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1. 发明授权

US5116586A Method for the reduction of nitrogen oxides from waste gases using a zeolite 失效
标题翻译：使用ZEOLITE从废气中还原氮氧化物的方法
公开(公告)号：US5116586A
公开(公告)日：1992-05-26
申请号：US448198
申请日：1989-12-14
申请人： Michael Baacke , Reinhold Beand , Bernd Engler , Akos Kiss , Peter Kleine-Mollhoff , Peter Kleinschmit , Edgar Koberstein , Mustafa Siray
发明人： Michael Baacke , Reinhold Beand , Bernd Engler , Akos Kiss , Peter Kleine-Mollhoff , Peter Kleinschmit , Edgar Koberstein , Mustafa Siray
IPC分类号： B01D53/86 , B01D53/56 , B01D53/94 , B01J29/18 , B01J29/20 , B01J29/24 , B01J29/26
CPC分类号： B01J29/26 , B01D53/9418 , B01J29/24 , B01D2251/2062 , B01D2255/2065 , B01D2255/20738 , B01D2255/20761 , B01D2255/20769 , B01D2255/50
摘要： A zeolite catalyst and a method for reduction of nitrogen oxides present in waste gas streams is described. The method includes mixing the waste gas containing nitrogen oxides with ammonia. At an elevated temperature, this mixture is passed over a zeolite catalyst. Preferably, the zeolite catalyst is in a monolithic or honeycomb form. The zeolite catalyst includes one or more of the following subgroup metals: copper, iron, molybdeum and cerium. The zeolite catalysts made in accordance with this invention show better conversion of nitrogen oxides and longer life than known catalysts.
摘要翻译：描述了沸石催化剂和还原废气流中存在的氮氧化物的方法。该方法包括将含有氮氧化物的废气与氨混合。在升高的温度下，将该混合物通过沸石催化剂。优选地，沸石催化剂为整体或蜂窝形式。沸石催化剂包括一种或多种以下亚族金属：铜，铁，钼和铈。根据本发明制备的沸石催化剂表现出比已知催化剂更好的氮氧化物转化和更长的寿命。

2. 发明授权

US5100852A Compounds of catalysts for dealkoxylation of gem-dialkoxy 失效
标题翻译：催化剂化合物用于制备二氧化硅的方法
公开(公告)号：US5100852A
公开(公告)日：1992-03-31
申请号：US163147
申请日：1988-02-25
申请人： Dietrich Arntz , Michael Baacke , Peter Kleinschmit , Guenter Prescher
发明人： Dietrich Arntz , Michael Baacke , Peter Kleinschmit , Guenter Prescher
IPC分类号： B01J29/00 , B01J29/18 , B01J29/40 , C07B61/00 , C07C41/00 , C07C41/28 , C07C43/04 , C07C43/164 , C07C67/00
CPC分类号： C07C41/28 , B01J29/18 , B01J29/40
摘要： Catalytic dealkoxylation of gem-dialkoxy compounds for synthesizing vinyl ethers is disclosed. Zeolites of the mordenite or ZSM5 type with an Na.sub.2 O/Al.sub.2 O.sub.3 molar ratio of 1:1.05 (.+-.0.25) are used as catalysts.
摘要翻译：公开了用于合成乙烯基醚的偕二烷氧基化合物的催化脱烷基化。使用Na2O / Al2O3摩尔比为1：1.05（+/- 0.25）的丝光沸石或ZSM5型沸石作为催化剂。

