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1. 发明授权

US08188211B2 Oxymethylene polymers, process for the preparation thereof and use thereof 失效
标题翻译：甲醛聚合物，其制备方法和用途
公开(公告)号：US08188211B2
公开(公告)日：2012-05-29
申请号：US12423682
申请日：2009-04-14
申请人： Michael Haubs , Michael Hoffmockel , Jürgen Lingnau , Robert Gronner , Horst Roeschert
发明人： Michael Haubs , Michael Hoffmockel , Jürgen Lingnau , Robert Gronner , Horst Roeschert
IPC分类号： C08G65/34
CPC分类号： C08G2/04 , C08G2/24 , C08G2/34 , C08L59/02 , C08L59/04 , C08L2666/16
摘要： Oxymethylene polymers having a bimodal distribution or having a distribution of higher modality and having a targeted content of a low molecular weight fraction of from 1 to 5 percent by mass are described. Moldings of these polymers are distinguished by high low-temperature notched impact strength associated with a high modulus of elasticity.
摘要翻译：描述具有双峰分布或具有较高模态分布并且具有1至5质量％的低分子量分数的目标含量的甲醛聚合物。这些聚合物的模制品通过与高弹性模量相关的高低温缺口冲击强度来区分。

2. 发明授权

US08133966B2 Oxymethylene copolymers and the use thereof and process for the preparation of oxymethylene copolymers 失效
标题翻译：甲醛共聚物及其用途和制备甲醛共聚物的方法
公开(公告)号：US08133966B2
公开(公告)日：2012-03-13
申请号：US12423625
申请日：2009-04-14
申请人： Michael Haubs , Michael Hoffmockel , Jürgen Lingnau , Robert Gronner , Michael Gene Yearwood
发明人： Michael Haubs , Michael Hoffmockel , Jürgen Lingnau , Robert Gronner , Michael Gene Yearwood
IPC分类号： C08G12/00
CPC分类号： C08G2/24 , C08G2/04 , C08G2/34
摘要： Oxymethylene copolymers having a high proportion of terminal alkyl ether groups and having terminal hydroxyalkylene groups are described. These polymers are distinguished by high thermal stability and high hot water resistance. Furthermore, a process for the preparation of oxymethylene copolymers is described in which the polymerization of at least one monomer forming —CH2—O— units is effected in the presence of at least one acetal of formaldehyde and of at least one initiator of cationic polymerization and the initiator of cationic polymerization is used in an amount of less than or equal to 10−4 mol %, based on the amount of the monomers present at the beginning of the polymerization and forming —CH2—O— units, in which starting materials of the polymerization are used such that the content of water and formic acid at the beginning of the polymerization is less than or equal to 40 ppm, and in which the initiator and/or the active polymer chains are deactivated by treatment of the prepared polymer with a base-containing protic solvent.
摘要翻译：描述了具有高比例的末端烷基醚基团并具有末端羟基亚烷基的甲醛共聚物。这些聚合物的特征在于高热稳定性和高耐热水性。此外，描述了制备甲醛共聚物的方法，其中形成-CH 2 -O-单元的至少一种单体的聚合在至少一种甲醛缩醛和至少一种阳离子聚合引发剂的存在下进行，并且基于聚合开始时存在的单体的量和形成-CH 2 -O-单元，阳离子聚合引发剂的用量小于或等于10-4mol％，其中起始原料为使用聚合，使得聚合开始时的水和甲酸的含量小于或等于40ppm，并且其中引发剂和/或活性聚合物链通过用制备的聚合物处理而失活含碱性质子溶剂。

3. 发明申请

US20110160428A1 Initiator 有权
公开(公告)号：US20110160428A1
公开(公告)日：2011-06-30
申请号：US13043080
申请日：2011-03-08
申请人： Michael Hoffmockel , Michael Haubs , Horst Röschert
发明人： Michael Hoffmockel , Michael Haubs , Horst Röschert
IPC分类号： C08G65/10
CPC分类号： C08G75/24 , C08G2/06 , C08G2/10
摘要： An initiator for cationic polymerization comprises a salt of a protic acid as well as a protic acid. The molar ratio of protic acid to salt is in the range from 1:0.01 to 1:2000. The initiator is used for example for cationic homo- or copolymerization of trioxane, and permits stable and flexible operation of the polymerization.

