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1. 发明申请

US20120189525A1 Contamination Free Compression of Corrosive Gas 有权
标题翻译：腐蚀性气体的无污染压缩
公开(公告)号：US20120189525A1
公开(公告)日：2012-07-26
申请号：US13188353
申请日：2011-07-21
申请人： Matthew Sakae Forkin
发明人： Matthew Sakae Forkin
IPC分类号： C01B33/08
CPC分类号： B01J8/10 , B01J19/0073 , B01J19/18 , B01J2208/00212 , B01J2208/0046 , B01J2219/00094 , B01J2219/00146 , C01B33/10705 , Y02P20/149
摘要： A process for the synthesis of a high purity corrosive gas generated by decomposition of a precursor solid at high temperature deploys a dry vacuum pump and a compressor in series so that the corrosive gas is pressured as it fills storage containers.
摘要翻译：合成由高分子前体固体分解产生的高纯度腐蚀性气体的方法是将干式真空泵和压缩机串联在一起，使得腐蚀性气体在填充储存容器时受到压力。

2. 发明授权

US08840860B2 Contamination free compression of corrosive gas 有权
标题翻译：无腐蚀性气体的无污染压缩
公开(公告)号：US08840860B2
公开(公告)日：2014-09-23
申请号：US13188353
申请日：2011-07-21
申请人： Matthew Sakae Forkin
发明人： Matthew Sakae Forkin
IPC分类号： C01B33/08 , B01J19/18 , B01J19/00 , B01J8/10 , C01B33/107
CPC分类号： B01J8/10 , B01J19/0073 , B01J19/18 , B01J2208/00212 , B01J2208/0046 , B01J2219/00094 , B01J2219/00146 , C01B33/10705 , Y02P20/149
摘要： A process for the synthesis of a high purity corrosive gas generated by decomposition of a precursor solid at high temperature deploys a dry vacuum pump and a compressor in series so that the corrosive gas is pressured as it fills storage containers.
摘要翻译：合成由高分子前体固体分解产生的高纯度腐蚀性气体的方法是将干式真空泵和压缩机串联在一起，使得腐蚀性气体在填充储存容器时受到压力。

3. 发明申请

US20090263307A1 Silicon Production Process 审中-公开
标题翻译：硅生产工艺
公开(公告)号：US20090263307A1
公开(公告)日：2009-10-22
申请号：US12425714
申请日：2009-04-17
申请人： Leonard Nanis , Shi Yuan , Matthew Sakae Forkin
发明人： Leonard Nanis , Shi Yuan , Matthew Sakae Forkin
IPC分类号： C01B33/32 , C01B33/02
CPC分类号： C01B33/03 , C01B33/103 , C01B33/10705 , C01B33/24
摘要： An improved process for producing high purity silicon results from the reaction of sodium with pure silicon tetrafluoride gas, which produces sodium fluoride as a by-product. The silicon tetrafluoride gas is formed by decomposing sodium fluorosilicate. The sodium fluorosilicate is produced by precipitation when fluorosilicic acid (FSA) is reacted with the by-product sodium fluoride in closed loop process. Likewise, the fluorosilicic acid is preferably formed at high purity using a source material that consists essentially of silica by reacting the by-product sodium fluoride with an acid to create reactive fluoride ions.
摘要翻译：产生高纯度硅的改进方法是由钠与纯四氟化硅气体的反应产生的，其产生作为副产物的氟化钠。通过分解氟硅酸钠形成四氟化硅气体。当氟硅酸（FSA）在闭环过程中与副产物氟化钠反应时，氟硅酸钠通过沉淀产生。同样地，氟硅酸优选以高纯度形成，使用基本上由二氧化硅组成的源材料，使副产物氟化钠与酸反应以产生活性氟离子。

4. 发明申请

US20130115157A1 CALCINING CHAMBER AND PROCESS 审中-公开
标题翻译：计算室和过程
公开(公告)号：US20130115157A1
公开(公告)日：2013-05-09
申请号：US13810193
申请日：2011-07-12
申请人： Matthew Sakae Forkin
发明人： Matthew Sakae Forkin
IPC分类号： C01B33/10
CPC分类号： C01B33/10 , C01B33/10705 , F27B14/08
摘要： Solid materials capable of producing toxic and/or corrosive gases by thermal decomposition are heated in a stirred in a sealable crucible. The stirring rod is supported on a downward extending shaft using a combination of a lip seal or other mechanical seal and a ferro-fluidic seal or rotary feed through. The lip seal region is evacuated to reduce the chance that the small upward flow of corrosive gas will detrimentally react with components of the ferro-fluid. In a process for calcining sodium fluorosilicate to product silicon tetra-fluoride gas, the lip seal and ferro-fluidic seal regions are purged and/or blanked to prevent the absorption of water during an initial drying phase. A preferred embodiment of the process of synthesis of a high purity corrosive gas generated by decomposition of a precursor solid at high temperature deploys a dry vacuum pump and a compressor in series so that the corrosive gas is pressurized as it fills storage containers. Accordingly, the reaction of water with silicon tetra-fluoride to produce corrosive hydrogen fluoride gas is prevented.
摘要翻译：能够通过热分解产生有毒和/或腐蚀性气体的固体材料在可密封的坩埚中被搅拌加热。搅拌杆使用唇形密封件或其他机械密封件和铁流体密封件或旋转进料通过的组合来支撑在向下延伸的轴上。唇密封区域被抽真空以减少小的向上流动的腐蚀性气体将有害地与铁液体的组分反应的机会。在将氟硅酸钠煅烧成四氟化硅气体的过程中，唇形密封件和铁流体密封区域被清洗和/或消隐以防止在初始干燥阶段期间吸收水分。通过在高温下分解前体固体产生的高纯度腐蚀性气体的合成方法的优选实施方案是串联干燥真空泵和压缩机，使得腐蚀性气体在填充储存容器时被加压。因此，防止水与四氟化硅反应产生腐蚀性氟化氢气体。

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