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1. 发明授权

US06387843B1 Method of preparing Rh- and/or Ru-catalyst supported on MgO carrier and reforming process using the catalyst 有权
标题翻译：制备负载在MgO载体上的Rh-和/或Ru-催化剂的方法和使用该催化剂的重整方法
公开(公告)号：US06387843B1
公开(公告)日：2002-05-14
申请号：US09825966
申请日：2001-04-05
申请人： Fuyuki Yagi , Atsuro Nagumo , Yukitaka Wada , Mitsunori Shimura
发明人： Fuyuki Yagi , Atsuro Nagumo , Yukitaka Wada , Mitsunori Shimura
IPC分类号： B01J2358
CPC分类号： B01J37/0018 , B01J21/10 , B01J23/462 , B01J23/464 , B01J37/0009
摘要： A method of preparing a catalyst, including molding a mixture of magnesium oxide with a binder selected from carbon, fatty acids having 12-22 carbon atoms, magnesium salts of fatty acids having 12-22 carbon atoms, carboxymethyl cellulose, a magnesium salt of carboxymethyl cellulose and polyvinyl alcohol and calcining the molded mixture to obtain a carrier having a specific surface area of 5 m2/g of less. The carrier is impregnated with an aqueous solution containing Rh and/or Ru compounds for loading a catalytic metal component and then dried and calcined. The catalyst is used for reforming a lower hydrocarbon gas with steam and carbon dioxide or with carbon dioxide to produce a synthesis gas.
摘要翻译：一种制备催化剂的方法，包括将氧化镁与选自碳，12-22个碳原子的脂肪酸，含12-22个碳原子的脂肪酸镁盐，羧甲基纤维素，羧甲基镁盐，纤维素和聚乙烯醇，并煅烧模制的混合物以获得比表面积为5m 2 / g以下的载体。用含有Rh和/或Ru化合物的水溶液浸渍载体以负载催化金属组分，然后干燥和煅烧。催化剂用于用蒸汽和二氧化碳或二氧化碳重整低级烃气体以产生合成气。

2. 发明授权

US08758722B2 Method for producing hydrogen aimed at storage and transportation 有权
标题翻译：生产用于储存和运输的氢的方法
公开(公告)号：US08758722B2
公开(公告)日：2014-06-24
申请号：US13580643
申请日：2011-03-24
申请人： Yoshimi Okada , Masashi Saito , Shuhei Wakamatsu , Mitsunori Shimura
发明人： Yoshimi Okada , Masashi Saito , Shuhei Wakamatsu , Mitsunori Shimura
IPC分类号： C07C5/10 , C01B3/26
CPC分类号： H01M8/04216 , B01J21/12 , B01J23/755 , C01B3/0015 , C01B3/32 , C01B2203/0283 , C01B2203/0415 , C01B2203/043 , C01B2203/0445 , C01B2203/0475 , F17C11/005 , H01M8/0618 , H01M8/065 , Y02E60/321 , Y02E60/328 , Y02P30/30
摘要： Provided is a method for producing hydrogen aimed at storage and transportation, by which hydrogen for storage and transportation that is necessary for smoothly performing an organic chemical hydride method can be industrially produced efficiently at low cost. The method is a method for producing hydrogen aimed at storage and transportation in an organic chemical hydride method, in which: the hydrogenation process of an aromatic compound uses, as a hydrogen source for the reaction of the aromatic compound, a reaction gas is produced by a reforming reaction and adjusted a hydrogen concentration from 30 to 70 vol % by a shift reaction; and a hydrogenated aromatic compound is separated from a reaction mixture obtained in the hydrogenation process, which is followed by purification.
摘要翻译：本发明提供一种用于生产用于储存和运输的氢的方法，通过该方法可以有效地以低成本工业生产有机化学氢化物方法顺利进行所需的储存和运输用氢。该方法是在有机化学氢化物方法中制备用于储存和输送的氢的方法，其中：芳族化合物的氢化方法使用作为芳族化合物的反应的氢源，反应气体由重整反应，通过转移反应将氢浓度调整为30〜70体积％并从氢化过程中获得的反应混合物中分离氢化芳族化合物，然后进行纯化。