4. 发明授权

US07906594B2 Process for preparation of polymer blends composed of polyoxymethylenes and of thermoplastic elastomers 失效
标题翻译：由聚甲醛和热塑性弹性体组成的聚合物共混物的制备方法
公开(公告)号：US07906594B2
公开(公告)日：2011-03-15
申请号：US11520415
申请日：2006-09-13
申请人： Karl-Friedrich Mück , Ernst Hofmann , Michael Hoffmockel
发明人： Karl-Friedrich Mück , Ernst Hofmann , Michael Hoffmockel
IPC分类号： C08L61/02
CPC分类号： C08L59/00 , C08L75/04 , Y10T428/31942 , C08L2666/20
摘要： The invention relates to a process for preparation of polymer blends comprising at least one polyoxymethylene and at least one thermoplastic elastomer, where the thermoplastic elastomer is micropelletized by a pelletizing process and the pellets obtained in a) are dispersed in the polyoxymethylene matrix via melting of the components and mixing of these at low shear forces, and also to the use of micropelletized thermoplastic elastomers for preparation of polyoxymethylenes with low formaldehyde emission.
摘要翻译：本发明涉及一种制备包含至少一种聚甲醛和至少一种热塑性弹性体的聚合物共混物的方法，其中热塑性弹性体通过造粒工艺进行微胶体化，并且将a）中获得的颗粒分散在聚甲醛基体中，组分和这些在低剪切力下的混合，以及使用微胶体化热塑性弹性体制备低甲醛释放的聚甲醛。

5. 发明申请

US20090200153A1 Method for producing and dehydrating cyclic formals 审中-公开
标题翻译：生产和脱水循环甲醛的方法
公开(公告)号：US20090200153A1
公开(公告)日：2009-08-13
申请号：US11665047
申请日：2005-10-06
申请人： Reinhard Wagener , Michael Haubs , Juergen Lingnau , Matthias Göring , Michael Hoffmockel
发明人： Reinhard Wagener , Michael Haubs , Juergen Lingnau , Matthias Göring , Michael Hoffmockel
IPC分类号： B01D61/36
CPC分类号： B01D61/362 , B01D53/22 , C07D317/12
摘要： Processes are described which comprise: (a) providing a mixture comprising a cyclic formal and water, wherein the mixture has a cyclic formal concentration and a water concentration; (b) bringing the mixture into contact with an aqueously selective membrane; (c) creating a pressure differential across the membrane; and (d) obtaining a permeate having a higher water concentration and a lower cyclic formal concentration than the mixture, and a retentate having a lower water concentration and a higher cyclic formal concentration than the mixture.
摘要翻译：描述了方法，其包括：（a）提供包含环状缩甲醛和水的混合物，其中所述混合物具有环形形式浓度和水浓度; （b）使混合物与高选择性的膜接触; （c）跨过膜产生压力差; 和（d）获得具有比混合物更高的水浓度和较低的环状甲醛浓度的渗透物，以及具有比混合物低的水浓度和较高的环状甲醛浓度的滞留物。

6. 发明申请

US20080182966A1 POLYOXYMETHYLENE COPOLYMERS, THEIR PREPARATION AND USE 审中-公开
标题翻译：聚甲基乙烯共聚物，其制备和使用
公开(公告)号：US20080182966A1
公开(公告)日：2008-07-31
申请号：US12058197
申请日：2008-03-28
申请人： Karl-Friedrich Mück , Klaus Kurz , Michael Hoffmockel
发明人： Karl-Friedrich Mück , Klaus Kurz , Michael Hoffmockel
IPC分类号： C08G65/34
CPC分类号： C08G2/38
摘要： Copolymers are described containing blocks of the structural repeat units of the formula I and blocks containing structural units of the formula II [—O—CH2—]x, (I) [—O—R1—], (II) where R1 is a divalent radical derived from a hydroxy-terminated aliphatic or cycloaliphatic oligomer or polymer which, where appropriate, has ether groups and/or carbonyloxy groups in the chain, and x is a whole number, at least 10.The copolymers may be used for producing moldings.
摘要翻译：描述共聚物，其包含式I的结构重复单元的嵌段和含有式II的结构单元的嵌段<？in-line-formula description =“In-line Formulas”end =“lead”→[ - O-CH （I）<？in-line-formula description =“In-line Formulas”end =“tail”？> <？in-line-formula- 公式描述=“在线公式”end =“lead”？> [ - OR ^{1 - ]，（II）<？in-line-formula description =“In-line Formulas”end = 其中R 1是衍生自羟基封端的脂族或脂环族低聚物或聚合物的二价基团，其在适当的情况下在链中具有醚基和/或羰氧基，x 是整数，至少为10.共聚物可用于生产模制品。}

