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1. 发明授权

US4739041A Alkylated oxidized lignins as surfactants 失效
公开(公告)号：US4739041A
公开(公告)日：1988-04-19
申请号：US947226
申请日：1986-12-29
申请人： Lawrence R. Morrow , Michael G. DaGue , Lawrence E. Whittington
发明人： Lawrence R. Morrow , Michael G. DaGue , Lawrence E. Whittington
IPC分类号： B01F17/00 , B01F17/50 , C09K8/584 , C08H5/02
CPC分类号： C08H6/00 , B01F17/0028 , C09K8/584
摘要： The invention is a method of producing surfactants from lignin which comprises subjecting lignin to two reactions, alkylation with an alkyl chain having about 3 to about 24 carbon atoms at phenolic sites, and oxidation sufficient to break the lignin into smaller polymeric and monomeric units. The invention also includes using these lignin surfactants in surfactant floods for enhanced oil recovery.

2. 发明授权

US5094296A Lignin amine microemulsions 失效
标题翻译：木质素微乳液
公开(公告)号：US5094296A
公开(公告)日：1992-03-10
申请号：US591161
申请日：1990-10-01
申请人： Michael G. DaGue
发明人： Michael G. DaGue
IPC分类号： C09K8/584
CPC分类号： C09K8/584 , Y10S507/938
摘要： The invention is a method of recovering hydrocarbons from an underground hydrocarbon formation having at least one injecting well and at least one production well which comprises injecting a microemulsion into the formation through an injection well, driving said microemulsion through the formation and producing hydrocarbons through a production well, said microemulsion comprised of an internal phase of a primary amine having from about 8 to about 22 carbon atoms, lignin, a water-soluble anionic sulfonate surfactant, a solubilizer and an oil, and an external phase of brine.
摘要翻译：本发明是从具有至少一个注入井和至少一个生产井的地下烃地层回收烃的方法，其包括通过注入井将微乳液注入地层，通过生产驱动所述微乳液并通过生产产生烃所述微乳液由具有约8至约22个碳原子的伯胺的内相，木质素，水溶性阴离子磺酸盐表面活性剂，增溶剂和油以及盐水的外相组成。

3. 发明授权

US5230814A Hydrocarbon recovery comprising injecting a slug comprising oil soluble alkoxylated surfactants from lignin 失效
标题翻译：烃回收包括从木质素中注入包含油溶性烷氧基化表面活性剂的块塞
公开(公告)号：US5230814A
公开(公告)日：1993-07-27
申请号：US464480
申请日：1990-01-12
申请人： Douglas G. Naae , Michael G. DaGue , Nancy G. Dunn
发明人： Douglas G. Naae , Michael G. DaGue , Nancy G. Dunn
IPC分类号： C09K8/584
CPC分类号： C09K8/584 , Y10S507/936
摘要： A method of producing oil soluble surfactants from lignin is disclosed, along with a method for recovering oil from underground formations by means of a surfactant flooding system containing these lignin surfactants. Lignin is reduced in the presence of a carbon monoxide or hydrogen reducing agent at high temperature and pressure, alkoxylated with an .alpha.-olefin epoxide and then changed into oil soluble lignin surfactants by a reaction selected from the group consisting of sulfonation, sulfation and alkoxysulfation.
摘要翻译：公开了一种从木质素生产油溶性表面活性剂的方法，以及通过含有这些木质素表面活性剂的表面活性剂淹水系统从地下地层中回收油的方法。木质素在一氧化碳或氢还原剂存在下在高温和高压下还原，用α-烯烃环氧化物烷氧基化，然后通过选自磺化，硫酸化和烷氧基硫酸化的反应变成油溶性木质素表面活性剂。

4. 发明授权

US4435361A Corrosion inhibition system containing dicyclopentadiene sulfonate salts 失效
标题翻译：含有二环戊二烯磺酸盐的腐蚀抑制体系
公开(公告)号：US4435361A
公开(公告)日：1984-03-06
申请号：US420163
申请日：1982-09-20
申请人： Michael G. DaGue , Frederick W. Valone
发明人： Michael G. DaGue , Frederick W. Valone
IPC分类号： C09K8/54 , C23F11/04 , C04B9/02 , C09K7/00
CPC分类号： C09K8/54 , Y10S166/902 , Y10S507/939
摘要： A series of novel oil-dispersible corrosion inhibiting solutions are disclosed which contain dicyclopentadiene (3a, 4, 7, 7a-tetrahydro-4, 7 methanoindene) sulfonate salts along with an organic corrosion inhibitor in a low molecular weight solvent. The inhibiting solutions containing dicyclopentadiene sulfonate salts are effective in dramatically reducing corrosion rates in the oil field, especially pitting from hydrogen sulfide.
摘要翻译：公开了一系列新颖的油分散性腐蚀抑制溶液，其在低分子量溶剂中含有二环戊二烯（3a，4,7,7a-四氢-4,7-亚甲基茚）磺酸盐以及有机腐蚀抑制剂。含有二环戊二烯磺酸盐的抑制溶液有效地显着降低油田中的腐蚀速率，特别是从硫化氢中点蚀。

5. 发明授权

US4790382A Alkylated oxidized lignins as surfactants 失效
标题翻译：烷基化氧化木质素作为表面活性剂
公开(公告)号：US4790382A
公开(公告)日：1988-12-13
申请号：US112585
申请日：1987-10-26
申请人： Lawrence R. Morrow , Michael G. DaGue , Lawrence E. Whittington
发明人： Lawrence R. Morrow , Michael G. DaGue , Lawrence E. Whittington
IPC分类号： B01F17/00 , C09K8/584 , E21B43/22
CPC分类号： C08H6/00 , B01F17/0028 , C09K8/584 , Y10S507/936
摘要： The invention is a method of producing surfactants from lignin which comprises subjecting lignin to two reactions, alkylation with an alkyl chain having about 3 to about 24 carbon atoms at phenolic sites, and oxidation sufficient to break the lignin into smaller polymeric and monomeric units. The invention also includes using these lignin surfactants in surfactant floods for enhanced oil recovery.
摘要翻译：本发明是一种从木质素生产表面活性剂的方法，其包括使木质素进行两个反应，在酚部位用烷基链烷基化，具有约3至约24个碳原子的烷基链，以及足以将木质素破坏成更小的聚合物和单体单元的氧化。本发明还包括在表面活性剂泛滥中使用这些木质素表面活性剂以提高采收率。

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