3. 发明授权

US06340437B1 Process for preparing synthesis gas by autothermal reforming 有权
标题翻译：通过自热重整制备合成气的方法
公开(公告)号：US06340437B1
公开(公告)日：2002-01-22
申请号：US09254636
申请日：1999-03-11
申请人： Fuyuki Yagi , Atsuro Nagumo , Yukitaka Wada , Mitsunori Shimura , Sachio Asaoka , Shuhei Wakamatsu
发明人： Fuyuki Yagi , Atsuro Nagumo , Yukitaka Wada , Mitsunori Shimura , Sachio Asaoka , Shuhei Wakamatsu
IPC分类号： C07C102
CPC分类号： B01J23/40 , C01B3/40 , C01B32/40 , C01B2203/1064 , C01B2203/107 , C01B2203/1082 , Y02P20/52
摘要： Disclosed is a process for producing a synthesis gas by an autothermal reforming method including a step of partially oxidizing a carbon-containing organic compound to produce a high temperature mixed gas, and a synthesis producing step of reacting the unreacted carbon-containing organic compound contained in the high temperature mixed gas with carbon dioxide and/or steam, wherein a catalyst having a considerably suppressed carbon deposition activity is used as a catalyst for the synthesis gas producing step. The catalyst is characterized in that the catalyst comprises a carrier formed of a metal oxide, and at least one catalytic metal selected from rhodium, ruthenium, iridium, palladium and platinum and supported on the carrier, in that the catalyst has a specific surface area of 25 m2/g or less, in that metal ion of the carrier metal oxide has electronegativity of 13.0 or less, and in that the amount of the catalytic metal supported is 0.0005-0.1 mole %, in terms of a metal, based on the carrier metal oxide.
摘要翻译：公开了一种通过自热重整法制备合成气的方法，该方法包括将含碳有机化合物部分氧化以产生高温混合气体的步骤，以及合成制备步骤，使含有具有二氧化碳和/或蒸汽的高温混合气体，其中具有显着抑制的碳沉积活性的催化剂用作合成气生产步骤的催化剂。催化剂的特征在于催化剂包含由金属氧化物形成的载体和至少一种选自铑，钌，铱，钯和铂的催化金属并负载在载体上，因为催化剂具有比表面积 25m 2 / g以下，载体金属氧化物的金属离子的电负性为13.0以下，并且，以金属为基准，载体的载体量为0.0005〜0.1摩尔％金属氧化物。

4. 发明授权

US06312660B1 Process for preparing synthesis gas 有权
标题翻译：合成气的制备方法
公开(公告)号：US06312660B1
公开(公告)日：2001-11-06
申请号：US09254635
申请日：1999-03-11
申请人： Fuyuki Yagi , Atsuro Nagumo , Yukitaka Wada , Mitsunori Shimura , Sachio Asaoka , Shuhei Wakamatsu
发明人： Fuyuki Yagi , Atsuro Nagumo , Yukitaka Wada , Mitsunori Shimura , Sachio Asaoka , Shuhei Wakamatsu
IPC分类号： C01B326
CPC分类号： C01B3/40 , B01J23/40 , C01B32/40 , C01B2203/1064 , C01B2203/107 , C01B2203/1082 , Y02P20/52
摘要： Disclosed is a process for producing a synthesis gas by reacting a carbon-containing organic compound with steam and/or carbon dioxide using a catalyst whose carbon deposition activity is considerably suppressed. The catalyst is characterized in that it comprises a carrier formed of a metal oxide, and at least one catalytic metal selected from rhodium, ruthenium, iridium, palladium and platinum and supported on the carrier, in that the catalyst has a specific surface area of 25 m2/g or less, in that the electronegativity of the metal ion of the carrier metal oxide is 13.0 or less and in that the amount of the catalytic metal is 0.0005-0.1 mole %, in terms of metal, based on the carrier metal oxide.
摘要翻译：公开了一种通过使碳含量有机化合物与蒸汽和/或二氧化碳反应的催化剂，其碳沉积活性受到显着抑制而制备合成气的方法。该催化剂的特征在于其包含由金属氧化物形成的载体和至少一种选自铑，钌，铱，钯和铂的催化金属并负载在载体上，因为催化剂的比表面积为25 m 2 / g以下，其中载体金属氧化物的金属离子的电负性为13.0以下，催化剂金属的量为0.0005〜0.1摩尔％，以金属计，基于载体金属氧化物。

