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1. 发明授权

US5587240A Carbon fibers and process for preparing same 失效
标题翻译：碳纤维及其制备方法
公开(公告)号：US5587240A
公开(公告)日：1996-12-24
申请号：US462753
申请日：1995-06-05
申请人： Masanobu Kobayashi , Motoi Itoh , Yoji Matsuhisa , Kazuharu Shimizu
发明人： Masanobu Kobayashi , Motoi Itoh , Yoji Matsuhisa , Kazuharu Shimizu
IPC分类号： D01F11/14 , D01F11/16 , D02G3/00
CPC分类号： D01F11/16 , D01F11/14 , Y10T428/2913 , Y10T428/2918 , Y10T428/2933 , Y10T428/2964 , Y10T428/2971
摘要： Carbon fibers with a surface oxygen concentration (O/C ratio) of 0.20 or less as measured by X-ray photoelectron spectroscopy, a surface concentration of hydroxyl groups (C-OH/C ratio) of 0.5% or greater as measured by chemical modification X-ray photoelectron spectroscopy and a surface concentration of carboxylic groups (COOH/C ratio) of 2.0% or less as measured by chemical modification X-ray photoelectron spectroscopy, and an aliphatic compound applied as a sizing agent which has multiple epoxy groups or an aromatic compound which has multiple epoxy groups, the number of atoms between the epoxy groups and an aromatic ring being 6 or greater.
摘要翻译：通过X射线光电子能谱测定，表面氧浓度（O / C比）为0.20以下的碳纤维，通过化学改性测定的羟基的表面浓度（C-OH / C比）为0.5％以上通过化学修饰X射线光电子能谱法测定的X射线光电子能谱和羧基的表面浓度（COOH / C比）为2.0％以下，作为上胶剂使用的脂肪族化合物，其具有多个环氧基或具有多个环氧基的芳香族化合物，环氧基和芳香环之间的原子数为6以上。

2. 发明授权

US5691055A Carbon fibers and process for preparing same 失效
标题翻译：碳纤维及其制备方法
公开(公告)号：US5691055A
公开(公告)日：1997-11-25
申请号：US661323
申请日：1996-06-13
申请人： Masanobu Kobayashi , Motoi Itoh , Yoji Matsuhisa , Kazuharu Shimizu
发明人： Masanobu Kobayashi , Motoi Itoh , Yoji Matsuhisa , Kazuharu Shimizu
IPC分类号： D01F11/14 , D01F11/16 , D02G3/00 , B32B9/00
CPC分类号： D01F11/16 , D01F11/14 , Y10T428/2913 , Y10T428/2918 , Y10T428/2933 , Y10T428/2964 , Y10T428/2971
摘要： Carbon fibers with a surface oxygen concentration (O/C ratio) of 0.20 or less as measured by X-ray photoelectron spectroscopy, a surface concentration of hydroxyl groups (C--OH/C ratio) of 0.5% or greater as measured by chemical modification X-ray photoelectron spectroscopy and a surface concentration of carboxylic groups (COOH/C ratio) of 2.0% or less as measured by chemical modification X-ray photoelectron spectroscopy, and an aliphatic compound applied as a sizing agent which has multiple epoxy groups or an aromatic compound which has multiple epoxy groups, the number of atoms between the epoxy groups and an aromatic ring being 6 or greater.
摘要翻译：通过X射线光电子能谱测定，表面氧浓度（O / C比）为0.20以下的碳纤维，通过化学改性测定的羟基的表面浓度（C-OH / C比）为0.5％以上通过化学修饰X射线光电子能谱法测定的X射线光电子能谱和羧基的表面浓度（COOH / C比）为2.0％以下，作为上胶剂使用的脂肪族化合物，其具有多个环氧基或具有多个环氧基的芳香族化合物，环氧基和芳香环之间的原子数为6以上。

3. 发明授权

US5589055A Method for preparing carbon fibers 失效
标题翻译：碳纤维制备方法
公开(公告)号：US5589055A
公开(公告)日：1996-12-31
申请号：US460917
申请日：1995-06-05
申请人： Masanobu Kobayashi , Motoi Itoh , Yoji Matsuhisa , Kazuharu Shimizu
发明人： Masanobu Kobayashi , Motoi Itoh , Yoji Matsuhisa , Kazuharu Shimizu
IPC分类号： D01F11/14 , D01F11/16 , C25F1/00
CPC分类号： D01F11/16 , D01F11/14 , Y10T428/2913 , Y10T428/2918 , Y10T428/2933 , Y10T428/2964 , Y10T428/2971
摘要： A process for preparing carbon fibers including electrolyzing a carbon fiber in an alkaline aqueous solution, or electrolyzing a carbon fiber in an acidic aqueous solution followed by washing with an alkaline aqueous solution, and then applying a sizing agent of an aliphatic compound with multiple epoxy groups or an aromatic compound with multiple epoxy groups in which the number of atoms between the epoxy groups and an aromatic ring is 6 or greater. Alternatively, the carbon fibers are prepared by electrolyzing a carbon fiber in an aqueous solution of an ammonium salt and then applying a sizing agent of an aliphatic compound with multiple epoxy groups or an aromatic compound with multiple epoxy groups in which the number of atoms between the epoxy groups and an aromatic ring is 6 or greater.
摘要翻译：一种制备碳纤维的方法，包括在碱性水溶液中电解碳纤维，或在酸性水溶液中电解碳纤维，然后用碱性水溶液洗涤，然后施加具有多个环氧基团的脂族化合物的施胶剂或具有多个环氧基的芳族化合物，其中环氧基和芳香环之间的原子数为6以上。或者，碳纤维是通过在铵盐水溶液中电解碳纤维，然后将具有多个环氧基的脂肪族化合物或具有多个环氧基的芳族化合物的上浆剂，环氧基和芳香环为6以上。