3. 发明授权

US4721609A Process for preparing a pentasil zeolite 失效
标题翻译：戊烷沸石的制备方法
公开(公告)号：US4721609A
公开(公告)日：1988-01-26
申请号：US903625
申请日：1986-09-02
申请人： Michael Baacke , Peter Kleinschmit
发明人： Michael Baacke , Peter Kleinschmit
IPC分类号： C01B39/36 , C07C1/20 , C01B33/28
CPC分类号： C01B39/36 , C07C1/20 , C07C2529/40 , Y10S423/22 , Y10S423/34
摘要： Templating compounds of the formula:(HO--C.sub.2 H.sub.4).sub.3 N.sup..sym. --(CH.sub.2).sub.n -N.sup..sym. (C.sub.2 H.sub.4 --OH).sub.3 2 Br.sup..crclbar.wherein n equals 3, 4 or 5 are produced by reacting triethanolamine with .alpha., .omega.dibromoalkanes, for example in the presence of a solvent. One can also react dibromoalkane with the triethanolamine in dropwise manner at reaction temperature. The product is subsequently recovered by known methods. The templating compositions can be used for the preparation of the zeolites of the pentasil types. These zeolites have the composition represented by the summary formula:(0.4-0.7)Na.sub.2 O/(0.3-0.6)Q.sub.2 O/Al.sub.2 O.sub.3 /(30-80)SiO.sub.2 /(4-10)H.sub.2 Oand have the following X-ray diffraction pattern:______________________________________ d .ANG. I/Io ______________________________________ 11.0 .+-. 0.2 30-70 10.0 .+-. 0.2 30-80 4.4 .+-. 0.1 10-20 4.3 .+-. 0.1 10-20 3.85 .+-. 0.05 100 3.74 .+-. 0.05 40-65 3.66 .+-. 0.05 20-40 3.43 .+-. 0.03 15-25 2.01 .+-. 0.02 5-15 1.99 .+-. 0.02 5-15 ______________________________________ They are prepared by utilizing an aqueous suspension of precipitated silica and mixing with an aqueous sodium aluminate composition and an aqueous solution of the template compound. This mixture is then converted under autogeneous pressure, the product is dried and then calcined. The pentasil type zeolites can be used in the conversion of methanol into hydrocarbons.
摘要翻译：式（HO-C2H4）3N（+） - （CH2）nN（+）（C2H4-OH）3 2 Br（ - ）的模板化合物其中n等于3,4或5是通过使三乙醇胺与α， ω二溴烷烃，例如在溶剂存在下。也可以在反应温度下将二溴烷烃与三乙醇胺反应一次。随后通过已知方法回收产物。模板组合物可用于制备pentasil类型的沸石。这些沸石具有由以下总结式表示的组成：（0.4-0.7）Na 2 O /（0.3-0.6）Q 2 O / Al 2 O 3 /（30-80）SiO 2 /（4-10）H 2 O，并且具有以下X射线衍射图： -d ANGSTROM I / Io -11.0 +/- 0.2 30-70 -10.0 +/- 0.2 30-80 -4.4 +/- 0.1 10-20 -4.3 +/- 0.1 10-20 -3.85 +/- 0.05 100 - 3.74 +/- 0.05 40-65 -3.66 +/- 0.05 20-40 -3.43 +/- 0.03 15-25 -2.01 +/- 0.02 5-15 -1.99 +/- 0.02 5-15 - 它们通过利用将沉淀二氧化硅的水性悬浮液与铝酸钠水溶液组合物和模板化合物的水溶液混合。然后将该混合物在自动压力下转化，产物干燥，然后煅烧。 pentasil型沸石可用于将甲醇转化为烃。

4. 发明授权

US4935218A Catalyst for the production of hydrocarbons and process for their production 失效
标题翻译：用于生产碳氢化合物的催化剂及其生产工艺
公开(公告)号：US4935218A
公开(公告)日：1990-06-19
申请号：US518403
申请日：1983-07-29
申请人： Michael Baacke , Klaus Deller , Peter Kleinschmit , Edgar Koberstein
发明人： Michael Baacke , Klaus Deller , Peter Kleinschmit , Edgar Koberstein
IPC分类号： B01J37/30 , B01J23/06 , B01J29/08 , B01J29/18 , B01J29/70 , B01J37/04 , C07C1/04
CPC分类号： C07C1/043 , B01J29/08 , B01J29/185 , B01J29/70 , C07C2523/06 , C07C2529/08 , C07C2529/18 , C07C2529/40 , Y10S423/22 , Y10S423/34
摘要： A catalyst for the production of hydrocarbon consists essentially of crystalline aluminum silicate, at least one compound of the metal zinc and/or cadmium and additionally silica. The catalyst is produced by heating a crystalline aluminum silicate, in a given case partially or completely converted to the hydrogen form, with a zinc and/or cadmium compound and molding with a silica containing binder.

5. 发明授权

US4861937A Catalysts for converting alcohols and/or aliphatic ether to unsaturated hydrocarbons and process for their production 失效
标题翻译：用于将醇和/或脂肪族醚转化为不饱和烃的催化剂及其生产方法
公开(公告)号：US4861937A
公开(公告)日：1989-08-29
申请号：US518402
申请日：1983-07-29
申请人： Michael Baacke , Klaus Deller , Peter Kleinschmit , Edgar Koberstein
发明人： Michael Baacke , Klaus Deller , Peter Kleinschmit , Edgar Koberstein
IPC分类号： B01J23/06 , B01J29/70 , B01J37/04 , C01B39/02 , C07C1/20
CPC分类号： C01B39/026 , B01J29/70 , C07C1/20 , B01J2229/26 , B01J2229/42 , C07C2529/40
摘要： Alcohols and/or aliphatic ethers are converted to hydrocarbons employing catalysts consisting of crystalline aluminum silicate, a compound of zinc and/or cadmium and additional silica. The catalyst is produced by treating a crystalline aluminum silicate, in a given case, partially or completely converted into the hydrogen form with a zinc or cadmium compound and shaping with a silica containing binder.
摘要翻译：使用由结晶硅酸铝，锌和/或镉化合物和另外的二氧化硅组成的催化剂将醇和/或脂族醚转化为烃。催化剂是通过在一定情况下处理结晶硅酸铝，用锌或镉化合物部分或完全转化为氢形式并用含二氧化硅的粘合剂进行成型来制备的。