5. 发明授权

US5316821A Partition plate for multiple-stage adsorption separator 失效
标题翻译：多级吸附分离器分隔板
公开(公告)号：US5316821A
公开(公告)日：1994-05-31
申请号：US988888
申请日：1992-12-10
申请人： Seiya Otani , Hiroaki Taniguchi , Kei Yokoyama , Yoshimi Shiroto , Mitsunori Shimura , Osamu Akimoto , Masayoshi Notoya
发明人： Seiya Otani , Hiroaki Taniguchi , Kei Yokoyama , Yoshimi Shiroto , Mitsunori Shimura , Osamu Akimoto , Masayoshi Notoya
IPC分类号： B01D15/18 , B01D24/04 , B01D24/12 , B01D24/42 , B32B3/24
CPC分类号： B01D15/1842 , B01D2215/023 , Y10T428/24273 , Y10T428/24322 , Y10T428/24331 , Y10T428/24479 , Y10T428/24562 , Y10T428/24612
摘要： A partition plate for multiple-stage adsorption separator includes a planar body member having opposing external surfaces and a peripheral edge with conduits providing fluid communication between the opposing surfaces and different points on the peripheral edge. Each of the opposing surfaces is provided with a peripheral rim and covered with a perforated plate whereby an open chamber is defined between the body member and a perforated plate at each of the external faces.
摘要翻译：用于多级吸附分离器的分隔板包括具有相对的外表面的平面本体构件和具有导管的周边边缘，其提供相对表面与周边边缘上的不同点之间的流体连通。每个相对的表面设置有外围边缘并且被多孔板覆盖，由此在每个外表面处在主体构件和多孔板之间限定开放室。

6. 发明授权

US5200075A Separator 失效
标题翻译：分隔器
公开(公告)号：US5200075A
公开(公告)日：1993-04-06
申请号：US846198
申请日：1992-03-05
申请人： Seiya Otani , Hiroaki Taniguchi , Kei Yokoyama , Yoshimi Shiroto , Mitsunori Shimura , Osamu Akimoto , Masayoshi Notoya
发明人： Seiya Otani , Hiroaki Taniguchi , Kei Yokoyama , Yoshimi Shiroto , Mitsunori Shimura , Osamu Akimoto , Masayoshi Notoya
IPC分类号： B01D15/18
CPC分类号： B01D15/1842 , B01D2215/023 , Y10T428/24273 , Y10T428/24322 , Y10T428/24331 , Y10T428/24479 , Y10T428/24562 , Y10T428/24612
摘要： An adsorbent is charged into a horizontal type packed column having a multiplicity of packed vessels each of which is composed of a partition plate and a cylindrical body and which are connected through the partition plates, from an opening formed on the upper wall of each cylindrical body. Then, each opening is closed tightly with a detachable plug cover. The partition plate is provided with a first fluid passage through which a fluid is passed in the direction of the axis of the cylindrical body and a second fluid passage which is in communication with the first fluid passage, which extends toward the peripheral wall of the cylindrical body and which opens at the cylindrical body. This apparatus is suitable for use as a multiple-stage adsorption separator directed to a simulated moving-bed system.
摘要翻译：将吸附剂装入具有多个填充容器的水平型填充柱，每个填充容器由分隔板和圆柱体组成，并且通过隔板连接，从形成在每个圆柱体的上壁上的开口。然后，每个开口用可拆卸的插头盖紧紧地闭合。分隔板设置有第一流体通道，流体沿着圆柱体的轴线方向通过，第二流体通道与第一流体通道连通，第二流体通道朝向圆柱体的周壁延伸并且在圆柱体上打开。该装置适用于指向模拟移动床系统的多级吸附分离器。