4. 发明授权

US5462799A Carbon fibers and process for preparing same 失效
标题翻译：碳纤维及其制备方法
公开(公告)号：US5462799A
公开(公告)日：1995-10-31
申请号：US293817
申请日：1994-08-22
申请人： Masanobu Kobayashi , Motoi Itoh , Yoji Matsuhisa , Kazuharu Shimizu
发明人： Masanobu Kobayashi , Motoi Itoh , Yoji Matsuhisa , Kazuharu Shimizu
IPC分类号： D01F11/14 , D01F11/16 , D02G3/00
CPC分类号： D01F11/16 , D01F11/14 , Y10T428/2913 , Y10T428/2918 , Y10T428/2933 , Y10T428/2964 , Y10T428/2971
摘要： Carbon fibers with a surface oxygen concentration (O/C ratio) of 0.20 or less as measured by X-ray photoelectron spectroscopy, a surface concentration of hydroxyl groups (C--OH/C ratio) of 0.5% or greater as measured by chemical modification X-ray photoelectron spectroscopy and a surface concentration of carboxylic groups (COOH/C ratio) of 2.0% or less as measured by chemical modification X-ray photoelectron spectroscopy, and comprising applied as a sizing agent an aliphatic compound which has multiple epoxy groups or an aromatic compound which has multiple epoxy groups, the number of atoms between the epoxy groups and an aromatic ring being 6 or greater. They are prepared by electrolyzing a carbon fiber in an alkaline aqueous solution, or electrolyzing a carbon fiber in an acidic aqueous solution followed by washing with an alkaline aqueous solution, and then applying a sizing agent of an aliphatic compound with multiple epoxy groups or an aromatic compound with multiple epoxy groups in which the number of atoms between the epoxy groups and an aromatic ring is 6 or greater. Alternatively, they are prepared by electrolyzing a carbon fiber in an aqueous solution of an ammonium salt and then applying a sizing agent of an aliphatic compound with multiple epoxy groups or an aromatic compound with multiple epoxy groups in which the number of atoms between the epoxy groups and an aromatic ring is 6 or greater.
摘要翻译：通过X射线光电子能谱测定，表面氧浓度（O / C比）为0.20以下的碳纤维，通过化学改性测定的羟基的表面浓度（C-OH / C比）为0.5％以上通过化学修饰X射线光电子能谱法测定的X射线光电子能谱和羧基的表面浓度（COOH / C比）为2.0％以下，并且包括作为上浆剂应用具有多个环氧基的脂肪族化合物或具有多个环氧基的芳族化合物，环氧基和芳香环之间的原子数为6以上。它们是通过在碱性水溶液中电解碳纤维，或在酸性水溶液中电解碳纤维，然后用碱性水溶液洗涤来制备的，然后施加具有多个环氧基或芳香族的脂族化合物的施胶剂具有多个环氧基的化合物，其中环氧基和芳环之间的原子数为6以上。或者，它们通过在铵盐水溶液中电解碳纤维，然后将具有多个环氧基的脂肪族化合物或具有多个环氧基的芳族化合物的施胶剂，其中环氧基团之间的原子数芳环为6以上。

5. 发明授权

US5298576A Sizing agent for carbon fiber and carbon fiber treated with said sizing agent 失效
标题翻译：用上述施胶剂处理碳纤维和碳纤维的施胶剂
公开(公告)号：US5298576A
公开(公告)日：1994-03-29
申请号：US840235
申请日：1992-02-24
申请人： Atsushi Sumida , Toyokazu Minakuchi , Motoi Itoh , Itsuki Taniguchi , Hiroshi Hasegawa , Manabu Saito
发明人： Atsushi Sumida , Toyokazu Minakuchi , Motoi Itoh , Itsuki Taniguchi , Hiroshi Hasegawa , Manabu Saito
IPC分类号： D01F11/14 , C08F283/00
CPC分类号： D01F11/14
摘要： A sizing agent for carbon fibers which comprises, as the indispensable ingredients, an epoxy resin having a viscosity of more than 1,000 P but up to 20,000 P at 50 .degree. C. and a urethane compound prepared from a polyol having an oxyalkylene unit with a polyisocyanate.
摘要翻译：作为不可或缺的成分的碳纤维用上胶剂，其包含在50℃下粘度大于1,000P但高达20,000P的环氧树脂，以及由具有氧化烯单元的多元醇与多异氰酸酯制备的氨基甲酸酯化合物。

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