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1. 发明申请

US20050002853A1 Process for producing zinc sulfide particles 失效
标题翻译：硫化锌颗粒生产方法
公开(公告)号：US20050002853A1
公开(公告)日：2005-01-06
申请号：US10902208
申请日：2004-07-30
申请人： Milan Hubacek , Kenji Takahashi
发明人： Milan Hubacek , Kenji Takahashi
IPC分类号： C01G9/00 , C01G9/08 , C01G45/00 , C09K11/02 , C09K11/08 , C09K11/56 , C09K11/57 , C09K11/77 , C01G11/02
CPC分类号： C01G9/08 , C01G9/00 , C01G45/00 , C09K11/02 , C09K11/574 , C09K11/7701
摘要： A mixed melt, which contains urea and/or a urea derivative and contains a sulfur source and a zinc source, is prepared. A temperature of the mixed melt is raised, and a precipitate of zinc sulfide is thereby formed. The temperature of the mixed melt is raised even further, and a solid material containing the zinc sulfide is thereby formed. The solid material is fired, and organic constituents contained in the solid material are thus removed. Zinc sulfide particles having uniform particle size and free from inclusion of impurities are thus produced without any precipitant being added.
摘要翻译：制备含有尿素和/或尿素衍生物并含有硫源和锌源的混合熔体。混合熔体的温度升高，从而形成硫化锌的沉淀。混合熔体的温度进一步升高，由此形成含有硫化锌的固体材料。固体材料被烧制，并且固体材料中包含的有机成分被除去。因此，在没有添加任何沉淀剂的情况下，生产粒径均匀且不含杂质的硫化锌颗粒。

2. 发明授权

US07070756B2 Process for producing zinc sulfide particles 失效
标题翻译：硫化锌颗粒生产方法
公开(公告)号：US07070756B2
公开(公告)日：2006-07-04
申请号：US10902208
申请日：2004-07-30
申请人： Milan Hubacek , Kenji Takahashi
发明人： Milan Hubacek , Kenji Takahashi
IPC分类号： C01G9/08 , C09K11/56
CPC分类号： C01G9/08 , C01G9/00 , C01G45/00 , C09K11/02 , C09K11/574 , C09K11/7701
摘要： A mixed melt, which contains urea and/or a urea derivative and contains a sulfur source and a zinc source, is prepared. A temperature of the mixed melt is raised, and a precipitate of zinc sulfide is thereby formed. The temperature of the mixed melt is raised even further, and a solid material containing the zinc sulfide is thereby formed. The solid material is fired, and organic constituents contained in the solid material are thus removed. Zinc sulfide particles having uniform particle size and free from inclusion of impurities are thus produced without any precipitant being added.
摘要翻译：制备含有尿素和/或尿素衍生物并含有硫源和锌源的混合熔体。混合熔体的温度升高，从而形成硫化锌的沉淀。混合熔体的温度进一步升高，由此形成含有硫化锌的固体材料。固体材料被烧制，并且固体材料中包含的有机成分被除去。因此，在没有添加任何沉淀剂的情况下，生产粒径均匀且不含杂质的硫化锌颗粒。

3. 发明授权

US07378038B2 Process for producing phosphors 失效
标题翻译：荧光体生产工艺
公开(公告)号：US07378038B2
公开(公告)日：2008-05-27
申请号：US10909374
申请日：2004-08-03
申请人： Milan Hubacek , Kenji Takahashi
发明人： Milan Hubacek , Kenji Takahashi
IPC分类号： C09K11/08
CPC分类号： C09K11/576 , C09K11/574 , C09K11/7774 , C09K11/7784 , C09K11/7789
摘要： A mixed melt, which contains urea and/or a urea derivative and contains a metal compound, is prepared. The mixed melt is solidified, by heating, whereby the urea and/or urea derivative is decomposed, a precursor being thereby prepared. The thus prepared precursor is ground, and then the thus ground precursor is fired. The metal of the metal compound may be at least one kind of a metal selected from the group consisting of Al, B, Ba, Be, Bi, Ca, Cd, Cs, Ga, Ge, Hf, In, K, Li, Mg, Mo, Na, Nb, P, Rb, Si, Sn, Sr, Ta, Ti, V, W, Zr, and rare earth metals. A finely powdered phosphor free from inclusion of impurities and having uniform particle size is thus produced at a low cost and efficiently.
摘要翻译：制备含有尿素和/或脲衍生物并含有金属化合物的混合熔体。混合的熔体通过加热固化，由此使尿素和/或尿素衍生物分解，由此制备前体。将如此制备的前体研磨，然后将如此研磨的前体烧制。金属化合物的金属可以是选自Al，B，Ba，Be，Bi，Ca，Cd，Cs，Ga，Ge，Hf，In，K，Li，Mg中的至少一种金属，Mo，Na，Nb，P，Rb，Si，Sn，Sr，Ta，Ti，V，W，Zr和稀土金属。因此，以低成本且有效地生产不含杂质并且具有均匀粒度的细粉末状磷光体。

4. 发明申请

US20050029495A1 Process for producing phosphors 失效
标题翻译：荧光体生产工艺
公开(公告)号：US20050029495A1
公开(公告)日：2005-02-10
申请号：US10909374
申请日：2004-08-03
申请人： Milan Hubacek , Kenji Takahashi
发明人： Milan Hubacek , Kenji Takahashi
IPC分类号： C09K11/08 , C09K11/56 , C09K11/57 , C09K11/59 , C09K11/77 , C09K11/78 , C09K11/79 , C09K11/84
CPC分类号： C09K11/576 , C09K11/574 , C09K11/7774 , C09K11/7784 , C09K11/7789
摘要： A mixed melt, which contains urea and/or a urea derivative and contains a metal compound, is prepared. A temperature of the mixed melt is raised, and the mixed melt is solidified, a precursor being thereby prepared. The thus prepared precursor is ground, and then the thus ground precursor is fired. The metal of the metal compound may be at least one kind of a metal selected from the group consisting of Al, B, Ba, Be, Bi, Ca, Cd, Cs, Ga, Ge, Hf, In, K, Li, Mg, Mo, Na, Nb, P, Rb, Si, Sn, Sr, Ta, Ti, V, W, Zr, and rare earth metals. A finely powdered phosphor free from inclusion of impurities and having uniform particle size is thus produced at a low cost and efficiently.
摘要翻译：制备含有尿素和/或脲衍生物并含有金属化合物的混合熔体。提高混合熔体的温度，使混合熔体固化，由此制备前体。将如此制备的前体研磨，然后将如此研磨的前体烧制。金属化合物的金属可以是选自Al，B，Ba，Be，Bi，Ca，Cd，Cs，Ga，Ge，Hf，In，K，Li，Mg中的至少一种金属，Mo，Na，Nb，P，Rb，Si，Sn，Sr，Ta，Ti，V，W，Zr和稀土金属。因此，以低成本且有效地生产不含杂质并且具有均匀粒度的细粉末状磷光体。

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