7. 发明授权

US4992622A Method of separating 2,6-diisopropylnaphthalene from a mixture containing diisopropylnaphthalene isomers 失效
标题翻译：从含有二异丙基萘异构体的混合物中分离2,6-二异丙基萘的方法
公开(公告)号：US4992622A
公开(公告)日：1991-02-12
申请号：US388590
申请日：1989-08-02
申请人： Yoshimi Shiroto , Mitsunori Shimura , Kenji Shimokawa , Yoshio Fukui , Yakudo Tachibana , Kazuhiko Tate , Hiroaki Taniguchi
发明人： Yoshimi Shiroto , Mitsunori Shimura , Kenji Shimokawa , Yoshio Fukui , Yakudo Tachibana , Kazuhiko Tate , Hiroaki Taniguchi
IPC分类号： C07C7/13
CPC分类号： C07C7/13
摘要： A method of separating 2,6-diisopropylnaphthalene from a mixture containing 2,6-diisopropylnaphthalene and structural isomers thereof including the 2,7-isomer is disclosed, wherein the mixture is first subjected to a selective adsorption and desorption treatment using a zeolite absorbent capable of adsorbing the 2,7-isomer to obtain a first extract containing the sorbed 2,7-isomer and a first raffinate containing non-sorbed isomers including the 2,6-isomer, the 2,6-isomer being thereafter separated from the first raffinate.
摘要翻译：公开了从包含2,6-二异丙基萘的混合物中分离2,6-二异丙基萘的方法及其结构异构体，其中包括2,7-异构体，其中首先使用具有沸石吸收能力的混合物进行选择性吸附和解吸处理吸收2,7-异构体以获得含有吸附的2,7-异构体的第一提取物和含有包含2,6-异构体的非吸附异构体的第一残液，然后将2,6-异构体从第一个残液

8. 发明申请

US20120321549A1 METHOD FOR PRODUCING HYDROGEN AIMED AT STORAGE AND TRANSPORTATION 有权
标题翻译：用于生产存储和运输氢的方法
公开(公告)号：US20120321549A1
公开(公告)日：2012-12-20
申请号：US13580643
申请日：2011-03-24
申请人： Yoshimi Okada , Masashi Saito , Shuhei Wakamatsu , Mitsunori Shimura
发明人： Yoshimi Okada , Masashi Saito , Shuhei Wakamatsu , Mitsunori Shimura
IPC分类号： C01B3/02 , C01B3/26
CPC分类号： H01M8/04216 , B01J21/12 , B01J23/755 , C01B3/0015 , C01B3/32 , C01B2203/0283 , C01B2203/0415 , C01B2203/043 , C01B2203/0445 , C01B2203/0475 , F17C11/005 , H01M8/0618 , H01M8/065 , Y02E60/321 , Y02E60/328 , Y02P30/30
摘要： Provided is a method for producing hydrogen aimed at storage and transportation, by which hydrogen for storage and transportation that is necessary for smoothly performing an organic chemical hydride method can be industrially produced efficiently at low cost. The method is a method for producing hydrogen aimed at storage and transportation in an organic chemical hydride method, in which: the hydrogenation process of an aromatic compound uses, as a hydrogen source for the reaction of the aromatic compound, a reaction gas is produced by a reforming reaction and adjusted a hydrogen concentration from 30 to 70 vol % by a shift reaction; and a hydrogenated aromatic compound is separated from a reaction mixture obtained in the hydrogenation process, which is followed by purification.
摘要翻译：本发明提供一种用于生产用于储存和运输的氢的方法，通过该方法可以有效地以低成本工业生产有机化学氢化物方法顺利进行所需的储存和运输用氢。该方法是在有机化学氢化物方法中制备用于储存和输送的氢的方法，其中：芳族化合物的氢化方法使用作为芳族化合物的反应的氢源，反应气体由重整反应，通过转移反应将氢浓度调整为30〜70体积％并从氢化过程中获得的反应混合物中分离氢化芳族化合物，然后进行纯化。

