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    • 1. 发明授权
    • Method for compensating for the time-dependent change in coolant level during gas sorption analysis
    • 用于补偿气体吸附分析中冷却液液位时间变化的方法
    • US06387704B1
    • 2002-05-14
    • US09550887
    • 2000-04-17
    • Martin A. ThomasNicholas N NovellaSeymour Lowell
    • Martin A. ThomasNicholas N NovellaSeymour Lowell
    • G01N3508
    • G01N15/0893G01N2015/0873Y10T436/10Y10T436/11Y10T436/115831Y10T436/12
    • For use in a sorption analysis system, a method compensating for measuring error due to the time-dependent evaporation of liquid coolant and the resulting change in the level of the coolant and temperature increase around the stem of the sample cell, during a gas sorption analysis of a sample in the sample cell. This error compensation does not inhibit coolant evaporation and is without recourse to mechanical means or other physical contrivances for causing the system to act as if the coolant were not evaporating. This method employs fixed and time-dependent data, including: changing coolant level and sample cell stem temperature changes, both of which can be obtained off-line, cold zone volume changes, and volumes of adsorptive gas transferred into the sample cell, to generate progressive error correction; whereby, system output is being corrected throughout the duration of the sorption analysis.
    • 在吸附分析系统中使用补偿液体冷却剂时间依赖性蒸发的测量误差的方法以及在气体吸附分析期间,样品池周围的冷却剂水平和温度升高的变化增加 的样品池中的样品。 该误差补偿不会阻止冷却剂的蒸发,并且不利用机械装置或其他物理设备使系统起作用,因为冷却剂不会蒸发。 该方法采用固定和时间依赖的数据,包括:改变冷却液液位和样品池温度变化,两者都可以离线获得,冷区体积变化,以及转移到样品池中的吸附气体的体积,产生 渐进式纠错; 从而,在吸附分析的整个持续时间期间系统输出被校正。