-50g / L磷酸盐，按PO 4计算，0.03-3g / L的至少一种胍包含至少一个以硝基胍计算的硝基的化合物和0.001-0.9g / L的过氧化氢并且具有小于80℃的温度。本发明还涉及相应的酸性水性组合物。

7. 发明授权

US5294266A Process for a passivating postrinsing of conversion layers 失效
标题翻译：转化层的钝化方法
公开(公告)号：US5294266A
公开(公告)日：1994-03-15
申请号：US978193
申请日：1992-11-18
申请人： Dieter Hauffe , Thomas Kolberg , Gerhard Muller , Horst Gehmecker , Werner Rausch , Peter Schubach , Thomas Wendel
发明人： Dieter Hauffe , Thomas Kolberg , Gerhard Muller , Horst Gehmecker , Werner Rausch , Peter Schubach , Thomas Wendel
IPC分类号： C23C22/34 , C23C22/36 , C23C22/60 , C23C22/83
CPC分类号： C23C22/73 , C23C22/34 , C23C22/361 , C23C22/60 , C23C22/83
摘要： The invention is in a composition and process for the chromium free passivating postrinsing of conversion layers on metals before the application of a paint or adhesive. The conversion layers can be on the bases of phosphate layers, at least two polyvalent metal ions with complex formers, titanium, zirconium and/or hafnium. The postrinsing agent is an aqueous solution which has been adjusted to a pH value of up to 5 and which contains an aluminum fluorozirconate having an Al:Zr:F mole ratio of (0.15 to 8.0):1:(5 to 52), and in which solutions the total concentration of Al+Zr+F is 0.1 to 8.0 g/l. The postrinsing solutions may additionally contain at least one of the anions benzoate, caprylate, ethyl hexoate, salicylate in a total concentration of 0.05 to 0.5 g/1 and may preferably be adjusted to the required pH value with cations of volatile bases, such as ammonium, ethanolammonium and di- and triethanolammonium. The paint is subsequently applied suitably by cathodic electrocoating or powder coating or from a low-solvent high-solids paint.The rinsing treatment is over a period of 1 to 120 seconds at temperatures of 20.degree. to 80.degree. C. The invention is used as a pretreatment to the application of a paint coating, film coating or adhesive coating.
摘要翻译：本发明是用于在施加涂料或粘合剂之前的金属上的转化层的无铬钝化的组合物和方法。转化层可以在磷酸盐层，至少两种具有复合成型剂的多价金属离子，钛，锆和/或铪的基础上。 postrinsing剂是一种水溶液，其pH值调至5以下，并含有Al：Zr：F摩尔比为（0.15〜8.0）：1：（5〜52）的氟锆酸铝，其中Al + Zr + F的总浓度为0.1〜8.0g / l。 postrinsing溶液还可以含有至少一种阴离子苯甲酸酯，辛酸酯，己酸乙酯，水杨酸酯，总浓度为0.05至0.5g / l，并且可优选用挥发性碱如铵的阳离子调节至所需的pH值，乙醇铵和二乙醇胺和三乙醇铵。随后通过阴极电涂或粉末涂料或低溶剂高固体涂料适当地施涂涂料。在20〜80℃的温度下，漂洗处理时间为1〜120秒。本发明用作涂料涂料，薄膜包衣或粘合剂涂料的预处理。

8. 发明授权

US5268041A Process for phosphating metal surfaces 失效
标题翻译：磷化金属表面的工艺
公开(公告)号：US5268041A
公开(公告)日：1993-12-07
申请号：US949349
申请日：1992-09-22
申请人： Horst Gehmecker , Werner Rausch , Peter Schubach
发明人： Horst Gehmecker , Werner Rausch , Peter Schubach
IPC分类号： C23C22/18 , C23C22/36 , C23C22/83 , C23C22/12
CPC分类号： C23C22/83 , C23C22/186 , C23C22/188 , C23C22/368
摘要： In a process of phosphating metal surfaces phosphating solutions are employed which are substantially free of nickel and contain______________________________________ 0.3 to 1.7 g/l Zn 0.2 to 4.0 g/l Mn 0.001 to 0.030 (preferably 0.003 to 0.020) g/l Cu 5 to 30 g/l phosphate (calculated as P.sub.2 O.sub.5) ______________________________________ in which by oxygen and/or other equivalent oxidizers the concentration of Fe(II) is kept below 0.1 g/1 and which are adjusted to a pH value from 3.0 to 3.8. The weight ratio of Cu to P.sub.2 O.sub.5 is preferably adjusted to I: (170 to 30,000) and Cu and P.sub.2 O.sub.5 are preferably replenished in a weight ratio of 1 : (5 to 2000). The phosphating solutions should contain 0.3 to 1.0 g/1 Zn if they are applied by spraying and should contain 0.9 to 1.7 g/1 Zn if they are applied by spraying/dipping operations or by a dipping operation. The process serves particularly for the pretreatment of metal surfaces for a succeeding painting, particularly by electro-dipcoating, and for the phosphating of steel, galvanized steel, zinc alloy-plated steel, aluminum and its alloys.
摘要翻译：在磷化金属表面的过程中，使用基本上不含镍的磷酸盐溶液，并且含有-0.3至1.7g / l的Zn-0.2至4.0g / l的Mn-0.001至0.030（优选0.003至-0.20）g / l的Cu -5至30g / l磷酸盐（计算为P 2 O 5） - 其中通过氧气和/或其它等效氧化剂将Fe（II）的浓度保持在0.1g / l以下，并将其调节至pH值为3.0至 3.8。优选将Cu与P 2 O 5的重量比调整为I：（170〜30,000），优选以1：（5〜2000）的重量比补充Cu和P2O5。如果通过喷涂施用，磷酸盐溶液应含有0.3至1.0 g / l的Zn，如果通过喷涂/浸渍操作或浸渍操作施加，则应含有0.9至1.7 g / l的Zn。该方法特别用于后续涂漆的金属表面的预处理，特别是通过电沉积，以及用于钢，镀锌钢，镀锌钢，铝及其合金的磷化。