9. 发明授权

US06806296B2 Process of producing liquid hydrocarbon oil or dimethyl ether from lower hydrocarbon gas containing carbon dioxide 有权
标题翻译：从含有二氧化碳的低碳氢化合物气体生产液态烃油或二甲醚的方法
公开(公告)号：US06806296B2
公开(公告)日：2004-10-19
申请号：US10649735
申请日：2003-08-28
申请人： Yoshimi Shiroto , Kenichi Kawazuishi , Masato Tauchi , Mitsunori Shimura
发明人： Yoshimi Shiroto , Kenichi Kawazuishi , Masato Tauchi , Mitsunori Shimura
IPC分类号： C07C2700
CPC分类号： C10G2/32 , C01B3/38 , C01B2203/0233 , C01B2203/0238 , C01B2203/062 , C01B2203/1247 , C01B2203/1264 , C07C41/01 , C10G2/332 , C10G2/333 , C07C43/043
摘要： A process for the production of a liquid hydrocarbon oil from a gas feed containing a lower hydrocarbon and CO2, wherein the gas feed is mixed with H2O to obtain a mixed gas having specific CO2, H2O and lower hydrocarbon contents. The mixed gas is contacted with a Rh, Ru/MgO catalyst having a specific surface area of 5 m2/g or less to produce a synthesis gas with a carbon conversion efficiency Cf of at least 50%. The thus obtained synthesis gas having a H2/CO molar ratio of 1.5-2.5 is reacted in the presence of a Fischer-Tropsch catalyst to obtain a liquid hydrocarbon oil, while the synthesis gas having a H2/CO molar ratio of 0.5-1.5 is reacted in the presence of one or more catalysts having methanol synthesizing, dehydrating and CO shift reaction activities to obtain dimethyl ether.
摘要翻译：一种从含有较低烃和二氧化碳的气体原料生产液体烃油的方法，其中气体进料与H 2 O混合以获得具有特定CO 2，H 2 O和较低烃含量的混合气体。混合气体与比表面积为5m 2 / g以下的Rh，Ru / MgO催化剂接触，生成碳转化效率Cf为50％以上的合成气。将由此获得的H 2 / CO摩尔比为1.5-2.5的合成气在费 - 托催化剂的存在下反应得到液态烃油，而H 2 / CO摩尔比为0.5-1.5的合成气为在一种或多种具有甲醇合成，脱水和CO转化反应活性的催化剂的存在下反应，得到二甲醚。

10. 发明授权

US06656978B2 Process of producing liquid hydrocarbon oil or dimethyl ether from lower hydrocarbon gas containing carbon dioxide 有权
标题翻译：从含有二氧化碳的低碳氢化合物气体生产液态烃油或二甲醚的方法
公开(公告)号：US06656978B2
公开(公告)日：2003-12-02
申请号：US09825967
申请日：2001-04-05
申请人： Yoshimi Shiroto , Kenichi Kawazuishi , Masato Tauchi , Mitsunori Shimura
发明人： Yoshimi Shiroto , Kenichi Kawazuishi , Masato Tauchi , Mitsunori Shimura
IPC分类号： C07C2700
CPC分类号： C10G2/32 , C01B3/38 , C01B2203/0233 , C01B2203/0238 , C01B2203/062 , C01B2203/1247 , C01B2203/1264 , C07C41/01 , C10G2/332 , C10G2/333 , C07C43/043
摘要： A process for the production of a liquid hydrocarbon oil from a gas feed containing a lower hydrocarbon and CO2, wherein the gas feed is mixed with H2O to obtain a mixed gas having specific CO2, H2O and lower hydrocarbon contents. The mixed gas is contacted with a Rh, Ru/MgO catalyst having a specific surface area of 5 m2/g or less to produce a synthesis gas with a carbon conversion efficiency Cf of at least 50%. The thus obtained synthesis gas having a H2/CO molar ratio of 1.5-2.5 is reacted in the presence of a Fischer-Tropsch catalyst to obtain a liquid hydrocarbon oil, while the synthesis gas having a H2/CO molar ratio of 0.5-1.5 is reacted in the presence of one or more catalysts having methanol synthesizing, dehydrating and CO shift reaction activities to obtain dimethyl ether.
摘要翻译：一种从含有较低烃和二氧化碳的气体原料生产液体烃油的方法，其中气体进料与H 2 O混合以获得具有特定CO 2，H 2 O和较低烃含量的混合气体。混合气体与比表面积为5m 2 / g以下的Rh，Ru / MgO催化剂接触，生成碳转化效率Cf为50％以上的合成气。将由此获得的H 2 / CO摩尔比为1.5-2.5的合成气在费 - 托催化剂的存在下反应得到液态烃油，而H 2 / CO摩尔比为0.5-1.5的合成气是在一种或多种具有甲醇合成，脱水和CO转化反应活性的催化剂的存在下反应，得到二甲醚。

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