7. 发明授权

US08742065B2 Oxymethylene polymers, process for the preparation thereof and use thereof 有权
标题翻译：甲醛聚合物，其制备方法和用途
公开(公告)号：US08742065B2
公开(公告)日：2014-06-03
申请号：US13482158
申请日：2012-05-29
申请人： Michael Haubs , Michael Hoffmockel , Jürgen Lingnau , Robert Gronner , Horst Roeschert
发明人： Michael Haubs , Michael Hoffmockel , Jürgen Lingnau , Robert Gronner , Horst Roeschert
IPC分类号： C08G65/34
CPC分类号： C08G2/04 , C08G2/24 , C08G2/34 , C08L59/02 , C08L59/04 , C08L2666/16
摘要： Oxymethylene polymers having a bimodal distribution or having a distribution of higher modality and having a targeted content of a low molecular weight fraction of from 1 to 5 percent by mass are described. Moldings of these polymers are distinguished by high low-temperature notched impact strength associated with a high modulus of elasticity.
摘要翻译：描述具有双峰分布或具有较高模态分布并且具有1至5质量％的低分子量分数的目标含量的甲醛聚合物。这些聚合物的模制品通过与高弹性模量相关的高低温缺口冲击强度来区分。

8. 发明授权

US08691936B2 Initiator 有权
标题翻译：发起人
公开(公告)号：US08691936B2
公开(公告)日：2014-04-08
申请号：US13527356
申请日：2012-06-19
申请人： Michael Hoffmockel , Michael Haubs , Horst Röschert
发明人： Michael Hoffmockel , Michael Haubs , Horst Röschert
IPC分类号： C08F6/00 , C08G2/28 , C09K3/00
CPC分类号： C08G75/24 , C08G2/06 , C08G2/10
摘要： An initiator for cationic polymerization comprises a salt of a protic acid as well as a protic add. The molar ratio of protic acid to salt is in the range from 1:0.01 to 1:2000. The initiator is used for example for cationic homo- or copolymerization of trioxane, and permits stable and flexible operation of the polymerization.
摘要翻译：阳离子聚合引发剂包括质子酸和质子酸的盐。质子酸与盐的摩尔比在1:0.01至1:2000的范围内。引发剂用于例如三恶烷的阳离子均聚或共聚，并且允许聚合的稳定和灵活的操作。

9. 发明授权

US07301055B2 Process for removing methanol from formaldehyde-containing solutions 有权
标题翻译：从含甲醛溶液中除去甲醇的方法
公开(公告)号：US07301055B2
公开(公告)日：2007-11-27
申请号：US10451469
申请日：2001-11-19
申请人： Michael Hoffmockel , Matthias Göring , Juergen Lingnau , Karl-Friedrich Mück
发明人： Michael Hoffmockel , Matthias Göring , Juergen Lingnau , Karl-Friedrich Mück
IPC分类号： C07C45/29 , C07C27/26
CPC分类号： C08G2/24 , C07C45/002 , C07C45/38 , C07C45/82 , C07C45/85 , C07D323/06 , C08G2/08 , C08G2/10 , Y02P20/127 , C07C47/04
摘要： Process for removing methanol from formaldehyde-containing solutions. The present invention relates to a process for removing methanol from formaldehyde-containing solutions, with methanol being converted into formaldehyde dimethyl acetal by reactive distillation in the presence of an acidic fixed-bed catalyst, and the resultant mixture comprising methanol, formaldehyde dimethyl acetal and possibly other impurities being distilled off.
摘要翻译：从含甲醛溶液中除去甲醇的方法。本发明涉及一种从含甲醛溶液中除去甲醇的方法，甲醇通过反应蒸馏在酸性固定床催化剂存在下转化为甲醛二甲缩醛，所得混合物包含甲醇，甲醛二甲基缩醛和可能的其他杂质被蒸馏掉。

10. 发明申请

US20070060715A1 Process for preparation of polymer blends composed of polyoxymethylenes and of thermoplastic elastomers 失效
标题翻译：由聚甲醛和热塑性弹性体组成的聚合物共混物的制备方法
公开(公告)号：US20070060715A1
公开(公告)日：2007-03-15
申请号：US11520415
申请日：2006-09-13
申请人： Karl-Friedrich Muck , Ernst Hofmann , Michael Hoffmockel
发明人： Karl-Friedrich Muck , Ernst Hofmann , Michael Hoffmockel
IPC分类号： C08L71/02 , C08L75/04 , B32B27/00
CPC分类号： C08L59/00 , C08L75/04 , Y10T428/31942 , C08L2666/20
摘要： The invention relates to a process for preparation of polymer blends comprising at least one polyoxymethylene and at least one thermoplastic elastomer, where the thermoplastic elastomer is micropelletized by a pelletizing process and the pellets obtained in a) are dispersed in the polyoxymethylene matrix via melting of the components and mixing of these at low shear forces, and also to the use of micropelletized thermoplastic elastomers for preparation of polyoxymethylenes with low formaldehyde emission.
摘要翻译：本发明涉及一种制备包含至少一种聚甲醛和至少一种热塑性弹性体的聚合物共混物的方法，其中热塑性弹性体通过造粒工艺进行微胶体化，并且将a）中获得的颗粒分散在聚甲醛基体中，组分和这些在低剪切力下的混合，以及使用微胶体化热塑性弹性体制备低甲醛释放的聚甲醛。

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