9. 发明授权

US09879349B2 Method for coating metallic surfaces with an aqueous composition 有权
公开(公告)号：US09879349B2
公开(公告)日：2018-01-30
申请号：US13326633
申请日：2011-12-15
申请人： Thomas Kolberg , Manfred Walter , Peter Schubach
发明人： Thomas Kolberg , Manfred Walter , Peter Schubach
IPC分类号： B05D3/00 , B05D7/00 , C09D1/00 , C23C26/00 , C09D5/08 , C23C18/12 , C23C18/14 , C23C22/34 , C23C22/36 , B05D3/04
CPC分类号： C23C26/00 , B05D3/007 , B05D3/0413 , B05D7/52 , C09D1/00 , C09D5/08 , C23C18/122 , C23C18/1241 , C23C18/14 , C23C22/34 , C23C22/364 , C23C22/365 , C23C22/367 , C23C22/368 , C23C2222/20 , Y02T50/67 , Y10T428/273 , Y10T428/31529 , Y10T428/31663
摘要： The invention relates to a process for coating metallic surfaces with a composition containing at least one of a silane, silanol, siloxane or polysiloxane that is capable of condensation, water and optionally an organic solvent. The composition also contains compound containing Ti, Hf, Zr, Al or B; and at least one type of cation or an organic compound d) selected from monomers, oligomers, polymers, copolymers and block copolymers. The coating freshly applied with this composition is rinsed with a fluid and is not dried thoroughly before this rinsing step so that the compound capable of condensation does not condense substantially before the rinsing step.

10. 发明授权

US08349092B2 Process for coating metallic surfaces 有权
标题翻译：金属表面涂层工艺
公开(公告)号：US08349092B2
公开(公告)日：2013-01-08
申请号：US13080974
申请日：2011-04-06
申请人： Jürgen Specht , Peter Schubach , Rüdiger Rein , Peter Claude
发明人： Jürgen Specht , Peter Schubach , Rüdiger Rein , Peter Claude
IPC分类号： C23C22/12 , C23C22/07
CPC分类号： C23C22/365 , C23C22/362
摘要： A method for treating or pre-treating parts, profiled-pieces, strips, sheet metals or wires having metallic surfaces, in which at least 5% of these surfaces consists of aluminum or of at least one aluminum alloy with an acid aqueous solution which contains fluoride, zinc and phosphate and which has the following dissolved contents in the phosphatizing solution: sodium virtually none, from 0.04 to less than 2 g/L; potassium virtually none or in a concentration ranging from 0.025 to 2.5 g/L; sodium and potassium in a concentration ranging from 0.025 to 2.5 g/L as sodium, whereby the potassium content is converted to sodium on a molar basis; zinc 0.2 to 4 g/L zinc, 5 to 65 g/L calculated as PO4; 0.03 to 0.5 g/L phosphate free fluoride wherein the total fluoride is present in a concentration ranging from 0.1 to 5 g/L. A zinc-containing phosphate layer is thereby deposited onto the metallic surfaces with a layer weight ranging from 0.5 to 10 g/m2.
摘要翻译：用于处理或预处理部件，异形件，条带，金属片或具有金属表面的金属线的方法，其中至少5％的这些表面由铝或至少一种铝合金与酸性水溶液组成，所述酸性水溶液含有氟化物，锌和磷酸盐，并且在磷酸盐化溶液中具有以下溶解含量：钠实际上不为0.04至小于2g / L; 实际上无钾或浓度范围为0.025至2.5g / L的钾; 钠和钾的浓度范围为0.025至2.5g / L，钠的含量以摩尔计转换为钠; 锌0.2〜4g / L锌，5〜65g / L PO4计算; 0.03至0.5g / L磷酸盐氟化物，其中总氟化物以0.1至5g / L的浓度存在。因此，含锌磷酸盐层以0.5〜10g / m 2的重量沉积在金属表面上。

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