6. 发明授权

US4564512A Process for the production of coarse particle mordenite 失效
标题翻译：粗粒子丝光沸石生产工艺
公开(公告)号：US4564512A
公开(公告)日：1986-01-14
申请号：US432294
申请日：1982-10-01
申请人： Michael Baacke , Peter Kleinschmit
发明人： Michael Baacke , Peter Kleinschmit
IPC分类号： C01B33/26 , C01B39/26 , C01B33/28
CPC分类号： C01B33/2861 , Y10S423/25
摘要： There is produced coarse particle mordenite by treating a reaction mixture consisting essentially of on a molar basis 2.5-10 Na.sub.2 O, Al.sub.2 O.sub.3, 15-30 SiO.sub.2, 400-4000 H.sub.2 O, 5-30 NaCl in an autoclave at a temperature of 140.degree. to 180.degree. C. until formation of crystals separating the crystalline product, washing with water and drying.
摘要翻译：通过在140℃至180℃的温度下，在高压釜中处理基本上以摩尔计的2.5-10Na 2 O，Al 2 O 3，15-30SiO 2，400-4000H 2 O，5-30 NaCl的反应混合物来生产粗颗粒丝光沸石直到形成分离结晶产物的晶体，用水洗涤并干燥。

7. 发明授权

US4563480A Catalyst for the production of hydrocarbons and process for their production 失效
标题翻译：用于生产碳氢化合物的催化剂及其生产工艺
公开(公告)号：US4563480A
公开(公告)日：1986-01-07
申请号：US621460
申请日：1984-06-18
申请人： Michael Baacke , Klaus Deller , Peter Kleinschmit , Edgar Koberstein
发明人： Michael Baacke , Klaus Deller , Peter Kleinschmit , Edgar Koberstein
IPC分类号： B01J37/30 , B01J23/06 , B01J29/08 , B01J29/18 , B01J29/70 , B01J37/04 , C07C1/04
CPC分类号： C07C1/043 , B01J29/08 , B01J29/185 , B01J29/70 , C07C2523/06 , C07C2529/08 , C07C2529/18 , C07C2529/40 , Y10S423/22 , Y10S423/34
摘要： A catalyst for the production of hydrocarbon consists essentially of crystalline aluminum silicate, at least one compound of the metal zinc and/or cadmium and additionally silica. The catalyst is produced by heating a crystalline aluminum silicate, in a given case partially or completely converted to the hydrogen form, with a zinc and/or cadmium compound and molding with a silica containing binder.
摘要翻译：用于生产烃的催化剂基本上由结晶硅酸铝，金属锌和/或镉的至少一种化合物和另外的二氧化硅组成。催化剂是通过在一定情况下用锌和/或镉化合物加热结晶硅酸铝，部分或完全转化为氢形式，并用含二氧化硅的粘合剂进行成型制备的。

8. 发明授权

US4481174A Crystalline aluminosilicate and process for its production 失效
标题翻译：结晶硅铝酸盐及其生产工艺
公开(公告)号：US4481174A
公开(公告)日：1984-11-06
申请号：US477874
申请日：1983-03-23
申请人： Michael Baacke , Peter Kleinschmit
发明人： Michael Baacke , Peter Kleinschmit
IPC分类号： B01J23/28 , B01J29/70 , B01J29/85 , C01B33/26 , C01B33/38 , C07C1/20 , C07C1/24 , C01G39/00
CPC分类号： B01J29/70 , C01B33/38 , C07C1/20 , C07C2529/70 , Y10S423/30
摘要： The crystalline aluminosilicate PZ 1 is produced by carrying out the crystalline in the presence of an organic template compound of the formula R.sub.3 P--(CH.sub.2).sub.n --PR.sub.3 X.sub.2 where R is a lower alkyl group, n is an integer of 2 to 6 and X is Br.sup.- or I.sup.-. The synthesis mixture has the composition:______________________________________ SiO.sub.2 /Al.sub.2 O.sub.3 = 20-250 Na.sub.2 O/SiO.sub.2 = 0.01-0.5 OH/SiO.sub.2 = 0.01-1.0 T/SiO.sub.2 = 0.01-0.2 H.sub.2 O/SiO.sub.2 = 10-40 ______________________________________ whereas T means template compound.The synthesis mixture is stirred at a temperature between 90.degree. and 200.degree. C. at autogenous pressure. The aluminosilicate PZ 1 is changed into the aluminosilicate PZ 2 by treatment with dilute acids or with ammonium chloride and subsequent calcining. This aluminosilicate PZ 2 can be employed as catalyst in the conversion of alcohols into hydrocarbons.
摘要翻译：结晶硅铝酸盐PZ 1是通过在式R3P-（CH2）n-PR3X2的有机模板化合物存在下进行结晶而制备的，其中R是低级烷基，n是2-6的整数，X是 Br-或I-。合成混合物的组成如下：-SiO2 / Al2O3 = 20-250 -Na2O / SiO2 = 0.01-0.5 -OH / SiO2 = 0.01-1.0 -T / SiO2 = 0.01-0.2 -H2O / SiO2 = 10-40-而T 指模板化合物。将合成混合物在自生压力下在90至200℃的温度下搅拌。通过用稀酸或氯化铵处理将铝硅酸盐PZ 1改变成硅铝酸盐PZ 2并随后煅烧。这种硅铝酸盐PZ 2可以用作将醇转化成烃的催化剂。

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